What is the theoretical yield, pure % yield and crude % yield of Triphenylmethanol by Grignard...
A student decides to perform the synthesis of triphenylmethanol via the grignard reaction. She starts with 9.5g of bromobenzene (M.W. = 157) and uses 1.21g of Mg (M.W. = 24.3) and 9.1g of benzophenone (M.W. = 182). a. Calculate the limiting reagent. b. Calculate the theoretical yield of triphenylmethanol (M.W. = 260.3).
The synthesis of triphenylmethanol via the grignard reaction is given by the following equation (below): A student decides to perform the above reaction. She starts with 200 mg of bromobenzene (M.W. = 157) and uses 45 mg of Mg (M.W. = 24.3) and 0.36 g of benzophenone (M.W. = 182). a. Calculate the limiting reagent b. Calculate the theoretical yield of triphenylmethanol (M.W. = 260.3) c. She obtains 0.172 grams of of the product. What is her actual yield? d....
What is the theoretical yield (in grams) and percent yield of your triphenylmethanol product in this experiment? Assume you have collected 0.15 g of triphenylmethanol. Br 2 Mg Ether MgBr 1) PhCO2CH3 2) HCI 2 2 Ph3COH + CH3OH Figure 10.1. The stoichiometry of a Grignard reaction. Br MgBr 2 1) 2 Mg Ether 2 2) PhCO2CH3 i MgBr OCH3 Ph Ph Ph CH30 + Benzophenone, III II Ph - MgBr OH MgBr 3) HCI Ph Ph Ph Ph Ph...
help with calculating theoretical and percent yield? This is a grignard reaction which converts phenyagnesium bromide into triphenylmethanol. actual yield of product = 0.0958 grams picture of reaction as well as data below: also what would the limoting reagent be? magnesium? [Actual moucular massused img Acinal amount im mon Reagents gi moi Magnesium 24.305 51.4. 2.1 Bromöbenzene 157.01 410.2 2.61 methyl Benzoate 136.16 141.5 1.04 mmol ether -Br + Mg MgBr Bromobenzene Phenyimagnesium bromide Methyl benzoate MgBr OH HCI +...
MgBr + anhydrous ether Mg MW: 24.31 Grignard reagent MW: 157.02 R-X + Mg - R-X + Mga Single Electron Transfer (SET) R-X - R + X- R + Mg - RM RMG + X- RMX Ph MgBr Ph Lo MaBr H (Ph)3COH Pn H20 MW:260.34 Grignard reaction • Volume of bromobenzene is 4.5 mL. • Density of bromobenzene is 1.5 g/ml • Mass of benzophenone is 6.75g • We assume 65% yield of the product (triphenylmethanol) was obtained in...
MW: Molecular Weight, mmol: Millimoles mL MW mmol equivalents reagent bromobenzene magnesium benzophenone diethyl ether theoretical product triphenylmethanol 24.30 b.65 74.123 O. 70(p
The weight of triphenylmethanol is 0.060g QUESTIONS 1. (4 Points) What is the theoretical yield (in grams) and percent yield of your triphenyl- methanol product in this experiment? EXPERIMENTAL PROCEDURE All glassware used in a Grignard reaction must be scrupulously dried. Dry the following glassware in an oven at 110°C for at least 20 minutes: drying tube, Claisen adapter, 8 mL conical vial, 5 mL conical vial, air condenser, glass stirring rod, and a magnetic spinvane. DO NOT PLACE O-RINGS...
Grignard Reaction with a Ketone: Triphenylmethanol Introduction: The purpose of this lab is to prepare phenylmagnesium bromide, a Grignard reagent, and react it with benzophenone to give triphenylmethanol. Grignard reagents are very reactive and must be synthesized in an environment free of water or any other source of potential proton donor. Once made, the Grignard reagent will do a nucleophilic attack on the carbonyl carbon of the ketone, benzophenone. The result is an alkoxide that is then protonated to give...
What is the theoretical yield (in grams) and percent yield of your triphenylmethanol product in this experiment? (Weight of triphenylmethanol: 0.060g) BACKGROUND AND THEORY The Grignard reaction was one of the first organometallic reactions discovered and is still one of the most useful synthetically. By reacting an organohalide (usually a bromide) with magnesium in ethereal solvent, carbon becomes a nucleophile. Grignard reagents are the starting points for the syntheses of many alkanes, primary, secondary, and tertiary alcohols, alkenes, and carboxylic...
What is the theoretical yield and the percent yield of this Grignard reaction which converts phenyagnesiumbromide into triphenylmethanol? actual yield of final product is 0.00958grams also would the limiting reagent be magnesium?? Reagent Amountured maghlesinm 51.4 mg Bromo benzene 4.10.2 2 mg methyl benzoatel 141.5 mg