Give The NMR Assignment of the Following Disaccharide molecule. Assign the Protecting Groups, the ring and the Allyl and all measurable coupling Constant. C-1 for glucose and galactose as well and C6 and C6'. Expansions, COSY and HSQC are attached for reference. (HELP PLEASE)
Homework Answers
Based o the given spectral information we have asigned the
required protons form the disaccharide molecule as below
image.
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Give The NMR Assignment of the Following Disaccharide molecule.
Assign the Protecting Groups, the ring and...
Analyze the proton and carbon NMR of toluene: PROTON_01 4632-1_Toluene 3.05 7.4 7.2 7.0 6.8 6.6...
Analyze the proton and carbon NMR of
toluene:
PROTON_01 4632-1_Toluene 3.05 7.4 7.2 7.0 6.8 6.6 6.4 6.2 6.0 5.8 5.6 5.4 5.2 5.0 4.8 4.6 4.4 4.2 4.0 3.8 3.6 3.4 3.2 3.0 2.8 2.6 2.4 2.2 CARBON_01 4632-1_Toluene o nly in the human berkaitan dengan parte do plano niyo ba libog pompuan dalam till bra prowtwinpolvontado polownload to go to the worlogulowy o palpation and play a rapid plane ploha dhawa wala hawa nila bouwen 230 220 210...
To give you more practice with analyzing NMR spectra, match each of the following 'H-NMR spectra...
To give you more practice with analyzing NMR spectra, match each of the following 'H-NMR spectra to one of the five possible compounds (structures below). Assign the NMR peaks to their respective hydrogens. Possible compounds: CH2. (H3 diethyl malonate p-ethylanisole OH 3-methylbutanal 1-pentene 1-propanol 6.0 2.0 4.8 4.6 4.4 4.2 4.0 3.8 3.6 3.4 3.2 3.0 2.8 2.6 2.4 2.2 2.0 1.8 1.6 1.4 1.2 1.0 ppm a. 1.80 1.70 1.60 1.50 1.40 1.30 3.0 ( 2.0 | 2.0 2.32...
The above is just one question. please answer the following according to the above. 1. Assign...
The above is just one question. please answer the following
according to the above.
1. Assign signals of 13C and 1H spectra as well as find the
structural unit and functional group.
2. Give the structure
sample answer - as follows
1H NMR: p-substituted Ar at 7.27-7.97 ppm, benzylic CH3 group at
2.42 ppm, COOH proton at 12.9 ppm
13C NMR: carbonyl C at 167.8 ppm (ester or acid), benzylic CH3
at 21.40 ppm, 4 remaining signals are Ar carbons,...
(a) From the spectral data ( H, C NMR, IR, MS) you were given, identify the...
(a) From the spectral data ( H, C NMR, IR, MS) you were given,
identify the structure of your product. Explain why you chose your
particular product based on the spectroscopic data.
(b) Fully assign the 1H NMR spectrum of your product (i.e.
determine which peaks in the 1H NMR correspond to which hydrogens
in the product). You will not receive full marks for determination
of the unknown unless you assign the 1H NMR spectrum
completely.
(c) Now work backwards...
Please answer the NMR tables for wintergreen and Pear, can you please make it as neat...
Please answer the NMR tables for
wintergreen and Pear, can you please make it as neat as possible
thanks!
WINTERGREEN
Pear
The procedure below is written as if you were conducting this experiment in the lab. You will nee to read through it carefully to complete the lab report and answer the questions appropriately For NMR analyses, complete the spectral assignments as shown in the example below. Example of a 'H-NMR analysis table: HoHo Ha Iodomethane Há На Chemical Shift...
Match the peaks labeled A,B,C,D,E to the Diels-Adler product and what part of the products structure...
Match the peaks labeled A,B,C,D,E to the Diels-Adler
product and what part of the products structure creates each peak
on the NMR graph.
3.60 3.58 3.56 3.54 3.52 f1 (ppm) 3.50 3.48 3.46 C (dd) 7.34 7.45 7.40 7.35 7.30 7.25 i (ppm) 7,20 7.15 7.10 B (dd) A (dt) 7.39 7.20 D (t) 4.83 E (dd) 3.53 T T 1.98 1.93 4.00 2.09 2.01 .8 7.6 7.4 7.2 7.0 6.8 6.6 6.4 6.2 6.0 5.8 5.6 5.4 f1 (ppm)...
