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PART 1 - For the following compounds A. Predict how many signals would be detected in...
need help understanjng what the expected would be molecular formula is C4H6ClN HNMR Spectrum chemical shift,...
need help understanjng what the expected would be molecular
formula is C4H6ClN
HNMR Spectrum chemical shift, Hz 1200 900 2400 2100 1800 1500 600 3000 2.147 2.104 absorption 0.SHE 2,578 16.01 3.678 8 - 5 6 2 4 3 chemical shift, ppm (8) Observed Chemical Shift Table F: 'HNMR Functional Group Analysis Structural Expected Functional Group Fragment Name Chemical Structural Formula Shift Functionalized Structural Fragment 3.672 CH2-CH2 2.578 CH2-CH2 2.1256 CH2-CH2-CH2N HC-CN 2005 Chemical shift, st R-H or CH can...
7. Which compound below best fits the following spectral data? 8. How many signals would you...
7. Which compound below best fits the following
spectral data?
8. How many signals would you expect to see in the
broadband decoupled C^13 spectra of the following compounds?
9. If a proton gave an NMR signal at 3.2 ppm on a MHz
NMR, what would the chemical shift be of this proton (in ppm) if
the sample was run in 400 MHz NMR?
7. Which compound below best fits the following spectral data? (6 points) H-1 NMR 0.9 ppm...
4. Predict the number of signals in a 'H NMR spectrum for (CH2),CHOCH,CH, pts A. One...
4. Predict the number of signals in a 'H NMR spectrum for (CH2),CHOCH,CH, pts A. One signal Two signals Three signals Four signals Five signals B. 5. Identify a compound that has a formula of C 6,0 and a 'H NMR signal at 89.5. A. A carboxylic acid B. An aldehyde A ketone An ester An alcohol C. D.
2. List the expected spectral data of 2-ethyl-3-hydroxy-hexanal observed from an IR, a 'H-NMR and mass...
2. List the expected spectral data of 2-ethyl-3-hydroxy-hexanal observed from an IR, a 'H-NMR and mass spectrum. CH3 -CH2 CH C-Hal C-N C-o CEC Intensity CEN Aromatic C=C C=0 220 200 180 160 140 120 60 40 20 0 ppm 100 80 Chemical shift (8) Intensity Bonding C-H Type of Vibration (Stretching unless noted) alkane CH -CH, alkene w-m m w-m bending bending out-of-plane bending alkyne arene Frequency (cm) 2850-3000 1375 and 1450 1450-1475 3000-3100 650-1000 3300 3030 690-900 2720...
6) The IR-, 1H- and 13C-spectra of an unknown sample having the formula C8H1602 are shown...
6) The IR-, 1H- and 13C-spectra of an unknown sample having the formula C8H1602 are shown on the next page. a) What can you conclude about the structure form the 13C NMR data ? b) What functional group is present ? Explain your rational c) Propose a structure that is consistent with the spectroscopic data ? 8 8 3 3 8 3000 innn 500 400 2000 1500 Wavenumber[cm-11 TR2009-87586TK 13C NMR NB: solvent peaks have been edited out. 140 120...
Thank you so much to anyone who decides to help me with this page. I am very grateful! 1. (4pts) How many signal...
Thank you so much to anyone who decides to help me
with this page. I am very grateful!
1. (4pts) How many signals do you expect each of the following compounds to have in its 'H NMR spectrum? Write the appropriate number below to each structure. OH OH H 2. (5.5pts) Use your spectrOscopy data table to identify the chemical shift range in which each of the identified signals in the folowing molecule wDuld be lournd in the 'H NMR...
Write down problem number. Provide formula, HDI value, and a complete, chemically correct structure for each...
Write down problem number.
Provide formula, HDI value, and a complete, chemically correct
structure for each problem.
Assign signals in the 1H and 13C spectra to specific atoms,
identify structural units and/or functional groups.
Example:
Problem # 3
Formula: C8H8O2
HDI: 5
1H NMR: p-substituted Ar at 7.27-7.97 ppm, benzylic CH3 group at
2.42 ppm, COOH proton at 12.9 ppm
13C NMR: carbonyl C at 167.8 ppm (ester or acid), benzylic CH3
at 21.40 ppm, 4 remaining signals are Ar...
How to do a summary on this compound: 1)mention how many signals there are in the...
How to do a summary on this compound:
1)mention how many signals there are in the NMR and what this
means.
2) Find the location of the signals and describe what they
mean.(ex peak 1.3 could indicate a possible CH>CH2>CH3)
3)Talk about the integrals and the possible number of hydrogen's
there could be based on the other integrals.
4)Discuss the signal splitting and how many neighbors each
proton has.
intensity 0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9...
7. Which compound below be H-1 NMR 0.9 ppm (quartet fits the following spectral data? (6...
7. Which compound below be H-1 NMR 0.9 ppm (quartet fits the following spectral data? (6 points) 1.2 ppm (sextet 2 hydrogens), 2.1 ppm (triplet, hydrogens), 4.3 ppm (singlet 3 hydrogens) C-13 NMR 5 signals 25 ppr ppm (CH2); 61 ppm: (CH3) 198 Ppm (C). IR strong peak 1735 cm Ignals 25 ppm (CH): 35 ppm (CH2), 46 ppm (CH2); 61 ppm: em Mass Spee parent M+ = 102 Mass Spec paren ou 0 H2 CH3 HjC Holo H3C- CC...
