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Experiment 10: Results Table (Allowed on concept review, pass in with your concept review quiz an...
Heat lamp or drying oven Hydrated copper chloride Distilled water Aluminum wire 30-ml beaker Glass rod Watch glass Buchner fiannel Hot plate Ethanol Füter paper CAUTION: Wear all safety equipment, follow all normal safety procedures and experiment as directed by your instructor follow instructions. Dispose of all liquid AND solid waste products from the 1. Weigh a clean, dry 30-mL beaker and record its mass to 3 decimal places. When-it-is-time,heat the beaker 2. Add approximately 1.00 gram of the hydrated...
QUESTION: Write a flow scheme for the work-up. THE WORK UP: C. Work-up (save all layers) and Isolation of Product MgBrCl Benzoic acid Transfer the mixture into a test tube. Rinse the beaker with about 3 mL of regular (not anhydrous) diethyl ether and pour the washings into the test tube. There should be two distinct layers in the test tube Remove the aqueous layer (to be discarded) and shake the ether layer with about 2 mL of 3 M...
Write out your separation scheme for this experiment. 1. Heat 75 mL of water to 90 °C in a 250-mL beaker. 2. While the water is being heated, place 250 mg of salicylic acid, 1 drop of 85% phosphoric acid and 0.5 mL of acetic anhydride in a test tube. Add a boiling chip to the mixture and gently shake it in order to mix the reactants. 3. Heat the tube in the beaker of water at 85 - 90...
Consider the following reaction at 25 degree C: 2HNO_3 (aq) + NO(g) rlhar 3 NO_2(g) + H_2O(l) Calculate Delta G degree rxn using the following information HNO_3 (aq) NO(g) NO_2(g) H_2O(l) Delta H^degree (kJ/mol) -207 91.3 33.2 -285. 8 S^degree (J/mol K) 146 210.8 240.1 70.0 Calculate the value of the equilibrium constant, K, at 25 degree C At 25 degree C does the above reaction favor reactant or product formation? What evidence supports your conclusion? Procedure: Obtain the five...
i did the synthesis of aspirin experiment and got the data below. how do you do the theoretical yield? percent yield of the pure aspirin? DATA: Mass of Salicylic Acid: 2.034g Volume of Acetic Anhydride used in synthesis: 4.00ml Mass of filter paper: 0.196g Mass of filter paper plus Aspirin: 1.868g Mass of Aspirin: 1.672g Percent Yield of Pure Aspirin: I Experimental Procedure HAZARD: Sulfuric acid, acetic anhydride and glacial acetic acid are corrosive to the skin. They are also...
for this experiment of syntheis of aspirin, was the product obtained pure (based on color)? how do you know? the color was white Experimental Procedure HAZARD: Sulfuric acid, acetic anhydride and glacial acetic acid are corrosive to the skin. They are also irritants, and all operations in which these substances are used should be carried out under the hood. Prepare a hot-water bath by heating a 400-ml beaker containing about 200 mL of water. 1. Use a centigram balance and...
Calculate the % Al in the sample. Preparation of a stock solution of aluminum. Accurately weigh out approximately 1 g of the aluminum foil. Tear it up into small pieces, place the pieces into a covered 250 mL beaker and add 60 mL of 6M HCl. This should be carried out in the fume hood because the reaction is exothermic and leads to violent frothing and emission of vapors. Cool, quantitatively transfer to a 250 mL flask, rinsing with deionized...
#5 Write the solubility product expression for PbCl2. Using the concentration for the Pb+2 and Cl- ions, solve for your experimental Ksp. #6 Using your book, find the theoretical Ksp for PbCl2 to determine your percent error A Solubility Product Constant Introduction: Many substances are very soluble in water. However, in this experiment you will be concerned with substances that are insoluble or only slightly soluble. Dynamic equilibrium is established when an excess of a slightly soluble substance is placed...
Principles of Inorganic Chemistry! Week 5 Effect of Temperature on Solubility of a Salt In this experiment, you will study the effect of changing temperature on the amount of solute that will dissolve in a given amount of water. Water solubility is an important physical property in chemistry, and is often expressed as the mass of solute that dissolves in 100 g of water at a certain temperature. In this experiment, you will completely dissolve different quantities of potassium nitrate,...
Calculate the % Al in the sample. Preparation of a stock solution of aluminum Accurately weigh out approximately 1 g of the aluminum foil. Tear it up into small pieces, place the pieces into a covered 250 mL beaker and add 60 mL of 6M HCl. This should be carried out in the fume hood because the reaction is exothermic and leads to violent frothing and emission of vapors. Cool, quantitatively transfer to a 250 mL flask, rinsing with deionized...