tell how each of the following experimental errors will affect your experimental results ( yield,purity,or both) and explain why.a)you failed to dry the product completely.b) you used enough water to recrystallize phenacetin, but your unknown was acetanilide.c)inexperiment 2, you didn't extract all of the aspirin from the dichloromethane solution.
tell how each of the following experimental errors will affect your experimental results (...
Describe and explain the possible effect on your results of the following experimental errors or variations. a) you used a solution cell with a 0.1mm spacer for the infrared spectrum, b) you dissolved your unknown in petroleum ether for the UV analysis c) There was no deuterochloroform available for the NMR sample so you used ordinary chloroform
Describe and explain the possible effect on your results if the following experimental errors or variations occurred. You used pure water as the reaction solvent. You started with 2.5mmol of vanillin and assumed that a 100% excess of NaBH_4 was 5.0 mmol and used that amount. Explain how to differentiate between the IR spectra of vanillin and vanillyl alcohol.
Uuuuuup ALDU 9.128 5. Discuss how the following instances would affect the results of this synthesis? (1.5 points) a. The product was washed with hot water during filtration instead of cold water. b. The aspirin was left out to dry for weeks, resulting in a vinegar-like smell. Write the possible reaction. c. A student performing this experiment misread the amount of reactants and added 0.50 ml of acetic anhydride instead of 5.0 ml. Did this procedural error affect the theoretical...
LABORATORY 8 Post-Lab 1. Explain how each of the following errors would have altered your results. Clearly explain why your calculated answer would be high, low, or unchanged. (A single word answer is not acceptable.) a. You decided to take the pH after each addition of 5.0 mL of NaOH rather than after every 0.5 mL during the neutralization of your acid sample. b. While using the Half Volume method, your solution was dark pink (you overshot the endpoint) and...
For each of the following errors, tell whether your calculated molecular weight would be too high, too low, or unaffected. a) unawares, you inadvertently spilled some solute(so it didn't make it into the test tube) after it was weighed out. b) your thermometer is poorly calibrated and reads 0.3C lower than the actual temperature. c) while mixing the solution you spilled some over the sides of the test tube. Assume the solution was well mixed before the spill occurred.
If you were to run this reaction on a 0.5 g acetaminophen, how much powdered potassium carbonate would you use ? Show your work Alcohols and Ethers 185 14.3 THE WILLIAMSON ETHER SYNTHESIS: PREPARATION OF PHENACETIN FROM ACETAMINOPHEN One of the most common methods used to prepare ether Williamson ether synthesis. In this reaction, an alkoxide anion (RO) acts as a nucleophile in an S, 2 process, displacing a leaving group (X) from an electrophile (R-X). R-20 . RY ROR...
7. For each of the following experimental or calculation errors, tell if the calculated value of R, in question 4, would be too high, too low or unchanged. Explain your answers. a. The temperature of the water was recorded too low. b. The mass of the magnesium was recorded too high. c. The magnesium was coated with magnesium oxide. d. Some air bubbles were introduced when the eudiometer was inverted. Some of the hydrogen gas dissolved in the water. (Hint:...
1. for each of the given situations, tell how the error will affect the calculated specific heat. Will it be too high, too low, or have no effect on the result? explain your answer. a. the balance used to determine the mass of the metal was in error by 10g on the high side. In other words, the balance gave a larger mass than the true mass. b. it was thought that the metal was in the boiling water long...
What effect on your calculated yield would the following experimental errors have had? A) Incomplete evaporation of the excess hydrochloric acid B) Excessive heating of the product to cause decomposition (say to manganese(II) oxide) C) Cooling the product in the open air (especially on a humid day) D) Which of the above errors are the most probable? Experiment: Manganese sample is dissolved in concentrated HCl, exess HCl and water will be evaporated to obtain solid manganese(II) chloride.
using the procedures, we used dichloromethane as the unknown mixture and i was able to extract benzoic acid for an acid, 5-chloro-2-methoxyanaline for a base compound and biphenyl for neutral compound. i don't know if that answers the missing part but if it didn't could you be specific please? thank you! 2. Construct a flow chart of the acid-base extraction you carried out. Use the specific structure of the compounds isolated. Don't use the molecular formula. (15 pts) We used...