Combine 0.925 grams of 4-(diethylamino)salicyaldehyde (1.0 equivalent), ethyl acetoacetate (7.65 equivalents) and piperidine (1.95 equivalents) in a 50 mL round bottom flask with stirring.
What quantity of ethyl acetoacetate do you need to add? Enter a quantity accurate to three significant figures. For liquids, enter a volume in millilitres (mL). For solids, enter a mass in grams (g).
Quantity of ethyl acetoacetate =
What quantity of piperidine do you need to add? Enter a quantity accurate to three significant figures. For liquids, enter a volume in millilitres (mL). For solids, enter a mass in grams (g).
Quantity of piperidine =
If you isolate 0.695 g at the end of your purification, what is your experimental yield? Enter a percentage accurate to three significant figures.
Experimental yield =
Use a quantity table with MW, quantity, density, moles, and equivalents to show values and calculations
Combine 0.925 grams of 4-(diethylamino)salicyaldehyde (1.0 equivalent), ethyl acetoacetate (7.65 equivalents) and piperidine (1.95 equivalents) in...
Just Answer Question 5
Synthesis of 2-chloro-2-methylbutane (literature version) Concentrated aqueous hydrochloric acid (HCI, 3.3 equivalents) was slowly added to 2-methyl-2-butanol (1.0 equivalents) in a 100 mL round bottom flask with stirring. The reaction was stirred for 15 minutes at room temperature. Upon completion, the reaction mixture was transferred to a 60 mL separatory funnel and the aqueous layer was removed. The organic layer (i.e. the product) was successively washed with: (1) saturated aqueous NaCl (brine), (2) saturated aqueous NaHCO,...
What is the theoretical yield (in grams) and percent yield of your
triphenylmethanol product in this experiment? (Weight of
triphenylmethanol: 0.060g)
BACKGROUND AND THEORY The Grignard reaction was one of the first organometallic reactions discovered and is still one of the most useful synthetically. By reacting an organohalide (usually a bromide) with magnesium in ethereal solvent, carbon becomes a nucleophile. Grignard reagents are the starting points for the syntheses of many alkanes, primary, secondary, and tertiary alcohols, alkenes, and carboxylic...