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What is the product of a diels-alder reaction between
9-anthracenemethan and N-methylmaleimide in water? what is...
Need help labelling all possible peaks from the attached Diels-Alder reaction. H20 N- Δ1hr он 9-anthracenemethanol N-methylmaleimide 9-(hydroxymethyl)-13-methyl-9,10- dihydro-9,10-13,4]epipyrrolo...
Need help labelling all possible peaks from the attached
Diels-Alder reaction.
H20 N- Δ1hr он 9-anthracenemethanol N-methylmaleimide 9-(hydroxymethyl)-13-methyl-9,10- dihydro-9,10-13,4]epipyrroloanthracene- 12,14-dione adues 09 1%
H20 N- Δ1hr он 9-anthracenemethanol N-methylmaleimide 9-(hydroxymethyl)-13-methyl-9,10- dihydro-9,10-13,4]epipyrroloanthracene- 12,14-dione
adues 09 1%
Explain the Diels-Alder reaction of anthracene-9-methanol and N-methylmaleimide with water.
Explain the Diels-Alder reaction of anthracene-9-methanol and N-methylmaleimide with water.
What is the balanced chemical equation for this reaction? HE ALDOL REACTION: TETRAPHENYLCYCLOPENTADIENONE Synthetic Chemistry Lab....
What is the balanced chemical equation for this reaction?
HE ALDOL REACTION: TETRAPHENYLCYCLOPENTADIENONE Synthetic Chemistry Lab. Semester 1, 2019 1F Ph Ph Ph Ph КОН, ETOH Ph Ph Ph Ph Reflux Buchner filtration KOH: corrosive - especially as a solution in ethanol! Dissolve potassium hydroxide (145 mg) in ethanol (1 mL) in a 10 mL round bottomed flask. Add benzil (1 g) and 1,3-diphenylacetone (1 g) to a 50 mL round bottomed flask. Add ethanol (7 mL) and a magnetic...
Anthracene -9-methanol and 3 equivalents of N-methylmaleimide were mixed with water in an Erlenmeyer flask and...
Anthracene -9-methanol and 3 equivalents of N-methylmaleimide were mixed with water in an Erlenmeyer flask and heated to reflux( Diels-Adler reaction) TLC was prepared using a 1:1 ratio ethyl acetate: hexane. We got Rf=0.8 for N-methylmaleimide Rf=0.6 for anthracene and Rf=0.3 for the mixture. What information does this provide?
Can someone please help me interpret the IR data of a diels alder reaction product between...
Can someone please help me interpret the IR data of a diels
alder reaction product between 9-anthracenemethanol and
N-methylmaleimide. Can you show the DA product structure with the
various H species associated? Thank you.
90 Joe lan Diels Alder product 85 80 75 70 65 60 55 50 45 40 35 30 25 3000 2500 500 3500 2000 1500 1000 4000 Wavenumbers (cm-1) % Transmittance 6 3069.03 1766.39 1681.46 1474.36 1465.21 1455.61 1382 93 1295.54 1282.09 1318.30 1209.16 1141 30...
Organic Chemistery Lab This is my crude product H NMR. (Exp: Diels-Alder Reaction in water) Anthracene-9-methanol...
Organic Chemistery Lab
This is my crude product H NMR. (Exp: Diels-Alder Reaction in
water)
Anthracene-9-methanol and N-methylmaleimide react in water, and
refulx 1.5h, than Anthracene-N-methylmaleimide Des-Alder adduct was
created.
TA told me that specturm is excellent, but there are so many
mistakes at labels. Please see my data, and let me know if there
are mistakes.
17091 5i3-0502 exp#1 crude CD-04-Suwon gyenewow 27 27 26 26 26 26 25 25 25 25 24 24 23 23 22 21 20...
In this Diels-Alder reaction, what is the limiting reagent for this reaction? Please show work In...
In this Diels-Alder reaction, what is the limiting reagent for
this reaction? Please show work
In this experiment, a Diels-Alder reaction will be performed to generate 4-cyclohexene- 1,2-dicarboxylic anhydride. The reaction occurs when 1,3-butadiene is combined with maleic anhydride and heated as shown below. Once the product has been isolated, the IR spectrum, melting point, and experimental yield can be determined. 5.- I111NI O Due to the inherent difficulties with the handling of gaseous 1,3-butadiene, it will be generated in...
EXPERIMENT 2A DIELS-ALDER REACTION OF ANTHRACENE REFERENCES Pavia et al (4/e): Tech. 6.1/6.2, 7.2-7.4 Klein (1/e)...
EXPERIMENT 2A DIELS-ALDER REACTION OF ANTHRACENE REFERENCES Pavia et al (4/e): Tech. 6.1/6.2, 7.2-7.4 Klein (1/e) pp. 784-792 EQUATION heat Diels-Alder Adduct 9,30-dihydroanthracene-9,10- endo-o B-seccinic anhydride mp 262264 PROCEDURE Place 0.200 grams of anthracene and an equal molar amount of maleic anhydride in 5 mL of xylenes in a 10-mL round-bottom flask with a magnetic stir bar. Attach a water-cooled condenser and reflux for 60 minutes. Allow the solution to cool to room temperature and then place the flask in...
