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11. Provide reagents (or a combination of reagents) that will bring about transformations. (4 pts total)...
SUR- 4. Diagram a flow chart (similar to the one on page 31) of the exact...
SUR- 4. Diagram a flow chart (similar to the one on page 31) of the exact extraction that you performed. Be sure to include labels for all layers and all structures, both organic and ionic. 5. Write an acid/base reaction for all of the exact reactions that you performed during this experiment. Acid Base Disolve in organie solvent (ether or CH.01.) Extract with NaHCO, pune layer Ho Extract with NaOH (4) organe layer separate water layer Na Extract with Ha...
Acidic compound: Ethyl 4 aminobenzoate Neutral compound: Fluorenone (12 points). Separation Scheme:_(5 points for the aqueous...
Acidic compound: Ethyl 4 aminobenzoate
Neutral compound: Fluorenone
(12 points). Separation Scheme:_(5 points for the aqueous extract or layer and 7 points for the organic extract or layer). By drawing the actual structures of the neutral compound that you have identified and either the acidic or basic compound or impurity present in your mixture, write a separation scheme for this binary mixture. Draw the appropriate complete structures with the correnct number of unshared electrons and/ or charges if any during...
A student has a mixture of butanoic acid (liquid) and phenol ( ) (solid). The mixture...
A student has a mixture of butanoic acid (liquid) and phenol ( ) (solid). The mixture is almost (1:1). The pas for both compounds are 4 -5 and 10 respectively. Both compounds are soluble in ether (organic solvent that is insoluble in water). Select the best technique to separate and recover each compounds. Recrystallization. Use strong basic water as a solvent and recover the solid while leaving the liquid behind. Add acid to recover the butanoic acid. Recrystallization. Use ether...
Attached below are the pages from this lab report to help give context to the questions....
Attached below are the pages from this lab report to help give
context to the questions. Please be as detailed as possible when
answering the questions and include any relevant information about
intermolecular forces at play. Thank you for your help!
Here are the questions which I need answered. Thank you in
advance for your help! :) Please be as detailed as possible and
discuss any intermolecular forces in detail if they are relevant to
the question. Thanks!
PARTA. SEPARATION...
Liquid-Liquid Extraction P14. Your instructor gives you 1g of a 50:50 mixture of the following solids...
Liquid-Liquid Extraction P14. Your instructor gives you 1g of a 50:50 mixture of the following solids and asks you to separate them from one another. First you dissolve the mixture in ether: methyl trains-cinnamate OH trans-cinnamic acid OMe mp 34-38°c mp 133°C Using what you learned in P11-P12, complete the extraction plan below (aqueous acid or base should be added?): Aqueous solution of added Top layer: circle one (aqueous or organic?) Bottom layer: circle one (aqueous or organic?) Beaker compounds...
Acid/Base Extraction 1. Provide a flow chart detailing the acid/base extraction/separation of the compounds shown below....
Acid/Base Extraction
1. Provide a flow chart detailing the acid/base
extraction/separation of the compounds shown below. Your answer
must employ the following reagents: methylene chloride,
hydrochloric acid (1M & 6M), sodium hydroxide (1M & 6M),
10% sodium bicarbonate (aq). Clearly indicate the product(s) and
layers formed following each step of your separation scheme.
IMPORTANT: p-cresol is soluble in sodium hydroxide solution but
insoluble in neutral water or sodium bicarbonate solution. 2-
ethylbenzoic acid is soluble in both sodium hydroxide and...
Provide a flow chart detailing the acid/base extraction/separation of the compounds show below. Your answer must...
Provide a flow chart detailing the acid/base extraction/separation of the compounds show below. Your answer must employ the following reagents: methylene chloride, hydrochloric acid (1M & 6M), sodium hydroxide (1M & 6M), 10% sodium bicarbonate (aq). Clearly indicate the product(s) and layers formed following each step of your separation scheme. IMPORTANT: p-cresol is soluble in sodium hydroxide solution but insoluble in neutral water or sodium bicarbonate solution. 2-ethylbenzoic acid is soluble in both sodium hydroxide and sodium bicarbonate solutions. Use...
Experiment 3.5B Acid / Base Separations scheme worksheet Consider the following acid base separation scheme. Initialy,...
Experiment 3.5B Acid / Base Separations scheme worksheet Consider the following acid base separation scheme. Initialy, all compounds are dissolved in methylene chiloride and tne solution is extracted by 10% HCI . You will finish the extraction scheme with the following reagents: 10% HCI, 10% NaOH, Na SO Be sore to inclede the reagents and steps required so finish the estraction scheme. In the boses indicate which compounds (structures) are present in each layer after the extraction steps. (More than...
Post-Lab 3. You vigourously shake a separatory funnel, and notice an emulsion forming. What can you...
Post-Lab 3. You vigourously shake a separatory funnel, and notice an emulsion forming. What can you do to help break up the emulsion? 4. Complete the following acid-base reaction and provide the keq. Is sodium bicarbonate (NaHCO) a suitable base in this situation? + NaHCO, 5. A mixture of benzoic acid and a neutral nonpolar compound is dissolved in ether and mixed thoroughly with aqueous sodium bicarbonate. What is the organic chemical species that is present in the ether layer?...
