Complete the reaction equations for the chemistry that took
place when the organic layer was extracted with the aqueous acid.
Cross out analyte that is no longer present in the organic layer
during the extraction (the analyte that was extracted by base).
Write NR if it does not react. Indicate which later, organic or
aqueous each analyte compound would be.
Homework Answers
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Complete the reaction equations for the chemistry that took
place when the organic layer was extracted...
Complete the reactions equations for the chemistry that took place when the organic layer was extracted....
Complete the reactions equations for the chemistry that took
place when the organic layer was extracted. Cross out analyte that
is no longer present and indicate which layer it would be
opts) Complete the reaction equations for the chemistry that took place when the organic layer was extracted with aqueous acid (reaction with H2O*). Cross out the analyte that is no longer present in the organic layer during the extraction with aqueous acid (i.e. the analyte that was extracted by...
Complete the rxn equations that place with your analyte compound when you extracted with aqueous base...
Complete the rxn equations that place with your analyte compound
when you extracted with aqueous base solution. Write NR if analyte
compound doesnt react. Indicate which layer, organic or aqueous
each would be
compound does not react. Indicate which layer, organic or aqueous, eac base extraction. Hoy NO₂ con O-H OO-H HN "NO2
Identify which compound appeared on your TLC plate where the aqueous acid, aqueous base, and organic...
Identify which compound appeared on your TLC plate where the
aqueous acid, aqueous base, and organic layers were spotted. Liquid
extraction technique involved benzophenone, m-nitroaniline, and
m-nitrobenzoic acid
(3pts) Identify which compound appeared on your TLC plate where the aqueous acid, aqueous base, and organic layers were spotted. Org. 3-nitrobenzoic acid Aq. Ac. Aq. Ba. 101
Organic chemistry post-lab question: "Why is important to add the alkyl halide dropwise in your reaction?...
Organic chemistry post-lab question: "Why is important
to add the alkyl halide dropwise in your reaction? (Hint: your
reaction is not heated, but you still need a water-cooled
condenser!)" Please answer in detail!
Here is a copy of the experiment, thank you!
The Grignard reaction is an important synthetic process by which a carbon-carbon bond is formed. Magnesium metal is first reacted with an organic halide. The resultant organo-magnesium halide (Grignard reagent) is then combined with a carbonyl compound, ultimately...
Construct a flow chart describing the seperation of the mixture and the isolation of each compound...
Construct a flow chart describing the seperation of the
mixture and the isolation of each compound in this experiment. (Lab
steps/procedures includes for reference)
4. Construct a flow chart describing the separation of the mixture and the isolation of each compound in this experiment. A commonly used method of separating a mixture of organic compounds is known as liquid-liquid extraction. Most reactions of organic compounds require extraction at some stage of product purification. In this experiment you will use extraction...
Organic Chemistry Lab question In the experiment we did acid-base extractions to find impurities. The impurity...
Organic Chemistry Lab question In the experiment we did acid-base extractions to find impurities. The impurity was either benzoic acid (acid) or 4-chloroaniline (base) So in this experiment we did Acid-Base extraction with an unknown compound. So we had an unknown of 0.150 grams and mixed it with 20 mL of diethyl ether. We placed this in a separatory funnel and added 2mL of 1.0 NaOH solution to the separatory funnel and placed the stopper over the top of the...
Experiment Write Up Proposal You will write up a synthesis procedure for one reaction that could...
Experiment Write Up Proposal You will write up a synthesis procedure for one reaction that could be potentially run in a face- to-face Chem 2321 lab session. Your proposal will include an introduction and procedure. The procedure will include step-by-step instructions for running the reaction (including reaction monitoring), work-up. (product isolation and purification), and analysis (characterization). You will need to include sample calculations for percent yield and provide sample spectra analysis. You must upload your proposal as a single document...
1 - Provide a balanced equation for this reaction 2 - Provide a mechanism for the...
1 - Provide a balanced equation for this reaction
2 - Provide a mechanism for the transformation of cyclohexanol
into cyclohexanone
3 - Provide a flow chart for the workup procedure for isolating
cyclohexane from all the by-products, making sure to note in which
layer you expect to find your product in each extraction.
4 - Provide the theoretical yield of cyclohexane in this
experiment.
PROCEDURE OXIDATION OF CYCLOHEXANOL TO CYCLOHEXANONE Set up a water bath as the heat source...
