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Experiment 4: Synthesis of a tertiary alkyl halide Page 4 of 6 Why do we wash...
Scenario: While working in an organic lab, you have been asked to prepare 5.0 g of...
Scenario: While working in an organic lab, you have been asked to prepare 5.0 g of 2,5-dichloro-2,5- dimethylhexane from 2,5-dimethyl-2,5-hexanediol. Draw the complete mechanism for the reaction. [2 Marks] When setting up the reaction above, is your starting material a solid or a liquid? [1 Mark]
Experiment 4: Synthesis of a tertiary alkyl halide Page 3 of 6 Distillation is a technique that is to purify liquid com...
Experiment 4: Synthesis of a tertiary alkyl halide Page 3 of 6 Distillation is a technique that is to purify liquid compounds. Use theoretical data to explain how distillation is used to separate the target product in this reaction from any residual unreacted starting material in the reaction. [2 marks]
Experiment 4: Synthesis of a tertiary alkyl halide Page 5 of 6 Experiment 4: Synthesis of...
Experiment 4: Synthesis of a tertiary alkyl halide Page 5 of
6
Experiment 4: Synthesis of a tertiary alkyl halide Page 5 of 6 Assuming that all other experimental conditions are the same; explain if an S,1 reaction would still occur if the following changes were made. If an Sk1 reaction would still occur: then state the IUPAC name and draw the structure of the product formed compare the rate of reaction to the rate of the original reaction (in...
Experiment 4: Synthesis of a tertiary alkyl halide Page 3 of 6 The term "side reactions"...
Experiment 4: Synthesis of a tertiary alkyl halide Page 3 of 6 The term "side reactions" refers to any chemical reaction that can occur that form products other than the desired product. Side reactions can consume the reactants of your intended reaction, and can affect the percent yield of your target product. Draw the full reaction mechanism for a possible side reaction that can occur under these reaction conditions. Include all charges and intermediates. Vaguely directed arrows will not receive...
Page 1 Synthesis using Carbonyl O-Substitution Chemistry Preamble This experiment involves the synthesis of target molecules...
Page 1 Synthesis using Carbonyl O-Substitution Chemistry Preamble This experiment involves the synthesis of target molecules using a-substitution chemistry. You are assigned two target molecules, one of which is best synthesized by an alkylation approach, while the other is best synthesized by an addition or condensation approach. You must do the following: 1. Perform a retrosynthetic analysis on the two target molecules assigned to you. In each case the organic starting material (what you have to work backwards toward) depends...
2) Predict the order of reactivity (1=least, 4=most) of primary, secondary, tertiary, and aryl halides toward...
2) Predict the order of reactivity (1=least, 4=most) of
primary, secondary, tertiary, and aryl halides toward nucleophilic
displacement by an SN1 reaction mechanism. Explain
3) Give a detailed summary of the chemistry in both reactions
SN2 and SN1 in details please for both reactions. include any
general statements about the experiments.
LAB)o Organic Chemistry I Lab CHEM 3512 Nueleophilic Substitution Reactions: Sl vs S2 To review Sul, S2, El and E2 reactions and mechanisms and compare and contrast the effect...
Synthesis using Carbonyla-Substitution Chemistry Preamble This experiment involves the synthesis of target molecules using a-substitution chemistry....
Synthesis using Carbonyla-Substitution Chemistry Preamble This experiment involves the synthesis of target molecules using a-substitution chemistry. You are assigned two target molecules, one of which is best synthesized by an alkylation approach, while the other is best synthesized by an addition or condensation approach. My two target molecules are number 2 and number 12 in the last page. You must do the following: 1. Perform a retrosynthetic analysis on the two target molecules assigned to you. In each case the...
Experiment Write Up Proposal You will write up a synthesis procedure for one reaction that could...
Experiment Write Up Proposal You will write up a synthesis procedure for one reaction that could be potentially run in a face- to-face Chem 2321 lab session. Your proposal will include an introduction and procedure. The procedure will include step-by-step instructions for running the reaction (including reaction monitoring), work-up. (product isolation and purification), and analysis (characterization). You will need to include sample calculations for percent yield and provide sample spectra analysis. You must upload your proposal as a single document...
The following questions are from an experiment titled Friedel-Crafts Alkylation for Organic Chemistry II Lab. There...
The following questions are from an experiment titled
Friedel-Crafts Alkylation for Organic Chemistry II Lab. There are
pictures attached of the lab manual.
