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Spectroscopic Analysis Unknown 1: Molecule Number a) Determine the empirical formula from the microanalysis data, showing...
Spectroscopic Analysis Unknown 1: Molecule Number a) Determine the empirical formula from the microanalysis data, showing your working: Empirical Formula b) Does the mass spectrum imply the molecular formula is the same as the empirical formula? Why/Why not? Molecular Formula c) Use the 'double bond equivalents' formula to determine the degree on unsaturation for this molecule: d) What structural information can you garner from the IR spectrum? e) What structural information can you garner from the 'H NMR spectrum? Specify...
Spectroscopic Analysis Unknown 1: Molecule Number a) Determine the empirical formula from the microanalysis data, showing your working: Empirical Formula b) Does the mass spectrum imply the molecular formula is the same as the empirical formula? Why/Why not? Molecular Formula c) Use the 'double bond equivalents' formula to determine the degree on unsaturation for this molecule: d) What structural information can you garner from the IR spectrum? e) What structural information can you garner from the 'H NMR spectrum? Specify...
Data Interpretation - Molecular Formula Based on the following microanalysis data and mass spectrum, determine the molecular formula for the molecule. Elemental Analysis: C, 57.84; H, 3.64; 0, 38.52 100 MS-NW-8142 80 60 Relative Intensity 40 20 o tommittit 25 50 75 125 150 100 m/z Select one: Cg H₂O4 O C5H.02 C4H₂O₂ C10H8O4 o C₂H₂O
Based on the following spectroscopic data of an unknown compound with molecular formula C8H6S, (i) determine the chemical structure of this compound; (ii) assign all the signals in the 1H-NMR spectrum & 13C-NMR spectrum. NMR is complete ۳۳-۳-rr-T-------- IR Spectrum (KBr disc) 4000 3000 1200 800 2000 1600 V (cm) M ** = 13 Mass Spectrum بالليليللليلعليا % of base peak CgHES 40 80 200 240 280 120 m 160 /e 13C NMR Spectrum (100.0 MHz, CDCI, solution) expansion DEPT...
An unknown compound A has an empirical formula of c3h6o and a molecular ion peak in its mass spectrum at m/z 116. It also has no IR absorption at 3200-3600cm^-1 but shows a peak at 1740cm^-1. The H NMR spectra data of A is given below in table format. Use this information to answer questions a-d below. 9 (15 Points). An unknown compound A has empiricl rmula of C,HO and a molecular ion peak in its mass spectrum at an...
thanks for the help! Consider an unknown compound with the following molecular formula and spectral data: CH3O2 a. Calculate the degrees of unsaturation for the formula. b. Draw a structure consistent with the spectral data. IR Spectrum CHO, 4000 3000 1800 1200 800 8 Mass Spectrum M12 8 8 No significant UV absorption above 220 mm 9 C6H802 240 220 40 80 120 160 200 13C NMR Spectrum (100 MHE, COCI, DEPT со сно сне prolon de coupled 200 TH...
NMR Exercise Lab Determine the structure of the following unknown organic compounds from the 'H and C NM below. When supplying spectroscopic information for parts b-c below, be sure to give units appropriately when identifying specific peaks in a spectrum that are associated with specific portions of the structural formula that you give in part a. (a) Provide a structural formula which is consistent with all of the given information; give the degrees of unsaturation (DoU). (b) For the 15'C...
1. What is the chemical formula of the unknown? 2. what is the mass of the unknown? 3. What is the HDI? 4. According to IR spectra, what functional groups are present? 5. What is the structure of the molecule? 138 PRACTICAL SPECTROSCOPY Compound 80 is a liquid (boiling point 212 C), that can be prepared by the reaction of Compound 79 with acidic, anhydrous ethanol. The Mass, IR, and 'H NMR spectra, along with C NMR data, are given...
For the following questions, provide the following information. (1) Ifa molecular formula is provided, indicate the units of unsaturation in this molecule. (2) Label any important relevant peaks in the IR spectrum by indicating which type of bond it corresponds to (3) If the integration is not provided in the 'H NMR spectrum, determine the integration for each signal in th spectrum (4) Examine the mass spectrum carefully. If I have placed an asterisk above a peak, propose a valid...
determine the structure of your unknown from the molecular formula, IR, and 13C NMR spectra. assign all of your 13C NMR absorptions. IR & 1C NMR Lab Unknown Your group's mission is to determine the structure of your unknown from the molecular forrmula, IR and 13C NMR spectra. Assign all of your C NMR absorptions. You want to know which resonances correspond to which parts of the product's structure. The best way to do this is to draw a picture...