Grignard Reaction with a Ketone: Triphenylmethanol Introduction: The purpose of this lab is to prepare phenylmagnesium...
Grignard Reaction with a Ketone: Triphenylmethanol Introduction: The purpose of this lab is to prepare phenylmagnesium bromide, a Grignard reagent, and react it with benzophenone to give triphenylmethanol. Grignard reagents are very reactive and must be synthesized in an environment free of water or any other source of potential proton donor. Once made, the Grignard reagent will do a nucleophilic attack on the carbonyl carbon of the ketone, benzophenone. The result is an alkoxide that is then protonated to give...
Need help, numbers 3-6 please show work. and fill out table of chemicals for all chemical...
Need help, numbers 3-6 please show work. and fill out table of
chemicals for all chemical used.
calculate mmol in the table as well show work please
and each of these must be listed in its own row. There are 10 column headings: IUPAC name OR common name, structure, CAS number (Chemical Abstract Service number) molecular mass, melting point (if applicable), boiling point (if applicable), solubility (in water, if applicable), density, amounts to be used in the experiment, and the...
Complete the reactions equations for the chemistry that took
place when the organic layer was extracted. Cross out analyte that
is no longer present and indicate which layer it would be
opts) Complete the reaction equations for the chemistry that took place when the organic layer was extracted with aqueous acid (reaction with H2O*). Cross out the analyte that is no longer present in the organic layer during the extraction with aqueous acid (i.e. the analyte that was extracted by...
Complete the rxn equations that place with your analyte compound
when you extracted with aqueous base solution. Write NR if analyte
compound doesnt react. Indicate which layer, organic or aqueous
each would be
compound does not react. Indicate which layer, organic or aqueous, eac base extraction. Hoy NO₂ con O-H OO-H HN "NO2
Identify which compound appeared on your TLC plate where the
aqueous acid, aqueous base, and organic layers were spotted. Liquid
extraction technique involved benzophenone, m-nitroaniline, and
m-nitrobenzoic acid
(3pts) Identify which compound appeared on your TLC plate where the aqueous acid, aqueous base, and organic layers were spotted. Org. 3-nitrobenzoic acid Aq. Ac. Aq. Ba. 101
Organic chemistry post-lab question: "Why is important
to add the alkyl halide dropwise in your reaction? (Hint: your
reaction is not heated, but you still need a water-cooled
condenser!)" Please answer in detail!
Here is a copy of the experiment, thank you!
The Grignard reaction is an important synthetic process by which a carbon-carbon bond is formed. Magnesium metal is first reacted with an organic halide. The resultant organo-magnesium halide (Grignard reagent) is then combined with a carbonyl compound, ultimately...
Construct a flow chart describing the seperation of the
mixture and the isolation of each compound in this experiment. (Lab
steps/procedures includes for reference)
4. Construct a flow chart describing the separation of the mixture and the isolation of each compound in this experiment. A commonly used method of separating a mixture of organic compounds is known as liquid-liquid extraction. Most reactions of organic compounds require extraction at some stage of product purification. In this experiment you will use extraction...
Experiment Write Up Proposal You will write up a synthesis procedure for one reaction that could be potentially run in a face- to-face Chem 2321 lab session. Your proposal will include an introduction and procedure. The procedure will include step-by-step instructions for running the reaction (including reaction monitoring), work-up. (product isolation and purification), and analysis (characterization). You will need to include sample calculations for percent yield and provide sample spectra analysis. You must upload your proposal as a single document...
1 - Provide a balanced equation for this reaction
2 - Provide a mechanism for the transformation of cyclohexanol
into cyclohexanone
3 - Provide a flow chart for the workup procedure for isolating
cyclohexane from all the by-products, making sure to note in which
layer you expect to find your product in each extraction.
4 - Provide the theoretical yield of cyclohexane in this
experiment.
PROCEDURE OXIDATION OF CYCLOHEXANOL TO CYCLOHEXANONE Set up a water bath as the heat source...
Need help, numbers 3-6 please show work. and fill out table of
chemicals for all chemical used.
calculate mmol in the table as well show work please
and each of these must be listed in its own row. There are 10 column headings: IUPAC name OR common name, structure, CAS number (Chemical Abstract Service number) molecular mass, melting point (if applicable), boiling point (if applicable), solubility (in water, if applicable), density, amounts to be used in the experiment, and the...
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