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Analyze the NMR of benzoic acid
Product Name:Benzoic acid CAS: 65-85-0 89.56 MHz 0.040 g: 0.5...
Please analyze the IR and NMR spectra. The product is N,N-diethyl-m-toluamide. The product is obtained by...
Please analyze the IR and NMR spectra. The product is
N,N-diethyl-m-toluamide. The product is obtained by the following
reactions
Please label all major peaks.
Solvent is Et2O. Extracted with NaOH and then HCl and then
H2O. Dried and then evaporated. To further purify, hexane was used
in column chromatography to elute the product. Then
evaporated.
CH3 CH3 SOCI2 + SO2 O=0 ОН CH3 CH3 -- + excess (CH3CH2)2NH + (CH3CH2)2NH2* crt ether CI 'N-CH2CH3 CH,CHE 1000 11 100 100 100...
Analyze the attached product NMR spectrum. Justify the structure of your final product and deduce the...
Analyze the attached product NMR spectrum. Justify the
structure of your final product and deduce the identity of your
unknown starting material.
Provide a reaction mechanism using the starting material that
you deduced in Qu. 1.
Experimental Procedure In this experiment. Vou will perform a double reductive amination reac an unknown aldehyde to form the corresponding amine product determine the identity of the unknown starting material. reaction between ethylenediamine and oduct. Analyze the lab data obtained to HẠN NHA RE...
Please analyze the IR and NMR spectra. How pure it is? What impurities can be observed?...
Please analyze the IR and NMR spectra. How pure it is? What
impurities can be observed? Please label all major signals. The
product is N,N-diethyl-m-toluamide. The product is obtained by the
following reactions
Solvent is Et2O. Extracted with NaOH and then HCl and then
H2O. Dried and then evaporated. To further purify the product,
hexane was added to perform column chromatography.
Evaporated.
Clearer image for the IR image:
CH3 CH3 SOCI2 + SO2 O=0 ОН CH3 CH3 -- + excess...
analyze the peaks of the IR and NMR precipit 1act the crude pr sto a 50-ml....
analyze the peaks of the IR and NMR
precipit 1act the crude pr sto a 50-ml. Ind P nal until it is um filtra action flask Administrator Analyst Monday, June 10, 2019 3:49 PM Date 104 100 95 90 85 37m-1 2633 78cm-1 80 101.cm-1 2964 30-1 75- 1411 4153.99 2867 77cm-1 70 458.92 1044 05cm t 3369 72m-1 65 927.87 8 74m-1 60 249 96om-1 1064 47cm-1 9e-1 55 131.74dm-1 50- 67384cm-1 t1047am 45 701.90cm-1 13711cm-1 40- 847 01m-1...
The proton nmr and the infrared spectra of DCC, DMAP, DCU, the product and the nmrs...
The proton nmr and the infrared spectra of DCC, DMAP, DCU, the
product and the nmrs of the starting materials and products are
shown. These are labeled Compounds A, B and C. a.Which nmr is the
product?
b. Which is the nmr of the starting material?
c. What is the mixture of compounds shown as compound C?
tert-Butyl Ethyl Fumarate DCC, DMAP, CHCI OH Chemical Formula: C,H,O Chemical Formula: CH 0 Molecular Weight: 144.13 Molecular Weight: 74.12 Chemical Formula: CH...
Please identify all relevant peaks in both the IR and NMR for methyl 3-nitrobenzoate, please use...
Please identify all relevant peaks in both the IR and NMR for
methyl 3-nitrobenzoate, please use the following chart as a
template, thank you!
Spectral Database for Organic Compounds SDBS Japanese Introduction Disclaimer HELP Contact What's New RIO-DB FAQ LINK . AIST SDBS-H NMRSDBS No. 3528HSP-49-719 Cg H7 N04 methyl m-nitrobenzoate 399.65 MHz 0.038 g: 0.5 ml CDC13 9 8 7 6 4 3 2 1 5 ppm HSP-49-719 {AH 1 0 —CH, (E) ON -H (C) (BH HID) Spectral...
Please identify all relevant peaks in both the IR and NMR for methyl 3-nitrobenzoate, please use...
Please identify all relevant peaks in both the IR and NMR for
methyl 3-nitrobenzoate, please use the following chart as a
template, thank you!
