CRUDE PRODUCT COMPOSITION: (as determined by NMR) Show Calculations for % 9-fluorenol and % unreacted 9-fluorenone:
Relative amount of 9-fluorenol = {(8 × 0.13)/(1.00 + 0.66 + 0.04 + 1.13)} × 100% = 36.75 %
Therefore relative amount of 9-fluorenone = (100-36.75)% = 63.25%
CRUDE PRODUCT COMPOSITION: (as determined by NMR) Show Calculations for % 9-fluorenol and % unreacted 9-fluorenone: A0...
Expt 9: 'H NMR Data The following is a 'H NMR of a student's sample from Experiment 9. This is a crude reaction mixture, which means it has solvent, starting materials, and product all mixed in together. Therefore, we do NOT expect you to interpret all of the peaks or tabulate the data. We will only look at signature peaks that can help us determine what has happened. Note that this sample may not exactly match your reaction, but it...
for the following 2 compounds, please calculate, and show the calculations for, the degree of unsaturation, assign the IR spectrum peaks, assign the 13C NMR peaks, assign the 1H NMR peaks, and draw the structure for the unknown compound. CHIM 245 Spectroscopy Problem Set #2 In this problem set there are two unknown compounds. You are provided with the formula, IR spectrum, "C NMR spectrum, and 'H NMR spectrum for each compound. Each unknown is worth 10 points, with an...
Organic Chemistery Lab This is my crude product H NMR. (Exp: Diels-Alder Reaction in water) Anthracene-9-methanol and N-methylmaleimide react in water, and refulx 1.5h, than Anthracene-N-methylmaleimide Des-Alder adduct was created. TA told me that specturm is excellent, but there are so many mistakes at labels. Please see my data, and let me know if there are mistakes. 17091 5i3-0502 exp#1 crude CD-04-Suwon gyenewow 27 27 26 26 26 26 25 25 25 25 24 24 23 23 22 21 20...
Evaluate and investigate the following IR Spectrum, 13C NMR Spectrum and 1H NMR Spectrum. Identify the most important peaks and correlate the results as much as you can from the obtained product in the multi-step synthesis of ethyl acetoacetate. This is Product E from this multi-step synthesis where Product C was identified as in the figure below and as such, identify what product can be obtained after the synthesis from the spectra provided. Use the template below in analysing the...
What is answer of #10?? Report: Hydroboration of 1-Methylcyclohexene Mechanism / GC Analysis / Calculations 1. After reviewing the GC and 'H NMR spectra, what is the major product of the reaction? + 3 a. BH: . THF 3 b. 3 H2O2 OH + 3 OH c. NaOH MOH OH racemic racemic major 2. Draw the complete curved arrow mechanism for the reaction to produce the major product, including both the hydroboration and oxidation steps. Repetitive steps need only be...
What is answer of #9??? Help me Report: Hydroboration of 1-Methylcyclohexene Mechanism / GC Analysis / Calculations 1. After reviewing the GC and 'H NMR spectra, what is the major product of the reaction? + 3 a. BH: . THF 3 b. 3 H2O2 OH + 3 OH c. NaOH MOH OH racemic racemic major 2. Draw the complete curved arrow mechanism for the reaction to produce the major product, including both the hydroboration and oxidation steps. Repetitive steps need...