1. How many signals do you expect to see in the 'H NMR of the following...
1. How many signals do you expect to see in the 'H NMR of the following compounds? Label each H and use the same label (eg. Ha) for any equivalent H's. CH, CH CH CH O CH, CH,CHCHCHCH3 CH2CH2CH OCHCH; CH3 CH3 CH 2. For each compound label the proton or set of protons that gives the signal at the highest chemical shift (largest ppm) a next highest band so on. H CHỊCH,CH, SOCH, CH,CH, CH CH3CHCHCH
need help understanjng what the expected would be molecular
formula is C4H6ClN
HNMR Spectrum chemical shift, Hz 1200 900 2400 2100 1800 1500 600 3000 2.147 2.104 absorption 0.SHE 2,578 16.01 3.678 8 - 5 6 2 4 3 chemical shift, ppm (8) Observed Chemical Shift Table F: 'HNMR Functional Group Analysis Structural Expected Functional Group Fragment Name Chemical Structural Formula Shift Functionalized Structural Fragment 3.672 CH2-CH2 2.578 CH2-CH2 2.1256 CH2-CH2-CH2N HC-CN 2005 Chemical shift, st R-H or CH can...
7. Which compound below best fits the following
spectral data?
8. How many signals would you expect to see in the
broadband decoupled C^13 spectra of the following compounds?
9. If a proton gave an NMR signal at 3.2 ppm on a MHz
NMR, what would the chemical shift be of this proton (in ppm) if
the sample was run in 400 MHz NMR?
7. Which compound below best fits the following spectral data? (6 points) H-1 NMR 0.9 ppm...
4. Predict the number of signals in a 'H NMR spectrum for (CH2),CHOCH,CH, pts A. One signal Two signals Three signals Four signals Five signals B. 5. Identify a compound that has a formula of C 6,0 and a 'H NMR signal at 89.5. A. A carboxylic acid B. An aldehyde A ketone An ester An alcohol C. D.
2. List the expected spectral data of 2-ethyl-3-hydroxy-hexanal observed from an IR, a 'H-NMR and mass spectrum. CH3 -CH2 CH C-Hal C-N C-o CEC Intensity CEN Aromatic C=C C=0 220 200 180 160 140 120 60 40 20 0 ppm 100 80 Chemical shift (8) Intensity Bonding C-H Type of Vibration (Stretching unless noted) alkane CH -CH, alkene w-m m w-m bending bending out-of-plane bending alkyne arene Frequency (cm) 2850-3000 1375 and 1450 1450-1475 3000-3100 650-1000 3300 3030 690-900 2720...
6) The IR-, 1H- and 13C-spectra of an unknown sample having the formula C8H1602 are shown on the next page. a) What can you conclude about the structure form the 13C NMR data ? b) What functional group is present ? Explain your rational c) Propose a structure that is consistent with the spectroscopic data ? 8 8 3 3 8 3000 innn 500 400 2000 1500 Wavenumber[cm-11 TR2009-87586TK 13C NMR NB: solvent peaks have been edited out. 140 120...
Thank you so much to anyone who decides to help me
with this page. I am very grateful!
1. (4pts) How many signals do you expect each of the following compounds to have in its 'H NMR spectrum? Write the appropriate number below to each structure. OH OH H 2. (5.5pts) Use your spectrOscopy data table to identify the chemical shift range in which each of the identified signals in the folowing molecule wDuld be lournd in the 'H NMR...
Write down problem number.
Provide formula, HDI value, and a complete, chemically correct
structure for each problem.
Assign signals in the 1H and 13C spectra to specific atoms,
identify structural units and/or functional groups.
Example:
Problem # 3
Formula: C8H8O2
HDI: 5
1H NMR: p-substituted Ar at 7.27-7.97 ppm, benzylic CH3 group at
2.42 ppm, COOH proton at 12.9 ppm
13C NMR: carbonyl C at 167.8 ppm (ester or acid), benzylic CH3
at 21.40 ppm, 4 remaining signals are Ar...
How to do a summary on this compound:
1)mention how many signals there are in the NMR and what this
means.
2) Find the location of the signals and describe what they
mean.(ex peak 1.3 could indicate a possible CH>CH2>CH3)
3)Talk about the integrals and the possible number of hydrogen's
there could be based on the other integrals.
4)Discuss the signal splitting and how many neighbors each
proton has.
intensity 0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9...
7. Which compound below be H-1 NMR 0.9 ppm (quartet fits the following spectral data? (6 points) 1.2 ppm (sextet 2 hydrogens), 2.1 ppm (triplet, hydrogens), 4.3 ppm (singlet 3 hydrogens) C-13 NMR 5 signals 25 ppr ppm (CH2); 61 ppm: (CH3) 198 Ppm (C). IR strong peak 1735 cm Ignals 25 ppm (CH): 35 ppm (CH2), 46 ppm (CH2); 61 ppm: em Mass Spee parent M+ = 102 Mass Spec paren ou 0 H2 CH3 HjC Holo H3C- CC...
1. How many signals do you expect to see in the 'H NMR of the following compounds? Label each H and use the same label (eg. Ha) for any equivalent H's. CH, CH CH CH O CH, CH,CHCHCHCH3 CH2CH2CH OCHCH; CH3 CH3 CH 2. For each compound label the proton or set of protons that gives the signal at the highest chemical shift (largest ppm) a next highest band so on. H CHỊCH,CH, SOCH, CH,CH, CH CH3CHCHCH
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