Organic Lab: Synthesis of Triphenylmethanol and the Trityl Carbocation 1. If all of your solid dissolved...
Organic Lab: Synthesis of Triphenylmethanol and the Trityl Carbocation
1. If all of your solid dissolved in hexanes at the end of the separation what could that mean?
2. If water reacts with the Grignard reagent what by-product is formed?
3. When should you use a reflux apparatus? Sketch a picture of a simple reflux apparatus.
4. What two ways can the separatory funnel be used based on this experiment?
5. What is the difference between washing and extracting?
Homework Answers
1) It means that all the solids obtained during experiment can be collected and added (dissolved) in to the hexane.
2) corresponding Alkane is the product and Magnesium hydroxide as formed as by-product.
3) whenever temperature of reaction is above or near to the boiling point of the solvent used in the reaction that time reflux apparatus is uesd, picture will be added down.
4) for separation of organic layer from aqueous layer.
5) washing is taking solid compound in suitable solvent (by which you want to wash) and shaking with it for sometime. Extraction can be done in separating funnel here compound can be extracted of taken out in suaitable solvent by shaking in separating funnel.
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Organic Lab: Synthesis of Triphenylmethanol and the Trityl
Carbocation
1. If all of your solid dissolved...
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What is the theoretical yield (in grams) and percent yield of your
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Here is a copy of the experiment, thank you!
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