Hi there. I am super confused and thought that this molecule was a cinnamyl ester as...
Hi there. I am super confused and thought that this molecule was
a cinnamyl ester as shown here.
This does not seem to match up with the mass spectroscopy, but
it does seem to match with NMR. Can someone please teach me what I
am missing? I've included all data below.
i
just need to identify what molecule this is because the molecular
weight does not match. Thanks!
он O0 6 ppm 7.5 7.0 6.5 6.0 5.5 5.0 4.5 4.0...
Label peaks and determine the structure of the aldehyde in the 1H NMR and 13C1H NMR:...
Label peaks and determine the structure of the
aldehyde in the 1H NMR and 13C1H NMR:
pg 1H NMR of product from aldehyde Yin CDCI3 CHCI ppm Hz Intensity 17.73 3091.6 621.6 2 7.69 3075.7 690.3 3 7.59 3036.2 1108.5 4 7.57 3027.5 1199.0 5 6.98 2793.9 961.0 6 6.95 2779.9 1320.9 76.94 2778.0 1279.1 8 6.93 2771.1 1185.2 7.60 7.55 7.50 7.45 7.40 7.35 7.30 7.25 fl (ppm) 7.20 7.15 7.10 7.057.00 6.95 6.90 OK to group CHCl3 -...
An aldol condensation reaction was performed where benzaldehyde and cyclopentanone were used. The product is 2,5...
An aldol condensation reaction was performed where benzaldehyde
and cyclopentanone were used. The product is 2,5
dibenzylidenecyclopentanone or just 2-benzylidenecyclopentanone.
The spectra correspond with the aldehyde being benzaldehyde but the
ketone used could either be acetone, cyclopentanone or cyclohexane.
I need to find the NMR spectra that correspond to cyclopentanone
being the ketone in the aldol condensation. Which NMR spectra
correspond to the correct product?
I think the second set is with cyclohexanone and not
cyclopentanone but I could be...
Write down problem number. Provide formula, HDI value, and a complete, chemically correct structure for each...
Write down problem number.
Provide formula, HDI value, and a complete, chemically correct
structure for each problem.
Assign signals in the 1H and 13C spectra to specific atoms,
identify structural units and/or functional groups.
Example:
Problem # 3
Formula: C8H8O2
HDI: 5
1H NMR: p-substituted Ar at 7.27-7.97 ppm, benzylic CH3 group at
2.42 ppm, COOH proton at 12.9 ppm
13C NMR: carbonyl C at 167.8 ppm (ester or acid), benzylic CH3
at 21.40 ppm, 4 remaining signals are Ar...
Analyze the proton and carbon NMR of
toluene:
PROTON_01 4632-1_Toluene 3.05 7.4 7.2 7.0 6.8 6.6 6.4 6.2 6.0 5.8 5.6 5.4 5.2 5.0 4.8 4.6 4.4 4.2 4.0 3.8 3.6 3.4 3.2 3.0 2.8 2.6 2.4 2.2 CARBON_01 4632-1_Toluene o nly in the human berkaitan dengan parte do plano niyo ba libog pompuan dalam till bra prowtwinpolvontado polownload to go to the worlogulowy o palpation and play a rapid plane ploha dhawa wala hawa nila bouwen 230 220 210...
To give you more practice with analyzing NMR spectra, match each of the following 'H-NMR spectra to one of the five possible compounds (structures below). Assign the NMR peaks to their respective hydrogens. Possible compounds: CH2. (H3 diethyl malonate p-ethylanisole OH 3-methylbutanal 1-pentene 1-propanol 6.0 2.0 4.8 4.6 4.4 4.2 4.0 3.8 3.6 3.4 3.2 3.0 2.8 2.6 2.4 2.2 2.0 1.8 1.6 1.4 1.2 1.0 ppm a. 1.80 1.70 1.60 1.50 1.40 1.30 3.0 ( 2.0 | 2.0 2.32...
The above is just one question. please answer the following
according to the above.