2) Is this method a good route for the preparation of
p-sec-butyltoulene? Give reasons for your answer.
3) Why do you use a large excess of toulene. What are its
functions?
4) What is the purpose for adding the hydrochloric acid to the
water in the separatory funnel in step 5? Hint: If no acid is
added,...
Grignard Reaction with a Ketone: Triphenylmethanol Introduction: The purpose of this lab is to prepare phenylmagnesium...
Grignard Reaction with a Ketone: Triphenylmethanol Introduction: The purpose of this lab is to prepare phenylmagnesium bromide, a Grignard reagent, and react it with benzophenone to give triphenylmethanol. Grignard reagents are very reactive and must be synthesized in an environment free of water or any other source of potential proton donor. Once made, the Grignard reagent will do a nucleophilic attack on the carbonyl carbon of the ketone, benzophenone. The result is an alkoxide that is then protonated to give...
Scenario: While working in an organic lab, you have been asked to prepare 5.0 g of 2,5-dichloro-2,5- dimethylhexane from 2,5-dimethyl-2,5-hexanediol. Draw the complete mechanism for the reaction. [2 Marks] When setting up the reaction above, is your starting material a solid or a liquid? [1 Mark]
Experiment 4: Synthesis of a tertiary alkyl halide Page 3 of 6 Distillation is a technique that is to purify liquid compounds. Use theoretical data to explain how distillation is used to separate the target product in this reaction from any residual unreacted starting material in the reaction. [2 marks]
Experiment 4: Synthesis of a tertiary alkyl halide Page 5 of
6
Experiment 4: Synthesis of a tertiary alkyl halide Page 5 of 6 Assuming that all other experimental conditions are the same; explain if an S,1 reaction would still occur if the following changes were made. If an Sk1 reaction would still occur: then state the IUPAC name and draw the structure of the product formed compare the rate of reaction to the rate of the original reaction (in...
Experiment 4: Synthesis of a tertiary alkyl halide Page 3 of 6 The term "side reactions" refers to any chemical reaction that can occur that form products other than the desired product. Side reactions can consume the reactants of your intended reaction, and can affect the percent yield of your target product. Draw the full reaction mechanism for a possible side reaction that can occur under these reaction conditions. Include all charges and intermediates. Vaguely directed arrows will not receive...
Page 1 Synthesis using Carbonyl O-Substitution Chemistry Preamble This experiment involves the synthesis of target molecules using a-substitution chemistry. You are assigned two target molecules, one of which is best synthesized by an alkylation approach, while the other is best synthesized by an addition or condensation approach. You must do the following: 1. Perform a retrosynthetic analysis on the two target molecules assigned to you. In each case the organic starting material (what you have to work backwards toward) depends...
2) Predict the order of reactivity (1=least, 4=most) of
primary, secondary, tertiary, and aryl halides toward nucleophilic
displacement by an SN1 reaction mechanism. Explain
3) Give a detailed summary of the chemistry in both reactions
SN2 and SN1 in details please for both reactions. include any
general statements about the experiments.
LAB)o Organic Chemistry I Lab CHEM 3512 Nueleophilic Substitution Reactions: Sl vs S2 To review Sul, S2, El and E2 reactions and mechanisms and compare and contrast the effect...
Synthesis using Carbonyla-Substitution Chemistry Preamble This experiment involves the synthesis of target molecules using a-substitution chemistry. You are assigned two target molecules, one of which is best synthesized by an alkylation approach, while the other is best synthesized by an addition or condensation approach. My two target molecules are number 2 and number 12 in the last page. You must do the following: 1. Perform a retrosynthetic analysis on the two target molecules assigned to you. In each case the...
Experiment Write Up Proposal You will write up a synthesis procedure for one reaction that could be potentially run in a face- to-face Chem 2321 lab session. Your proposal will include an introduction and procedure. The procedure will include step-by-step instructions for running the reaction (including reaction monitoring), work-up. (product isolation and purification), and analysis (characterization). You will need to include sample calculations for percent yield and provide sample spectra analysis. You must upload your proposal as a single document...
The following questions are from an experiment titled
Friedel-Crafts Alkylation for Organic Chemistry II Lab. There are
pictures attached of the lab manual.
2) Is this method a good route for the preparation of
p-sec-butyltoulene? Give reasons for your answer.
3) Why do you use a large excess of toulene. What are its
functions?
4) What is the purpose for adding the hydrochloric acid to the
water in the separatory funnel in step 5? Hint: If no acid is
added,...
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