Spectral Database for Organic Compounds SDBS Japanese Introduction Disclaimer HELP Contact What's New RIO-DB FAQ LINK . AIST SDBS-H NMRSDBS No. 3528HSP-49-719 Cg H7 N04 methyl m-nitrobenzoate 399.65 MHz 0.038 g: 0.5 ml CDC13 9 8 7 6 4 3 2 1 5 ppm HSP-49-719 {AH 1 0 —CH, (E) ON -H (C) (BH HID) Spectral...
Please analyze the IR and NMR spectra. The product is
N,N-diethyl-m-toluamide. The product is obtained by the following
reactions
Please label all major peaks.
Solvent is Et2O. Extracted with NaOH and then HCl and then
H2O. Dried and then evaporated. To further purify, hexane was used
in column chromatography to elute the product. Then
evaporated.
CH3 CH3 SOCI2 + SO2 O=0 ОН CH3 CH3 -- + excess (CH3CH2)2NH + (CH3CH2)2NH2* crt ether CI 'N-CH2CH3 CH,CHE 1000 11 100 100 100...
Analyze the attached product NMR spectrum. Justify the
structure of your final product and deduce the identity of your
unknown starting material.
Provide a reaction mechanism using the starting material that
you deduced in Qu. 1.
Experimental Procedure In this experiment. Vou will perform a double reductive amination reac an unknown aldehyde to form the corresponding amine product determine the identity of the unknown starting material. reaction between ethylenediamine and oduct. Analyze the lab data obtained to HẠN NHA RE...
Please analyze the IR and NMR spectra. How pure it is? What
impurities can be observed? Please label all major signals. The
product is N,N-diethyl-m-toluamide. The product is obtained by the
following reactions
Solvent is Et2O. Extracted with NaOH and then HCl and then
H2O. Dried and then evaporated. To further purify the product,
hexane was added to perform column chromatography.
Evaporated.
Clearer image for the IR image:
CH3 CH3 SOCI2 + SO2 O=0 ОН CH3 CH3 -- + excess...
analyze the peaks of the IR and NMR
precipit 1act the crude pr sto a 50-ml. Ind P nal until it is um filtra action flask Administrator Analyst Monday, June 10, 2019 3:49 PM Date 104 100 95 90 85 37m-1 2633 78cm-1 80 101.cm-1 2964 30-1 75- 1411 4153.99 2867 77cm-1 70 458.92 1044 05cm t 3369 72m-1 65 927.87 8 74m-1 60 249 96om-1 1064 47cm-1 9e-1 55 131.74dm-1 50- 67384cm-1 t1047am 45 701.90cm-1 13711cm-1 40- 847 01m-1...
The proton nmr and the infrared spectra of DCC, DMAP, DCU, the
product and the nmrs of the starting materials and products are
shown. These are labeled Compounds A, B and C. a.Which nmr is the
product?
b. Which is the nmr of the starting material?
c. What is the mixture of compounds shown as compound C?
tert-Butyl Ethyl Fumarate DCC, DMAP, CHCI OH Chemical Formula: C,H,O Chemical Formula: CH 0 Molecular Weight: 144.13 Molecular Weight: 74.12 Chemical Formula: CH...
Please identify all relevant peaks in both the IR and NMR for
methyl 3-nitrobenzoate, please use the following chart as a
template, thank you!
Spectral Database for Organic Compounds SDBS Japanese Introduction Disclaimer HELP Contact What's New RIO-DB FAQ LINK . AIST SDBS-H NMRSDBS No. 3528HSP-49-719 Cg H7 N04 methyl m-nitrobenzoate 399.65 MHz 0.038 g: 0.5 ml CDC13 9 8 7 6 4 3 2 1 5 ppm HSP-49-719 {AH 1 0 —CH, (E) ON -H (C) (BH HID) Spectral...
Please identify all relevant peaks in both the IR and NMR for
methyl 3-nitrobenzoate, please use the following chart as a
template, thank you!
Spectral Database for Organic Compounds SDBS Japanese Introduction Disclaimer HELP Contact What's New RIO-DB FAQ LINK . AIST SDBS-H NMRSDBS No. 3528HSP-49-719 Cg H7 N04 methyl m-nitrobenzoate 399.65 MHz 0.038 g: 0.5 ml CDC13 9 8 7 6 4 3 2 1 5 ppm HSP-49-719 {AH 1 0 —CH, (E) ON -H (C) (BH HID) Spectral...
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