4. The proton NMR and IR spectra of Compound B are shown on the next page....
Identify the peaks that identify the functional groups
in the IR spectrum
Unknown 4 C2H60 TRANSMITTANCE 1001- 0 900- 0 800- 0.700- 0.600- 0.500- 0.400- 0.300- 0200- 0.100- 0.000- 4000 IR Unknown 3500 3000 2500 2000 1000 1500 Load IR spectrum Load proton NMR Show structure Spectra are displayed using JSpecView Website maintained by Jennifer Muzyka Contact me at jennifer muzyka@centre edu. Unknown 5 C3H5NO TRANSMITTANCE 1.001 - 0.900- 0800- 0.700- 0.600- 0.500- 0.400- 0.300- 0 200- 0.100- 0 000...
In this NMR handout, you will get practice interpreting NMR spectra. Refer to the NMR tutorial/theory for chemical shifts and descriptions of peak splitting. There are 4 NMR problems. For each problem, you have been given the chemical formula as well as the IR and NMR spectra. Draw the structure for each unknown compound and provide sufficient reasoning as to why you think it has that structure. To get full credit, determine the structure of the unknown compound, calculate the...
Deduce the following structure of the compound given their IR, H1
NMR, 13C NMR spectra, and assign IR functional group absorptions
and assign the structure's protons and carbons to their respective
spectral resonances.
Compound 4 Da- U6)+20 IR Spectrum Oquid fim) 1760 800 1200 2000 1600 3000 4000 v (cm) Mass Spectrum 100 43 No significant UV absorption above 220 nm M146 (1% ) 87 20 CH1004 280 40 80 120 m/e 160 200 240 13C NMR Spectrum (1000 MHz,...
A compound with molecular formula C7H160 displays the following IR and 'H-NMR spectra. The 13C NMR data suggest that there is some symmetry within the molecule. a) Calculate the degrees of unsaturation (DU) for the compound in the space provided below. DU = b) Identify and label the two indicated peaks in the IR spectrum in the boxes provided. Identify and label ALL peaks in the 'H NMR spectrum below. The numbers given on the 'H NMR are integration values...
A compound with molecular formula C7H160 displays the following IR and 'H-NMR spectra. The 13C NMR data suggest that there is some symmetry within the molecule. a) Calculate the degrees of unsaturation (DU) for the compound in the space provided below. DU = b) Identify and label the two indicated peaks in the IR spectrum in the boxes provided. Identify and label ALL peaks in the 'H NMR spectrum below. The numbers given on the 'H NMR are integration values...
Deduce the following structure of the compound given their IR, H1
NMR, 13C NMR spectra, and assign IR functional group absorptions
and assign the structure's protons and carbons to their respective
spectral resonances.
Compound 6 1756 IR Spectrum uid Sm) 15820 4000 3000 2000 1600 1200 800 V (cm) 100 55 Mass Spectrum 71 80 70 60 No significant UV M158 (1%) absorption above 220 nm C&H140s 40 80 120 160 200 240 280 m/e 13C NMR Spectrum (50.0 MHz,...
Compound 3: Use the information provided below and the IR and NMR spectra on the next page to answer the following questions. a) An MS was taken of compound 3 and the table is given below. Determine the molecular formula of 3 from the MS given below. . relative abundance m/z 152 100 153 9.7 154 4.5 b) Calculate the Index of Hydrogen Deficiency/Degree of Unsaturation for the molecule. c) Using the IR spectrum and the 'H- and 13C-NMR spectra...
1. The IR spectra shown below is for a compound of formula C.H.O (a) Calculate the degree(s) of unsaturation (b) What are the functional groups indicated ? (C)Match the peaks to each of the corresponding functional group. (d) Propose a structure (10 points) 90 % Transmittance 1250 Wernumbers ( 1) 2. The NMR spectra shown is for a compound of formula C.H.O. (a) Calculate the degree(s) of unsaturation (b) What are the functional groups indicated ? (c)Match the peaks to...
Camphor
Analyze any given IR and/or NMR data below.
Identify functional groups in IR spectra
Identify proton locations from the H NMR.
DL- Camphor INFRARED SPECTRUM Transmitance 4000 3000 2000 Wavenumber (cm-1) 1000 Borneol INFRARED SPECTRUM 0 Relative Transmittance 0.2 UUUUUUUUUU J 3000 1000 2000 Wavenumber (cm-1) ca 00549 in CDC13, position 203 ZGCPPR (zgcpor) [rell 15 TT 3.0 1.5 1.0 Ippm]
A compound with molecular formula C7H160 displays the following IR and 'H-NMR spectra. The 13C NMR data suggest that there is some symmetry within the molecule. a) Calculate the degrees of unsaturation (DU) for the compound in the space provided below. DU = b) Identify and label the two indicated peaks in the IR spectrum in the boxes provided. Identify and label ALL peaks in the 'H NMR spectrum below. The numbers given on the 'H NMR are integration values...