Question- The second step is a name reaction. a) What is its name: b) Is it...
Question- The second step is a name reaction. a) What is its name: b) Is it OK that we left the reaction in our drawer over the week? What would have happened if we didn’t have a good seal on the stopper? Draw a possible reaction scheme. Background The field of medicinal chemistry combines the specialties of synthetic organic chemistry and biology, and biochemistry. Compounds are generated and biological activity is screened using target specific assays. . These assays are...
I need help calculating theoretical yield for my Diels-Alder lab experiment. This reaction was between 1,3-butadiene...
I need help calculating theoretical yield for my
Diels-Alder lab experiment. This reaction was between 1,3-butadiene
and maleic anhydride, forming cis 1,2,3,6-tetrahydrophthalic
anhydride. In this experiment 1.0g of maleic anhydride was combined
with 1.8g 3-sulfolene and 2 mL dry xylene and refluxed for 30 mins.
6 mL of xylene was added to dissolve solids and then decanted, then
warm pet. ether was added to form crystalline product after
cooling. some of this info may be irrelevant in what is needed...
Need help labelling all possible peaks from the attached
Diels-Alder reaction.
H20 N- Δ1hr он 9-anthracenemethanol N-methylmaleimide 9-(hydroxymethyl)-13-methyl-9,10- dihydro-9,10-13,4]epipyrroloanthracene- 12,14-dione adues 09 1%
H20 N- Δ1hr он 9-anthracenemethanol N-methylmaleimide 9-(hydroxymethyl)-13-methyl-9,10- dihydro-9,10-13,4]epipyrroloanthracene- 12,14-dione
adues 09 1%
What is the balanced chemical equation for this reaction?
HE ALDOL REACTION: TETRAPHENYLCYCLOPENTADIENONE Synthetic Chemistry Lab. Semester 1, 2019 1F Ph Ph Ph Ph КОН, ETOH Ph Ph Ph Ph Reflux Buchner filtration KOH: corrosive - especially as a solution in ethanol! Dissolve potassium hydroxide (145 mg) in ethanol (1 mL) in a 10 mL round bottomed flask. Add benzil (1 g) and 1,3-diphenylacetone (1 g) to a 50 mL round bottomed flask. Add ethanol (7 mL) and a magnetic...
Can someone please help me interpret the IR data of a diels
alder reaction product between 9-anthracenemethanol and
N-methylmaleimide. Can you show the DA product structure with the
various H species associated? Thank you.
90 Joe lan Diels Alder product 85 80 75 70 65 60 55 50 45 40 35 30 25 3000 2500 500 3500 2000 1500 1000 4000 Wavenumbers (cm-1) % Transmittance 6 3069.03 1766.39 1681.46 1474.36 1465.21 1455.61 1382 93 1295.54 1282.09 1318.30 1209.16 1141 30...
Organic Chemistery Lab
This is my crude product H NMR. (Exp: Diels-Alder Reaction in
water)
Anthracene-9-methanol and N-methylmaleimide react in water, and
refulx 1.5h, than Anthracene-N-methylmaleimide Des-Alder adduct was
created.
TA told me that specturm is excellent, but there are so many
mistakes at labels. Please see my data, and let me know if there
are mistakes.
17091 5i3-0502 exp#1 crude CD-04-Suwon gyenewow 27 27 26 26 26 26 25 25 25 25 24 24 23 23 22 21 20...
In this Diels-Alder reaction, what is the limiting reagent for
this reaction? Please show work
In this experiment, a Diels-Alder reaction will be performed to generate 4-cyclohexene- 1,2-dicarboxylic anhydride. The reaction occurs when 1,3-butadiene is combined with maleic anhydride and heated as shown below. Once the product has been isolated, the IR spectrum, melting point, and experimental yield can be determined. 5.- I111NI O Due to the inherent difficulties with the handling of gaseous 1,3-butadiene, it will be generated in...
EXPERIMENT 2A DIELS-ALDER REACTION OF ANTHRACENE REFERENCES Pavia et al (4/e): Tech. 6.1/6.2, 7.2-7.4 Klein (1/e) pp. 784-792 EQUATION heat Diels-Alder Adduct 9,30-dihydroanthracene-9,10- endo-o B-seccinic anhydride mp 262264 PROCEDURE Place 0.200 grams of anthracene and an equal molar amount of maleic anhydride in 5 mL of xylenes in a 10-mL round-bottom flask with a magnetic stir bar. Attach a water-cooled condenser and reflux for 60 minutes. Allow the solution to cool to room temperature and then place the flask in...
I need help calculating theoretical yield for my
Diels-Alder lab experiment. This reaction was between 1,3-butadiene
and maleic anhydride, forming cis 1,2,3,6-tetrahydrophthalic
anhydride. In this experiment 1.0g of maleic anhydride was combined
with 1.8g 3-sulfolene and 2 mL dry xylene and refluxed for 30 mins.
6 mL of xylene was added to dissolve solids and then decanted, then
warm pet. ether was added to form crystalline product after
cooling. some of this info may be irrelevant in what is needed...
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