In a hypothetical experiment, a student performs an extraction by shaking 25.0 mL mineral oil with 50.0 mL of 1.00 M I2 aqueous solution. After allowing the layers to separate the student observes that the mineral oil layer has become purple in color, indicating that some of the I2 has been transferred from the aqueous layer to the mineral oil layer. The student then removes the aqueous layer and titrates it with 5.00 mM Na2S2O3 solution. At the endpoint of the titration, the student measures that 13.2 mL of the Na2S2O3 solution was needed to react completely with the remaining I2. Calculate the distribution coefficient for I2 between mineral oil and water for this experiment. Show all work.
In a hypothetical experiment, a student performs an extraction by shaking 25.0 mL mineral oil with...
please answer all these questions, thank you.
CHEM 242L Exp. 4 Report/ Synthesis of Oil of Wintergreen Name Score: 20 1) Assess the effectiveness of the experiment and your technique by A) reporting the yield of each step in grams and percent as well as the overall percent yield (What is "overall percent yield?). SHOW ALL CALCULATIONS! B) Give a complete analysis of the identity and purity of your final product and any isolated intermediates 2 What was the purpose...
1. Procedure A. Lithium 2,6-dimethylphenoxide. In a 300-ml. flask, equipped with a magnetic stirrer and a reflux condenser and flushed with nitrogen, are placed 150 ml. of toluene (freshly distilled from sodium), 1.40 g. (0.202 mole) of lithium metal (Note 1) and 25.0 g. (0.205 mole) of resublimed 2,6-dimethylphenol. The mixture is heated under reflux with stirring for 36 hours; a nitrogen atmosphere is maintained for the reflux period (Note 2). The condenser is replaced by a distillation head with...
Experiment Write Up Proposal You will write up a synthesis procedure for one reaction that could be potentially run in a face- to-face Chem 2321 lab session. Your proposal will include an introduction and procedure. The procedure will include step-by-step instructions for running the reaction (including reaction monitoring), work-up. (product isolation and purification), and analysis (characterization). You will need to include sample calculations for percent yield and provide sample spectra analysis. You must upload your proposal as a single document...