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1. A TLC experiment is performed to separate a mixture of the compounds shown below. 5.2...
1. A TLC experiment is performed to separate a mixture of the compounds shown below. Label...
1. A TLC experiment is performed to separate a mixture of the compounds shown below. Label each chemical with the appropriate letter based off the TLC data. (2 points) • B OCH 2. What would happen to the Rivalues for your compounds if 30:70 hexane:acetone were used as the developing solvent instead of 70:30 hexane:acetone? Briefly explain why. (2 points) 3. After first using 90:10 hexane:acetone as the solvent, we switched to 70:30 hexane:acetone. Why did we not use 70:30...
why is the mel di Using the TLC slide drawn below, calculate the Rr values for...
why
is the mel
di Using the TLC slide drawn below, calculate the Rr values for each spot. See page /o in the lab manual for help. b. State which of the three known substances are present in the unknown by comparing the Unknown Rr values to the Rx values for the Known substances. See page 76 in the lab manual for help. You will need a metric ruler. Solvent front- Origin of spot lu 1 2 3 U =...
2. A solution containing a mixture of naphthalene, benzoic acid, and benzaldehyde is analyzed via TLC...
2. A solution containing a mixture of naphthalene, benzoic acid, and benzaldehyde is analyzed via TLC and GC. Use the structures and properties of the compounds to aid in answering the following questions. A. In the TLC experiment, the mixture is spotted on a silica TLC plate and eluted with a 1:1 mixture of hexanes and ethyl acetate. Three spots are observed on the plate, with Re values of 0.25, 0.58, and 0.74. Indicate which spot corresponds to which compound....
if applicacable, please write clear stepwise mechanism for all synthetic transformations, showing important internediates where appropriate....
if applicacable, please write clear stepwise mechanism for all
synthetic transformations, showing important internediates where
appropriate. only do this if applicable for this lab.
Experiment SD Column Chromatography Running the Reaction. Once sodium borohydride has been added to the reaction meture Isee next paragraph take samples at the times just indicated. Because this must be done in such a short time you must be well prepared before starting the reaction. One person should be the timekeeper, and the other person...
1. (5 pt.) Soon you will synthesize the analgesic acetanilide in lab. It’s m.p. is 114C....
1. (5 pt.) Soon you will synthesize the analgesic acetanilide in lab. It’s m.p. is 114C. What does it indicate about your product if you obtain a m.p. of 103 - 112C. Explain. 2. (6 pt.) Neither aniline nor nitrobenzene is particularly water soluble. However, one is completely soluble in dilute aqueous HCl. Which one is soluble, and explain why? (For maximum credit, provide a chemical equation for your answer.) 3. (5 pt.) Name the two adsorbents that are most...
Didn't post this right the first time. Here is everything in full! Need help with Organic...
Didn't post this right the first time. Here is everything in
full!
Need help with Organic Chemistry, understanding the labs.
1. Soon you will synthesize the analgesic acetanilide in lab. It's me is 114°C. What does it indicate about your product if you obtain a mn of 103 - 112°C. Explain. acetanilide YO 2. Neither aniline nor nitrobenzene is particularly water soluble. However, one is completely soluble in dilute aqueous HCI. Which one is soluble, and explain why? (For maximum...
Need help, numbers 3-6 please show work. and fill out table of chemicals for all chemical...
Need help, numbers 3-6 please show work. and fill out table of
chemicals for all chemical used.
calculate mmol in the table as well show work please
and each of these must be listed in its own row. There are 10 column headings: IUPAC name OR common name, structure, CAS number (Chemical Abstract Service number) molecular mass, melting point (if applicable), boiling point (if applicable), solubility (in water, if applicable), density, amounts to be used in the experiment, and the...
Experiment Write Up Proposal You will write up a synthesis procedure for one reaction that could...
Experiment Write Up Proposal You will write up a synthesis procedure for one reaction that could be potentially run in a face- to-face Chem 2321 lab session. Your proposal will include an introduction and procedure. The procedure will include step-by-step instructions for running the reaction (including reaction monitoring), work-up. (product isolation and purification), and analysis (characterization). You will need to include sample calculations for percent yield and provide sample spectra analysis. You must upload your proposal as a single document...
1. A TLC experiment is performed to separate a mixture of the compounds shown below. Label each chemical with the appropriate letter based off the TLC data. (2 points) • B OCH 2. What would happen to the Rivalues for your compounds if 30:70 hexane:acetone were used as the developing solvent instead of 70:30 hexane:acetone? Briefly explain why. (2 points) 3. After first using 90:10 hexane:acetone as the solvent, we switched to 70:30 hexane:acetone. Why did we not use 70:30...
why
is the mel
di Using the TLC slide drawn below, calculate the Rr values for each spot. See page /o in the lab manual for help. b. State which of the three known substances are present in the unknown by comparing the Unknown Rr values to the Rx values for the Known substances. See page 76 in the lab manual for help. You will need a metric ruler. Solvent front- Origin of spot lu 1 2 3 U =...
2. A solution containing a mixture of naphthalene, benzoic acid, and benzaldehyde is analyzed via TLC and GC. Use the structures and properties of the compounds to aid in answering the following questions. A. In the TLC experiment, the mixture is spotted on a silica TLC plate and eluted with a 1:1 mixture of hexanes and ethyl acetate. Three spots are observed on the plate, with Re values of 0.25, 0.58, and 0.74. Indicate which spot corresponds to which compound....
if applicacable, please write clear stepwise mechanism for all
synthetic transformations, showing important internediates where
appropriate. only do this if applicable for this lab.
Experiment SD Column Chromatography Running the Reaction. Once sodium borohydride has been added to the reaction meture Isee next paragraph take samples at the times just indicated. Because this must be done in such a short time you must be well prepared before starting the reaction. One person should be the timekeeper, and the other person...
Didn't post this right the first time. Here is everything in
full!
Need help with Organic Chemistry, understanding the labs.
1. Soon you will synthesize the analgesic acetanilide in lab. It's me is 114°C. What does it indicate about your product if you obtain a mn of 103 - 112°C. Explain. acetanilide YO 2. Neither aniline nor nitrobenzene is particularly water soluble. However, one is completely soluble in dilute aqueous HCI. Which one is soluble, and explain why? (For maximum...
Need help, numbers 3-6 please show work. and fill out table of
chemicals for all chemical used.
calculate mmol in the table as well show work please
and each of these must be listed in its own row. There are 10 column headings: IUPAC name OR common name, structure, CAS number (Chemical Abstract Service number) molecular mass, melting point (if applicable), boiling point (if applicable), solubility (in water, if applicable), density, amounts to be used in the experiment, and the...
Experiment Write Up Proposal You will write up a synthesis procedure for one reaction that could be potentially run in a face- to-face Chem 2321 lab session. Your proposal will include an introduction and procedure. The procedure will include step-by-step instructions for running the reaction (including reaction monitoring), work-up. (product isolation and purification), and analysis (characterization). You will need to include sample calculations for percent yield and provide sample spectra analysis. You must upload your proposal as a single document...
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