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The H-NMR spectrum of an unknown compound (formula CaHgO2) is shown below. Draw the structure of...
Question 2 The 13 C-NMR spectrum of an unknown compound (formula CgH180) is shown below. Its...
Question 2 The 13 C-NMR spectrum of an unknown compound (formula CgH180) is shown below. Its "H-NMR spectrum only shows one singlet at 1.2 ppm. Draw the structure of this unknown compound. 240 220 '200'180' 160140120100' 80' 604020 PPM H3CU CH3 CH3 CH3 Create OscerSketch Answer 2 Incorrect: Answer has an incorrect structure. What would be the expected splitting pattern of the signal associated with the indicated hydrogen atoms? Question 3 A. singlet B. doublet C. triplet D. quartet E....
The 1H-NMR and 13C-NMR spectra of an unknown compound (formula C8H10) are shown below. Draw the structure of the unknown...
The 1H-NMR and 13C-NMR spectra of an unknown compound (formula
C8H10) are shown below. Draw the structure of the unknown compound.
The total integration of the peaks at around 7 ppm is 4. The
integration of the peak at around 2 ppm is 6.
7 6 5 4 3 ppm TTTTTTTTTTTTTTTT 200 180 160 140 120 100 80 60 40 20 0 pom CH3 Create OscerSketch Answer 8 Incorrect: Answer has an incorrect structure.
20. Propose a structure for compound GHOST with a formula C.HO, with the tom spectrum and...
20. Propose a structure for compound GHOST with a formula C.HO, with the tom spectrum and IR spectrum. *O2 with the following 'H NMR TRANSACTIEF 21 4000 HAVENUMERI Chem Shift Rel. Area Splitting 4.1 2.0 1.7 1.5 0.9 triplet singlet nonet quartet doublet EN ppm
21. Propose a structure for compound HALLOWEEN with a formula CsH1002 with the following 'H NMR...
21. Propose a structure for compound HALLOWEEN with a formula CsH1002 with the following 'H NMR spectrum and IR spectrum. NAVENTER Area Chem Shift Splitting singlet multiplet multiplet doublet triplet Ppm
Apply the n+1 rule to assign the multiplicity (splitting) of each of the protons indicated by...
Apply the n+1 rule to assign the multiplicity (splitting) of each of the protons indicated by an arrow. Possible answers include: singlet, doublet, triplet, quartet, quintet, sextet, septet, octet and nonet. A molecule with formula C_2H_gO gave the NMR peaks below. Draw its structure.^1H NMR: 2.6 ppm (quartet, 2 hydrogens) 2.1 ppm (singlet, 3 hydrogens) 1.1 ppm (triplet, 3 hydrogens)^13C NMR: 215 ppm, 36 ppm, 26 ppm, 8 ppm
for the following 2 compounds, please calculate, and show the calculations for, the degree of unsaturation, assign the IR spectrum peaks, assign the 13C NMR peaks, assign the 1H NMR peaks, and draw th...
for the following 2 compounds, please calculate, and
show the calculations for, the degree of unsaturation, assign the
IR spectrum peaks, assign the 13C NMR peaks, assign the 1H NMR
peaks, and draw the structure for the unknown compound.
CHIM 245 Spectroscopy Problem Set #2 In this problem set there are two unknown compounds. You are provided with the formula, IR spectrum, "C NMR spectrum, and 'H NMR spectrum for each compound. Each unknown is worth 10 points, with an...
4. Consider the following two diastercomers: Both compounds generate 'H NMR spectra with the following signals:...
4. Consider the following two diastercomers: Both compounds generate 'H NMR spectra with the following signals: A multiplet between 7.20-7.63 ppm with an integration of 5H Two separate doublets between 5.70-6.50 ppm, each with an integration of 1H A singlet around 1.30 ppm with an integration of 9H Despite the similarities, how could you differentiate between the H NMR spectra of these isomers? 5. Assign each set of protons to their appropriate signals in the 'H NMR spectrum shown below....
Draw the structure that gives the NMR below. The compound has the molecular formula, CsH1002. Signal...
Draw the structure that gives the NMR below. The compound has the molecular formula, CsH1002. Signal at 4.38 (broad singlet, 1H), 3.49 (triplet, 2H), 2.40 (triplet, 2H), 2.10 (singlet, 3H), and 1.86 (pentet, 2H). IR shows a broad band at 3350 cm and a strong band at 1710 cm (in addition to others). Make sure to indicate (label) which hydrogen gives which signal. PPM
Draw the structure that has a molecular formula of C3H7CIO that produced the 'H NMR shown...
Draw the structure that has a molecular formula of C3H7CIO that produced the 'H NMR shown below. singlet 2H singlet 1H doublet 2H doublet 2H JE 12 11 10 9 8 4 3 2 1 7 6 5 Chemical shift (ppm)
A compound of unknown structure gave the following spectroscopic data: Mass spectrum: M+ = 88.1 IR:...
