When the mixture of biodiesel and glycerol is in separatory funnel, glycerol appears denser than biodiesel. What can be the chemical reasoning of the observation?
as we can see from structure of glycerol that it have 3 -OH sites available for H bonding which give rise to very high intermolecular forces between molecules
And properties like viscosity boiling point and density depends upon intermolecular forces due to high intermolecular forces it have high density than biodiesel as it have only week vanderwall forces so less intermolecular forces give rise to less density.
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When the mixture of biodiesel and glycerol is in separatory funnel, glycerol appears denser than biodiesel....
1. What is the practical advantage of having the organic solvent be denser than water when one is extracting an organic compound from an aqueous solution in a separatory funnel?
Post-Lab 3. You vigourously shake a separatory funnel, and notice an emulsion forming. What can you do to help break up the emulsion? 4. Complete the following acid-base reaction and provide the keq. Is sodium bicarbonate (NaHCO) a suitable base in this situation? + NaHCO, 5. A mixture of benzoic acid and a neutral nonpolar compound is dissolved in ether and mixed thoroughly with aqueous sodium bicarbonate. What is the organic chemical species that is present in the ether layer?...
4. When a separatory funnel is shaken too vigorously, an emulsion may form. What would be the best way to quickly (!) break the emulsion?
Why is it important to open the stopcock on the separatory funnel when extracting from one phase (say, organic phase,) into another phase (say, aqueous phase)?
1) during liquid liquid extraction ( LLE) it is normal to use separatory funnel, and two non- miscible phases of solvents , for ex: water as polar phase and ethyl acetate is the organic phase. density of water is 1,0 g/ ml, while density of ethyl acetate is 0.90 g/ ml at 25.0 celsius degrees. which of the two solvents will end up at the buttom of the separatory funnel? 2) ) during liquid liquid extraction ( LLE) it is...
Why do we "vent" multiple times when using a separatory funnel? To speed-up the reaction by decreasing the pressure in the separatory tunnel To allow air into the system to help separate layers. To prevent the fumes from re-entering the liquid state. To release excess gases.
a) After the reaction is completed, the reaction mixture is transfered to a separatory funnel. The layers are separated and the organic layer is washed with each of the following: an equal amount of saturand NaCl, satured NaHCO3, deionized H2O, and again with saturated NaCl. This is an example of a "basic" work-up. Illustrate what is being neutralized in this work up using a balanced equation. (2 Marks) b) The base used is NaHCO3. This base can be dangerous in...
2. When using the separatory funnel you may have observed a oily emulsion between the aqueous and DCM layers. What components of tea are responsible for this emulsion? How can one minimize the size of the emulsion layer? 3. How does adding the anhydrous sodium sulfate to the dichloromethane solution remove water? 4. If the above step was omitted in the isolation procedure, how would this be reflected in the yield of caffeine? 5. A student used 8.23 g of...
5) When a small amount of CH3(CH2)4CO2H (pKa --4.8) is added to a separatory funnel that contains ether and water with a pH = 12.0, it is found mainly in the layer as A) ether; CH3(CH2)4CO2H B) water; CH3(CH2)4CO2- C) water; CH3(CH2)4CO2H D) ether; CH3(CH24CO2- E) none of the above
When a small amount of CH3(CH2)4CO2H, (pKa ~4.8) is added to a separatory funnel that contains ether and water with a pH = 2.0, it is found mainly in the ________ layer as ________. A) ether; CH3(CH2)4CO2- B) water; CH3(CH2)4CO2- C) ether; CH3(CH2)4CO2H D) water; CH3(CH2)4CO2H E) none of the above