Extraction of benzoic acid and 9-fluorenone using diethyl ether. (please do not include ethyl 4- aminobenzoate)....
Extraction of benzoic acid and 9-fluorenone using diethyl ether. (please do not include ethyl 4- aminobenzoate). I have to create a flow chart to diagram the key steps of the experiment and isolation of products. 0.100g of benzoic acid and 9-fluorenone are dissolved in diethyl ether. The extraction solvent is 5% sodium hydroxide (to extract the acidic component from the organic phase). Saturated sodium chloride is added to the organic layer. drying the organic solution: anhydrous sodium sulfate is added...
SUR- 4. Diagram a flow chart (similar to the one on page 31) of the exact extraction that you performed. Be sure to include labels for all layers and all structures, both organic and ionic. 5. Write an acid/base reaction for all of the exact reactions that you performed during this experiment. Acid Base Disolve in organie solvent (ether or CH.01.) Extract with NaHCO, pune layer Ho Extract with NaOH (4) organe layer separate water layer Na Extract with Ha...
Acidic compound: Ethyl 4 aminobenzoate
Neutral compound: Fluorenone
(12 points). Separation Scheme:_(5 points for the aqueous extract or layer and 7 points for the organic extract or layer). By drawing the actual structures of the neutral compound that you have identified and either the acidic or basic compound or impurity present in your mixture, write a separation scheme for this binary mixture. Draw the appropriate complete structures with the correnct number of unshared electrons and/ or charges if any during...
A student has a mixture of butanoic acid (liquid) and phenol ( ) (solid). The mixture is almost (1:1). The pas for both compounds are 4 -5 and 10 respectively. Both compounds are soluble in ether (organic solvent that is insoluble in water). Select the best technique to separate and recover each compounds. Recrystallization. Use strong basic water as a solvent and recover the solid while leaving the liquid behind. Add acid to recover the butanoic acid. Recrystallization. Use ether...
Attached below are the pages from this lab report to help give
context to the questions. Please be as detailed as possible when
answering the questions and include any relevant information about
intermolecular forces at play. Thank you for your help!
Here are the questions which I need answered. Thank you in
advance for your help! :) Please be as detailed as possible and
discuss any intermolecular forces in detail if they are relevant to
the question. Thanks!
PARTA. SEPARATION...
Liquid-Liquid Extraction P14. Your instructor gives you 1g of a 50:50 mixture of the following solids and asks you to separate them from one another. First you dissolve the mixture in ether: methyl trains-cinnamate OH trans-cinnamic acid OMe mp 34-38°c mp 133°C Using what you learned in P11-P12, complete the extraction plan below (aqueous acid or base should be added?): Aqueous solution of added Top layer: circle one (aqueous or organic?) Bottom layer: circle one (aqueous or organic?) Beaker compounds...
Acid/Base Extraction
1. Provide a flow chart detailing the acid/base
extraction/separation of the compounds shown below. Your answer
must employ the following reagents: methylene chloride,
hydrochloric acid (1M & 6M), sodium hydroxide (1M & 6M),
10% sodium bicarbonate (aq). Clearly indicate the product(s) and
layers formed following each step of your separation scheme.
IMPORTANT: p-cresol is soluble in sodium hydroxide solution but
insoluble in neutral water or sodium bicarbonate solution. 2-
ethylbenzoic acid is soluble in both sodium hydroxide and...
Provide a flow chart detailing the acid/base extraction/separation of the compounds show below. Your answer must employ the following reagents: methylene chloride, hydrochloric acid (1M & 6M), sodium hydroxide (1M & 6M), 10% sodium bicarbonate (aq). Clearly indicate the product(s) and layers formed following each step of your separation scheme. IMPORTANT: p-cresol is soluble in sodium hydroxide solution but insoluble in neutral water or sodium bicarbonate solution. 2-ethylbenzoic acid is soluble in both sodium hydroxide and sodium bicarbonate solutions. Use...
Experiment 3.5B Acid / Base Separations scheme worksheet Consider the following acid base separation scheme. Initialy, all compounds are dissolved in methylene chiloride and tne solution is extracted by 10% HCI . You will finish the extraction scheme with the following reagents: 10% HCI, 10% NaOH, Na SO Be sore to inclede the reagents and steps required so finish the estraction scheme. In the boses indicate which compounds (structures) are present in each layer after the extraction steps. (More than...
Post-Lab 3. You vigourously shake a separatory funnel, and notice an emulsion forming. What can you do to help break up the emulsion? 4. Complete the following acid-base reaction and provide the keq. Is sodium bicarbonate (NaHCO) a suitable base in this situation? + NaHCO, 5. A mixture of benzoic acid and a neutral nonpolar compound is dissolved in ether and mixed thoroughly with aqueous sodium bicarbonate. What is the organic chemical species that is present in the ether layer?...
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