A compound of unknown structure gave the following
spectroscopic data:
Mass spectrum: M+ = 88.1
IR: 3600cm-1
1H NMR: 1.4 (2H, quartet, J=7Hz); 1.2 (6H, singlet); 1.0 (1H,
singlet); 0.9 (3H, triplet, J=7Hz)
13C NMR: 74, 35, 27, 25
a. assuming that the compound contains C and H but may or may not
contain O, give three possible molecular formulas.
b. how many protons (H) does the compound contain?
c. what functional group(s) does the compound contain?
d. how many...
Question 2 The 13 C-NMR spectrum of an unknown compound (formula CgH180) is shown below. Its "H-NMR spectrum only shows one singlet at 1.2 ppm. Draw the structure of this unknown compound. 240 220 '200'180' 160140120100' 80' 604020 PPM H3CU CH3 CH3 CH3 Create OscerSketch Answer 2 Incorrect: Answer has an incorrect structure. What would be the expected splitting pattern of the signal associated with the indicated hydrogen atoms? Question 3 A. singlet B. doublet C. triplet D. quartet E....
The 1H-NMR and 13C-NMR spectra of an unknown compound (formula
C8H10) are shown below. Draw the structure of the unknown compound.
The total integration of the peaks at around 7 ppm is 4. The
integration of the peak at around 2 ppm is 6.
7 6 5 4 3 ppm TTTTTTTTTTTTTTTT 200 180 160 140 120 100 80 60 40 20 0 pom CH3 Create OscerSketch Answer 8 Incorrect: Answer has an incorrect structure.
20. Propose a structure for compound GHOST with a formula C.HO, with the tom spectrum and IR spectrum. *O2 with the following 'H NMR TRANSACTIEF 21 4000 HAVENUMERI Chem Shift Rel. Area Splitting 4.1 2.0 1.7 1.5 0.9 triplet singlet nonet quartet doublet EN ppm
21. Propose a structure for compound HALLOWEEN with a formula CsH1002 with the following 'H NMR spectrum and IR spectrum. NAVENTER Area Chem Shift Splitting singlet multiplet multiplet doublet triplet Ppm
Apply the n+1 rule to assign the multiplicity (splitting) of each of the protons indicated by an arrow. Possible answers include: singlet, doublet, triplet, quartet, quintet, sextet, septet, octet and nonet. A molecule with formula C_2H_gO gave the NMR peaks below. Draw its structure.^1H NMR: 2.6 ppm (quartet, 2 hydrogens) 2.1 ppm (singlet, 3 hydrogens) 1.1 ppm (triplet, 3 hydrogens)^13C NMR: 215 ppm, 36 ppm, 26 ppm, 8 ppm
for the following 2 compounds, please calculate, and
show the calculations for, the degree of unsaturation, assign the
IR spectrum peaks, assign the 13C NMR peaks, assign the 1H NMR
peaks, and draw the structure for the unknown compound.
CHIM 245 Spectroscopy Problem Set #2 In this problem set there are two unknown compounds. You are provided with the formula, IR spectrum, "C NMR spectrum, and 'H NMR spectrum for each compound. Each unknown is worth 10 points, with an...
4. Consider the following two diastercomers: Both compounds generate 'H NMR spectra with the following signals: A multiplet between 7.20-7.63 ppm with an integration of 5H Two separate doublets between 5.70-6.50 ppm, each with an integration of 1H A singlet around 1.30 ppm with an integration of 9H Despite the similarities, how could you differentiate between the H NMR spectra of these isomers? 5. Assign each set of protons to their appropriate signals in the 'H NMR spectrum shown below....
Draw the structure that gives the NMR below. The compound has the molecular formula, CsH1002. Signal at 4.38 (broad singlet, 1H), 3.49 (triplet, 2H), 2.40 (triplet, 2H), 2.10 (singlet, 3H), and 1.86 (pentet, 2H). IR shows a broad band at 3350 cm and a strong band at 1710 cm (in addition to others). Make sure to indicate (label) which hydrogen gives which signal. PPM
Draw the structure that has a molecular formula of C3H7CIO that produced the 'H NMR shown below. singlet 2H singlet 1H doublet 2H doublet 2H JE 12 11 10 9 8 4 3 2 1 7 6 5 Chemical shift (ppm)
A compound of unknown structure gave the following
spectroscopic data:
Mass spectrum: M+ = 88.1
IR: 3600cm-1
1H NMR: 1.4 (2H, quartet, J=7Hz); 1.2 (6H, singlet); 1.0 (1H,
singlet); 0.9 (3H, triplet, J=7Hz)
13C NMR: 74, 35, 27, 25
a. assuming that the compound contains C and H but may or may not
contain O, give three possible molecular formulas.
b. how many protons (H) does the compound contain?
c. what functional group(s) does the compound contain?
d. how many...
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