1. Assign signals of 13C and 1H spectra as well as find the
structural unit and functional group.
2. Give the structure
sample answer - as follows
1H NMR: p-substituted Ar at 7.27-7.97 ppm, benzylic CH3 group at
2.42 ppm, COOH proton at 12.9 ppm
13C NMR: carbonyl C at 167.8 ppm (ester or acid), benzylic CH3
at 21.40 ppm, 4 remaining signals are Ar carbons,...
(a) From the spectral data ( H, C NMR, IR, MS) you were given,
identify the structure of your product. Explain why you chose your
particular product based on the spectroscopic data.
(b) Fully assign the 1H NMR spectrum of your product (i.e.
determine which peaks in the 1H NMR correspond to which hydrogens
in the product). You will not receive full marks for determination
of the unknown unless you assign the 1H NMR spectrum
completely.
(c) Now work backwards...
Please answer the NMR tables for
wintergreen and Pear, can you please make it as neat as possible
thanks!
WINTERGREEN
Pear
The procedure below is written as if you were conducting this experiment in the lab. You will nee to read through it carefully to complete the lab report and answer the questions appropriately For NMR analyses, complete the spectral assignments as shown in the example below. Example of a 'H-NMR analysis table: HoHo Ha Iodomethane Há На Chemical Shift...
Match the peaks labeled A,B,C,D,E to the Diels-Adler
product and what part of the products structure creates each peak
on the NMR graph.
3.60 3.58 3.56 3.54 3.52 f1 (ppm) 3.50 3.48 3.46 C (dd) 7.34 7.45 7.40 7.35 7.30 7.25 i (ppm) 7,20 7.15 7.10 B (dd) A (dt) 7.39 7.20 D (t) 4.83 E (dd) 3.53 T T 1.98 1.93 4.00 2.09 2.01 .8 7.6 7.4 7.2 7.0 6.8 6.6 6.4 6.2 6.0 5.8 5.6 5.4 f1 (ppm)...
Hi there. I am super confused and thought that this molecule was
a cinnamyl ester as shown here.
This does not seem to match up with the mass spectroscopy, but
it does seem to match with NMR. Can someone please teach me what I
am missing? I've included all data below.
i
just need to identify what molecule this is because the molecular
weight does not match. Thanks!
он O0 6 ppm 7.5 7.0 6.5 6.0 5.5 5.0 4.5 4.0...
Label peaks and determine the structure of the
aldehyde in the 1H NMR and 13C1H NMR:
pg 1H NMR of product from aldehyde Yin CDCI3 CHCI ppm Hz Intensity 17.73 3091.6 621.6 2 7.69 3075.7 690.3 3 7.59 3036.2 1108.5 4 7.57 3027.5 1199.0 5 6.98 2793.9 961.0 6 6.95 2779.9 1320.9 76.94 2778.0 1279.1 8 6.93 2771.1 1185.2 7.60 7.55 7.50 7.45 7.40 7.35 7.30 7.25 fl (ppm) 7.20 7.15 7.10 7.057.00 6.95 6.90 OK to group CHCl3 -...
An aldol condensation reaction was performed where benzaldehyde
and cyclopentanone were used. The product is 2,5
dibenzylidenecyclopentanone or just 2-benzylidenecyclopentanone.
The spectra correspond with the aldehyde being benzaldehyde but the
ketone used could either be acetone, cyclopentanone or cyclohexane.
I need to find the NMR spectra that correspond to cyclopentanone
being the ketone in the aldol condensation. Which NMR spectra
correspond to the correct product?
I think the second set is with cyclohexanone and not
cyclopentanone but I could be...
Write down problem number.
Provide formula, HDI value, and a complete, chemically correct
structure for each problem.
Assign signals in the 1H and 13C spectra to specific atoms,
identify structural units and/or functional groups.
Example:
Problem # 3
Formula: C8H8O2
HDI: 5
1H NMR: p-substituted Ar at 7.27-7.97 ppm, benzylic CH3 group at
2.42 ppm, COOH proton at 12.9 ppm
13C NMR: carbonyl C at 167.8 ppm (ester or acid), benzylic CH3
at 21.40 ppm, 4 remaining signals are Ar...
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