Question

1)How would you synthesize the following product from the assigned reactants?

a. You have to show the shortest and most effective reaction schemes using the ONLY given compounds as carbon sources to make the product. You can use proper reagent(s) for each step.

b. Only two reactants allowed to build the carbon backbone are shown below.

c. Explain how you would confirm each step using 1H-NMR, 13C-NMR, IR, and UV-Vis spectroscopie. (no spectrums needed)

o - and to make Use

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Answer #1


NBS NAOE ChemN MR TH Estimation Br O 7.90 D) Bb37THF OH 7.30 2.78 KMnOy OH OH à H₂O₂/ Naolt (exess) OH 7.42 2.10 7.24 2.78 P2

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