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the compound is dibenzalacetone 3C - NMR (expansion 120-195 ppm) + DEPT (400 MHz) in CDC13...
the compound is dibenzalacetone -NMR (expansion 7.0-7.8 ppm (400 MHz) in CDC13 7.76 7.72 DO 7.07 Solvent peak (ignorel) 7.80 7.75 7.70 7.65 7.60 7.55 7.50 7.45 7.40 7.35 7.30 7.25 7.20 7.15 7.10 ppm 18 Peak List for 1H NMR (8 in ppm) TH NMR (draw labelled structure here) (10 marks) Multiplicity Chemical shift 8 (ppm, 4 decimal places) Coupling constant Integral J (Hz) Assignment indicate whether it is a singlet (s) doublet (a), triplet 3. quartet (allor dd...
Identify the compound C8H9NO2 from its 1H, 13C/DEPT, COSY, HMQC, and INADEQUATE spectra and show all correlations. 'H NMR 600 MHz 5480 5470 Hz 5200 5190 Hz 4910 4900 Hz 4370 4360 Hz 2590 2580 Hz 790 780 Hz 9.0 8.5 8.0 7.5 7.0 6.5 6.0 5.5 5.0 4.5 4.0 3.5 3.0 2.5 2.0 ppm 13C/DEPT 150.9 MHz 160 150 140 130 120 110 100 90 80 70 60 50 40 30 ppm 274 CHAPTER 5 Two-Dimensional NMR Spectroscopy Exercise...
Label peaks and determine the structure of the aldehyde in the 1H NMR and 13C1H NMR: pg 1H NMR of product from aldehyde Yin CDCI3 CHCI ppm Hz Intensity 17.73 3091.6 621.6 2 7.69 3075.7 690.3 3 7.59 3036.2 1108.5 4 7.57 3027.5 1199.0 5 6.98 2793.9 961.0 6 6.95 2779.9 1320.9 76.94 2778.0 1279.1 8 6.93 2771.1 1185.2 7.60 7.55 7.50 7.45 7.40 7.35 7.30 7.25 fl (ppm) 7.20 7.15 7.10 7.057.00 6.95 6.90 OK to group CHCl3 -...