assign peaks for the following spectra 4.0 5.0 9.0 10.0 10. min Peak R. Time 2.135...
i need help interpreting this for my unknown! please help. All I know is that it is a liquid amine, with boiling point 190-193 celcius. Unknown Determination 26,919,406 10.0 10 Peak R. Time 3.503 Peak Report TIC Area 82229865 82229865 Area% 100.00 100.00 50 60 30 90 100 110 120 130 140 150 160 170 180 CDC3 QE 300
Directly compare your own GCMS data to the three different stock GCMS data sets. CIGC Yukki 7 10000 3.488 Spoctrum 102030405060为80 90 100 110 120 10 140 150 160 170 180 190 Spectrum Peak Repet TIC Area Ast 28a86 100 4.118 Page 1 of 3 10 20 30 40 60 Prak Repon TIC Are Anat 2 4117 Page 2 of 3 TIC 1.00 min Spectnan 0 10 20 0 70300 10 120 140 150 160 170 10 190 Spectrum 0...
1) Which compound gives the following spectra? For the 'H-NMR assign all signals. Interpret base peak and mole peak in the mass spectrum if a mole peak exists. Assign at least two "C signals. How does the IR spectrum support your findings? (12 pts.) 100- Relative Intensity 0- 20 40 60 80 100 140 160 180 200 220 120 m/ 200 180 160 140 120 100 80 60 40 20 0 ppm t6H 9,4H 11H d, 2 H 9 8...
Use the spectra below to determine the molecular formula and chemical structure of the unknown compound. MASS 142 % of Base Peak 1147 40 50 70 80 5 100 % Transmittance Jari- 3000 1000 4000 'H NMR 300 MERE 2000 Wavenumber (cm) 3.0 25 20 15 Ppm 4.0 3.5 C/DEPT NMR 75.5 MHz ppm 60 50 40 80 70 90 100 110 120 170 160 150 140 130 ppm 4.5 4.0 3.5 3.0 2.5 2.0 1.5 ppm COSY 300 MHz...
Which compound gives the following spectra? For the 1H-NMR assign all signals. interpret mol peak and base peak in the mass spectrum if a mole peak exists. Assign at least two 13C signals. How does the IR spectrum support your finding? Check 200 180 160 120 80 60 40 20 0 140 a 100 ppm s, 3H t, 3 H d. 2 a. 2 H d. 2H s, 1 H 1 10 9 8 7 6 4 3 2 1...
Identify the the H-nmr and C-nmr peaks/signmas of ethyl acetate. 2 33 4.0 3.5 3.0 2.5 20 Chemical Shit (ppm) 13C 60 150 140 130 120 110 100 70 170 160 90 50 40 30 20 60z 8 09 171.8
Suggest a composition for the halogen compound whose mass spectrum is shown below and assign the labeled peaks. 127 100 173 160 158 162 25 48 TITTHTT 160 170 91 208 79 35 160 173 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 127 100 173 160 158 162 25 48 TITTHTT 160 170 91 208 79 35 160 173 30 40 50 60 70 80 90 100...
8. (10 points) The following spectra correspond to compounds AE listed below con pound to its corresponding spestre Label very simal on the spectrum (as Co . ctc.). Spectrum CDCI, 190 160 170 160 150 140 130 120 110 100 80 80 Spectrum 2 70 80 50 40 30 20 10 O le CDCI, 190 180 170 180 150 140 130 120 110 100 90 80 70 60 50 40 30 20 10 O de CDCI, 190 180 170 180...
(a) From the spectral data ( H, C NMR, IR, MS) you were given, identify the structure of your product. Explain why you chose your particular product based on the spectroscopic data. (b) Fully assign the 1H NMR spectrum of your product (i.e. determine which peaks in the 1H NMR correspond to which hydrogens in the product). You will not receive full marks for determination of the unknown unless you assign the 1H NMR spectrum completely. (c) Now work backwards...
please help me figure out what the compound is. thanks MASS % of Base Peak 1387 S47 677 957 123 50 60 70 80 90 100 110 120 130 140 awamp % Transmittance -2958 -2870 -16701 -13811 -1246 -903 STS TTT 4000 3000 1000 2000 Wavenumber (cm-') 'H NMR 300 MHz N 1750 1740 Hz 640 Hz 570 560 Hz 300 290 Hz 6.0 5.5 5.0 4.5 4.0 3.5 3.0 2.5 2.0 1.5 ppm 13C/DEPT NMR 75.5 MHz 200 180...