USU U PO the following questions. sono un u An MS was taken of compound 2...
Compound 2: Use the information provided below and the IR and NMR spectra on the next page to answer the following questions. a) An MS was taken of compound 2 and the table is given below. Determine the molecular formula of 2 from the MS given below relative abundance m/z 132 100 133 9.8 b) Calculate the Index of Hydrogen Deficiency/Degree of Unsaturation for the molecule. c) Using the IR spectrum and the 1H- and 13C-NMR spectra given below, determine...
Compound 3: Use the information provided below and the IR and NMR spectra on the next page to answer the following questions. a) An MS was taken of compound 3 and the table is given below. Determine the molecular formula of 3 from the MS given below. . relative abundance m/z 152 100 153 9.7 154 4.5 b) Calculate the Index of Hydrogen Deficiency/Degree of Unsaturation for the molecule. c) Using the IR spectrum and the 'H- and 13C-NMR spectra...
Compound 3: Use the information provided below and the IR and NMR spectra on the next page to answer the following questions. a) An MS was taken of compound 3 and the table is given below. Determine the molecular formula of 3 from the MS given below. m/z 166 relative abundance 100 10.9 4.5 167 168 b) Calculate the Index of Hydrogen Deficiency/Degree of Unsaturation for the molecule. c) Using the IR spectrum and the 'H- and 18C-NMR spectra given...
please can some one expalin how to get the molecular fomular and hnmr, cnmr Compound 8: Use the information provided below and the IR and NMR spectra on the next page to answer the following questions. 1) An MS was taken of compound 8 and the table is given below. Determine the molecular formula of 8 from the MS given below. relative m/z abundance 100 117 4.4 116 k) Calculate the Index of Hydrogen Deficiency/Degree of Unsaturation for the molecule...
for part a I need how to determine and draw the molecular formula part c and d is for the hnmr nad cnmr Compound 5: Use the information provided below and the IR and NMR spectra on the next page to answer the following questions. a) An MS was taken of compound 5 and the table is given below. Determine the molecular formula of 5 from the MS given below. relative abundance 138 33.3 139 m/z 2.9 b) Calculate the...
6. Characterization and Synthesis (20 points total) Use the information provided below and the IR and NMR spectra on the next page to answer the following questions. a) An MS was taken of molecule A and the table is given below. Determine the molecular formula of A from the MS given below m/z 119 118 Relative abundance (Intensity) 9.9 100 b) Calculate the Index of Hydrogen Deficiency (IHD) for the molecule in A, above. c) Using the information in a...
Example: Given the MS data below, determine the molecular formula and calculate the UN. Propose a reasonable structure for the compound. M: m/2 = 157 (100%); M+1 = 158 (9.39%) M+2 = 159 (34%)
The following slides contain 1H and 13C-NMR spectra as well as GC/MS spectra for compound 2 shown below. After analyzing the spectra, assign all proton and carbon NMR signals using the numbering given on the structure. Additionally, present your data in table form including chemical shift, integration, coupling pattern, and coupling constants (where possible). For mass spectral data, justify key fragmentations (those which are starred*) by proposing fragment structures. 5 96337 03828 047734 739073 23444 14703 3 8 9 2...
CHM 2845 (FA19) 5. The MS spectrum of a compound with formular C,H,O is shown below, Let's analyze it and deduce the structure step by step. (2 pts) MASS SPECTRUM 100 13 a. The element of unsaturation is 5 U : 209+2 - ID b. The peak at m/z=91 (combined with the EU above) strongly suggests a fragment. 134 c. The base peak at m/z-43 suggests two possibilities: and_ d. Finally the predicted structure must satisfy the EU 0.01 de...
A compound with molecular formula C7H160 displays the following IR and 'H-NMR spectra. The 13C NMR data suggest that there is some symmetry within the molecule. a) Calculate the degrees of unsaturation (DU) for the compound in the space provided below. DU = b) Identify and label the two indicated peaks in the IR spectrum in the boxes provided. Identify and label ALL peaks in the 'H NMR spectrum below. The numbers given on the 'H NMR are integration values...