Separating ethyl-4-aminobenzoate, phenanthrene, and salicylic
acid in a solution. Don't know the concentrations of any of
them.
Planning to use HCl to precipitate the salicylic acid out, but will
have access to 6 M and 1 M and I'm not sure which to use.
Then adding NaOH to organic layer to precipitate out the
ethyl-4-aminobenzoate, but again I'm not sure what molarity to use
between the 1 M and 6 M (we will have access to 1 M and 6 M NaOH
too).
Finally, planning to add NaCl to precipitate out the
phenanthrene.
Separating ethyl-4-aminobenzoate, phenanthrene, and salicylic acid in a solution. Don't know the concentrations of any of...
Okay, so we had solid benzoic acid, ethyl 4- aminobenzoate, and 9-fluorenone all dissolved in diethyl ether (4ml). We separated the basic component by adding 3M HCl, we separated the acidic component by adding 3M NaOH. I don't understand what happens here. To isolate the acidic solution, we added 6 M NaOH and used the vacuum to recover the solid. To isolate the basic solution we added 6M HCl. Here are the questions I am having trouble with... • Why...
The Separation of Three Organic Compounds by Acid, Base Reactions and Liquid, Liquid Extraction. Okay, so we had solid benzoic acid, ethyl 4- aminobenzoate, and 9-fluorenone all dissolved in diethyl ether. We separated the basic component by adding 3M HCl, we separated the acidic component by adding 3M NaOH. I don't understand what happens here. To isolate the acidic solution, we added 6 M NaOH and used the vacuum to recover the solid. To isolate the basic solution we added...
Extraction of benzoic acid and 9-fluorenone using diethyl ether. (please do not include ethyl 4- aminobenzoate). I have to create a flow chart to diagram the key steps of the experiment and isolation of products. 0.100g of benzoic acid and 9-fluorenone are dissolved in diethyl ether. The extraction solvent is 5% sodium hydroxide (to extract the acidic component from the organic phase). Saturated sodium chloride is added to the organic layer. drying the organic solution: anhydrous sodium sulfate is added...
The Separation of Three Organic Compounds by Acid, Base Reactions and Liquid, Liquid Extraction. Okay, so we had solid benzoic acid, ethyl 4- aminobenzoate, and 9-fluorenone all dissolved in methyleene chloride. We separated the basic component by adding 3M HCl, we separated the acidic component by adding 3M NaOH. I don't understand what happens here. To isolate the acidic solution, we added 6 M NaOH and used the vacuum to recover the solid. To isolate the basic solution we added...
You will apply what you have learned earlier in the semester when performing the Acid-Base Extraction experiment to perform a different separation: that of an organic neutral compound and organic base. You will also need to purify and characterize these compounds. You will have one lab period to execute your plan for separating the assigned mixture given below. There will be a 1:1 (by mass) mixture placed in the lab: 1,4-dichlorobenzene/ethyl 4-aminobenzoate. You will take approximately 1 g of your...
Options for each question: 6 M
HCL, 5% HCL solution, Dichloromethane, 6 M NaOH, 5% NaOH
solution
Question 8 Status: Not yet answered Points possible: 1.00 When separating benzoic acid, naphthalene, and aniline, identify the solution used for each described purpose. Reconstitute benzoic acid from aqueous layer Choose... Extract benzoic acid into the aqueous layer Choose... Reconstitute aniline from aqueous layer Choose.. Extract aniline into the aqueous layer Choose... Extract reconstituted benzoic acid out of the aqueous layer Choose... Extract...
Complete the flowchart below for the following extraction: Benzoic acid 4-aminoacetophenone benzophenone Step 1: Dissolve in ethyl acetate Step 2: Add 2M NaOH Step 3: Mix and Identify how layers separated: DRAW STRUCTURES IN THE CORRECT FORM AT THAT STEP (neutral? Salt? etc) AQUEOUS ORGANIC Step 4: Add 3 M HCL DRAW STRUCTURES OF COMPONENTS IN AQUEOUS LAYER Step 5: Collect with vacuum filtration DRAW STRUCTURE OF COMPONENTTS 2. Write a balanced chemical equation for each reaction which occurs in...
(If you need any more information just let me know) Determine the limiting reagent for the preparation of 2-bromo-2-methylbutane and calculate the theoretical yield of product. 1 CHEM-2223 Organic Chemistry Laboratory I Exp. 7: Synthesis of 2-chloro-2-methylbutane In this reaction a tertiary alcohol, 2-methyl-2-butanol, is converted to a tertiary halide, 2-chloro- 2-methylbutane through a SN1 reaction. 1) Chemicals 2-Methyl-2-butanol Hydrochloric acid, HCl (12 M) Saturated sodium bicarbonate Saturated sodium chloride (380 g/L) Anhydrous sodium sulfate...
Construct a flow chart describing the seperation of the
mixture and the isolation of each compound in this experiment. (Lab
steps/procedures includes for reference)
4. Construct a flow chart describing the separation of the mixture and the isolation of each compound in this experiment. A commonly used method of separating a mixture of organic compounds is known as liquid-liquid extraction. Most reactions of organic compounds require extraction at some stage of product purification. In this experiment you will use extraction...
Trial 6 Trial 5 Trial 2 Trial 4 Trial 3 Trial 1 Volume of acid sml solution acquired: smit smi smi 6 мм ISmI 1 omi omi omlomi Initial buret reading: OML Oml Final buret reading: umu 5ml smi u.sms . s u .s. *Volume of NaOH I UML solution used: smi I smi u.5ml 9.5 u.s. I volume trail m NaOH t (trail) 7 mol NaOH MGIHAI > MHCL *Molarity of acid solution: Name: *Average Molarity of acid: Percent...