Question

Compound G is a common contaminant in synthetic 2-chloro-2-methylbutane prepared from a tertiary alcohol. Using an...

Compound G is a common contaminant in synthetic 2-chloro-2-methylbutane prepared from a tertiary alcohol. Using an appropriate purification technique learnt in Organic Chemistry I, recover the pure product. You should also write a short essay or draw a separation scheme on the exercise.

0 0
Add a comment Improve this question Transcribed image text
Answer #1

The reaction proceeds via SN1 mechanism the product will be separated due to decreased water solubility the product will be analysed by silver nitrate test

Tertiary alcohol has good yield. Concentrator hydrogen halides are used in this reaction tertiary alcohol (2-methyl-2-butanol) will be converted to tertiary alkyl chloride (2-chloro-2-methyl butane) using concentrated hydrochloric acid

The hydroxide oxygen atom of 2 methyl 2 butanol is protonated with HCl which turns the group into a releasing group water is then expelled to generate awater is the finally at chloride ions attack the intermediate to carbo cation to give 2 chloro 2 methyl butane4-C\ +47 Mechanism ༩AA 4 4, + A– ༩A3 c-c༠༣་ ༢༢3 A ༦4 -04་་་་ ] ,, ་ ་ CHz 4 - ཨཱ༠༥ ཙག ༥ 4༩ -c-4༠4 ༩ ཡc4 +4 c elcrokeng Ctch P

2 chloro 2 methyl butane in across ethanol indicate very little precipitation of the substituent.These results in the sharp contrast earlier reports on secondary 2 chloro methyl substituted system

Add a comment
Know the answer?
Add Answer to:
Compound G is a common contaminant in synthetic 2-chloro-2-methylbutane prepared from a tertiary alcohol. Using an...
Your Answer:

Post as a guest

Your Name:

What's your source?

Earn Coins

Coins can be redeemed for fabulous gifts.

Not the answer you're looking for? Ask your own homework help question. Our experts will answer your question WITHIN MINUTES for Free.
Similar Homework Help Questions
  • EXERCISE # 3: Separation and Workup - (5 points; max time :15 minutes) Example b) Compound...

    EXERCISE # 3: Separation and Workup - (5 points; max time :15 minutes) Example b) Compound G is a common contaminant in synthetic 2 chloro 2 methyl butarie prepared froma tertiary alcohol, Using an appropriate purification technique learnt in CHE 201 recover pure the product. You should also write a short essay or draw a separation scheme on the exercise (as you would in your lab notebook).

  • You are working in a synthetic organic chemistry lab and you need to prepare 9.19 g of 2-chloro-2-methylbutane. The give...

    You are working in a synthetic organic chemistry lab and you need to prepare 9.19 g of 2-chloro-2-methylbutane. The given literature procedure typically results in a 75% experimental (isolated) yield for the preparation of the desired compound Question 1:  To ensure that you isolate the correct amount of material, what mass of product should you aim to prepare in this experiment? Enter a mass in grams, accurate to one decimal place. ____________ g Question 2:  What volume of 2-methyl-2-butanol should be used?...

  • Synthesis using Carbonyla-Substitution Chemistry Preamble This experiment involves the synthesis of target molecules using a-substitution chemistry....

    Synthesis using Carbonyla-Substitution Chemistry Preamble This experiment involves the synthesis of target molecules using a-substitution chemistry. You are assigned two target molecules, one of which is best synthesized by an alkylation approach, while the other is best synthesized by an addition or condensation approach. My two target molecules are number 2 and number 12 in the last page. You must do the following: 1. Perform a retrosynthetic analysis on the two target molecules assigned to you. In each case the...

  • need work and answers IlI. Preparation of Synthetic Eugenol (10 pts) Eugenol, the main component of clove oil, can be prepared from heating 2-allyl guaiacol (in the absence of oxygen) to tempera...

    need work and answers IlI. Preparation of Synthetic Eugenol (10 pts) Eugenol, the main component of clove oil, can be prepared from heating 2-allyl guaiacol (in the absence of oxygen) to temperatures>205 °C. In practice, however, it is most cost effective to extract eugenol from cloves, its natural source. Given a weight percentage of eugenol in cloves at-15%, calculate the minimum mass of cloves one needs to obtain 1.00 g of eugenol as product? Report your answer below. Show your...

  • Page 1 Synthesis using Carbonyl O-Substitution Chemistry Preamble This experiment involves the synthesis of target molecules...

    Page 1 Synthesis using Carbonyl O-Substitution Chemistry Preamble This experiment involves the synthesis of target molecules using a-substitution chemistry. You are assigned two target molecules, one of which is best synthesized by an alkylation approach, while the other is best synthesized by an addition or condensation approach. You must do the following: 1. Perform a retrosynthetic analysis on the two target molecules assigned to you. In each case the organic starting material (what you have to work backwards toward) depends...

  • **(left structure)****(right structure)** The two structures for the assignment are above and the task is: 1....

    **(left structure)****(right structure)** The two structures for the assignment are above and the task is: 1. Perform a retrosynthetic analysis on the two target molecules assigned to you. In each case the organic starting material (what you have to work backwards toward) depends upon the target. For the structure given above (structure on left), the starting material is either malonic ester or acetoacetic ester and any halide. For the structure given above (structure on right), the starting material is any...

  • Working on the questions at the end of this lab report (see above). I need help answering questio...

    Working on the questions at the end of this lab report (see above). I need help answering questions 2, 3, and 4 completely and thoroughly. Thank you! s, until the I hexano 1 clean disti CYCLOHEXENE from CYCLOHEXANOL be dehydrated with solfuric acid to yield cyclohexene and waterf Add a 0°C (record ct and cal H,SO + H20 ainer. s in purification of any crude product are (a) the preliminary separation of the product from the reaction mixture by distillation...

  • Experiment Write Up Proposal You will write up a synthesis procedure for one reaction that could...

    Experiment Write Up Proposal You will write up a synthesis procedure for one reaction that could be potentially run in a face- to-face Chem 2321 lab session. Your proposal will include an introduction and procedure. The procedure will include step-by-step instructions for running the reaction (including reaction monitoring), work-up. (product isolation and purification), and analysis (characterization). You will need to include sample calculations for percent yield and provide sample spectra analysis. You must upload your proposal as a single document...

  • Need help, numbers 3-6 please show work. and fill out table of chemicals for all chemical...

    Need help, numbers 3-6 please show work. and fill out table of chemicals for all chemical used. calculate mmol in the table as well show work please and each of these must be listed in its own row. There are 10 column headings: IUPAC name OR common name, structure, CAS number (Chemical Abstract Service number) molecular mass, melting point (if applicable), boiling point (if applicable), solubility (in water, if applicable), density, amounts to be used in the experiment, and the...

ADVERTISEMENT
Free Homework Help App
Download From Google Play
Scan Your Homework
to Get Instant Free Answers
Need Online Homework Help?
Ask a Question
Get Answers For Free
Most questions answered within 3 hours.
ADVERTISEMENT
ADVERTISEMENT
ADVERTISEMENT