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2. Please write down the proton NMR range in the table Hz (ketones) (3) R$C=CH2 (terminal...
2. List the expected spectral data of 2-ethyl-3-hydroxy-hexanal observed from an IR, a 'H-NMR and mass...
2. List the expected spectral data of 2-ethyl-3-hydroxy-hexanal observed from an IR, a 'H-NMR and mass spectrum. CH3 -CH2 CH C-Hal C-N C-o CEC Intensity CEN Aromatic C=C C=0 220 200 180 160 140 120 60 40 20 0 ppm 100 80 Chemical shift (8) Intensity Bonding C-H Type of Vibration (Stretching unless noted) alkane CH -CH, alkene w-m m w-m bending bending out-of-plane bending alkyne arene Frequency (cm) 2850-3000 1375 and 1450 1450-1475 3000-3100 650-1000 3300 3030 690-900 2720...
NMR IR CAN YOU PLEASE ANSWER AS SOON AS POSSIBLE THANK YOU PLEASE EXPLAIN IT IN DETAIL THANK YOU Experimental Data Only report the IR absorptions that provide diagnosis...
NMR
IR
CAN YOU PLEASE ANSWER AS SOON AS POSSIBLE THANK
YOU
PLEASE EXPLAIN IT IN DETAIL THANK YOU
Experimental Data Only report the IR absorptions that provide diagnosis for the major functional groups. Copies of your spectra will be included in your lab report with this information written on the spectra. However, the information should also be included in the body of the report in a text format similar to the example given below IR cm1: 1735 (C-o); MS:...
Please help identify conpound Sample A8 PPM DATE: 04/12/10 (09:15) AB FIR 60.010 SWI: 1000 PW:...
Please help identify conpound
Sample A8 PPM DATE: 04/12/10 (09:15) AB FIR 60.010 SWI: 1000 PW: 19.6 OF 1: 368.7 USER: PTSid: 8192 EX: HIV.ppg PD: 3.0 sec INAS Nutstemp 1605 3064 486 %Transmittance 2874 556 2895 746 3028 2932 1453 1496 269 772 3500 3000 1500 1000 500 2500 2000 Wavenumbers (cm-1) Date: Fri Oct 29 11:30:24 2010 (GMT-07:00) AB KBr Scans: 16 Resolution: 2.000 Name Organic Chemistry 2242 Spectroscopy Unknown A (S-05) During this lab period, you are...
please identify the unknown and write a derivative Unknown compound 3 Clear liquid Physcial Properties Solubility...
please identify the unknown and write a derivative
Unknown compound 3 Clear liquid Physcial Properties Solubility Dissolve in ethyl ether Not dissolved in water Boiling point 77 IR spectrum Transmitance 3000 1000 2000 Wavenumber cm-1) Classification Positive test in Alkaline Iron (III) Hydroxamate test test CLASSIFICATION TESTS These tests must be done together with known AND FOLLOW PROCEDURE IN YOUR TEXT CARBOXYLIC ACIDS are detected by teating aqueous solutions with limus or pH paper. Also, disolve In NaHCO with bubbles...
Grignard reagent THE GRIGNARD REAGENT-PREPARATION AND REACTION In this experiment, you will prepa...
i need help with the postlab questions please
Grignard reagent THE GRIGNARD REAGENT-PREPARATION AND REACTION In this experiment, you will prepare a Grignard reagent, phenyl magnesium bromide, from bromobenzene and magnesium metal. The Grignard reagent will then react with methyl benzoate to form triphenylmethanol. Introduction Grignard reagents, such as organomagnesium halides, were discovered in 1910 by French chemist Victor Grignard. The Grignard reaction is one of the most general methods for carbon- carbon bond formation in all of organic chemistry....
2. List the expected spectral data of 2-ethyl-3-hydroxy-hexanal observed from an IR, a 'H-NMR and mass spectrum. CH3 -CH2 CH C-Hal C-N C-o CEC Intensity CEN Aromatic C=C C=0 220 200 180 160 140 120 60 40 20 0 ppm 100 80 Chemical shift (8) Intensity Bonding C-H Type of Vibration (Stretching unless noted) alkane CH -CH, alkene w-m m w-m bending bending out-of-plane bending alkyne arene Frequency (cm) 2850-3000 1375 and 1450 1450-1475 3000-3100 650-1000 3300 3030 690-900 2720...
NMR
IR
CAN YOU PLEASE ANSWER AS SOON AS POSSIBLE THANK
YOU
PLEASE EXPLAIN IT IN DETAIL THANK YOU
Experimental Data Only report the IR absorptions that provide diagnosis for the major functional groups. Copies of your spectra will be included in your lab report with this information written on the spectra. However, the information should also be included in the body of the report in a text format similar to the example given below IR cm1: 1735 (C-o); MS:...
Please help identify conpound
Sample A8 PPM DATE: 04/12/10 (09:15) AB FIR 60.010 SWI: 1000 PW: 19.6 OF 1: 368.7 USER: PTSid: 8192 EX: HIV.ppg PD: 3.0 sec INAS Nutstemp 1605 3064 486 %Transmittance 2874 556 2895 746 3028 2932 1453 1496 269 772 3500 3000 1500 1000 500 2500 2000 Wavenumbers (cm-1) Date: Fri Oct 29 11:30:24 2010 (GMT-07:00) AB KBr Scans: 16 Resolution: 2.000 Name Organic Chemistry 2242 Spectroscopy Unknown A (S-05) During this lab period, you are...
please identify the unknown and write a derivative
Unknown compound 3 Clear liquid Physcial Properties Solubility Dissolve in ethyl ether Not dissolved in water Boiling point 77 IR spectrum Transmitance 3000 1000 2000 Wavenumber cm-1) Classification Positive test in Alkaline Iron (III) Hydroxamate test test CLASSIFICATION TESTS These tests must be done together with known AND FOLLOW PROCEDURE IN YOUR TEXT CARBOXYLIC ACIDS are detected by teating aqueous solutions with limus or pH paper. Also, disolve In NaHCO with bubbles...
i need help with the postlab questions please
Grignard reagent THE GRIGNARD REAGENT-PREPARATION AND REACTION In this experiment, you will prepare a Grignard reagent, phenyl magnesium bromide, from bromobenzene and magnesium metal. The Grignard reagent will then react with methyl benzoate to form triphenylmethanol. Introduction Grignard reagents, such as organomagnesium halides, were discovered in 1910 by French chemist Victor Grignard. The Grignard reaction is one of the most general methods for carbon- carbon bond formation in all of organic chemistry....
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