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H NMR Spectrum of 3-Chlorobenzoic Acid (CDCl3) 유. .533 .7.435

The attached 1H NMR spectrum of 3-chlorobenzoic acid, recorded as a solution in CDCl3 + D2O, lacks the broad resonance due to the carboxylic acid proton. Explain the lack of the indicated resonance in this spectrum.

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Answer #1

CooH peak may contain H2O in the solvent,or may be the sample is wet.

Peak usually appears at 10 to 12ppm.

CDCl3 is acidic in nature,so proton exchange also may be there .

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The attached 1H NMR spectrum of 3-chlorobenzoic acid, recorded as a solution in CDCl3 + D2O, lacks the broad resonance due to the carboxylic acid proton. Explain the lack of the indicated resonanc...
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