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e Why is it necessary to carry out this reaction when your starting material is a...
Working on the questions at the end of this lab report (see above). I need help answering questio...
Working on the questions at the end of this lab report
(see above). I need help answering questions 2, 3, and 4 completely
and thoroughly. Thank you!
s, until the I hexano 1 clean disti CYCLOHEXENE from CYCLOHEXANOL be dehydrated with solfuric acid to yield cyclohexene and waterf Add a 0°C (record ct and cal H,SO + H20 ainer. s in purification of any crude product are (a) the preliminary separation of the product from the reaction mixture by distillation...
The following questions are from an experiment titled Friedel-Crafts Alkylation for Organic Chemistry II Lab. There...
The following questions are from an experiment titled
Friedel-Crafts Alkylation for Organic Chemistry II Lab. There are
pictures attached of the lab manual.
2) Is this method a good route for the preparation of
p-sec-butyltoulene? Give reasons for your answer.
3) Why do you use a large excess of toulene. What are its
functions?
4) What is the purpose for adding the hydrochloric acid to the
water in the separatory funnel in step 5? Hint: If no acid is
added,...
using pictures and a maximum of 10 words, explain why an oven-dried 5-ml conical vial and...
using pictures and a maximum of 10 words, explain why an oven-dried
5-ml conical vial and drying tube(step 1 and 2 of part 1) are used
in the reaction. do both please! also the notebook pages are the
procedure
(1) Using pictures and a maximum of 10 words, explain why an oven-dried 5-ml conical vial and drying tube (step 1 and 2 of Part 1) are used in the reaction. (2) After the addition of benzophenone to the mixture of...
Grignard reagent THE GRIGNARD REAGENT-PREPARATION AND REACTION In this experiment, you will prepa...
i need help with the postlab questions please
Grignard reagent THE GRIGNARD REAGENT-PREPARATION AND REACTION In this experiment, you will prepare a Grignard reagent, phenyl magnesium bromide, from bromobenzene and magnesium metal. The Grignard reagent will then react with methyl benzoate to form triphenylmethanol. Introduction Grignard reagents, such as organomagnesium halides, were discovered in 1910 by French chemist Victor Grignard. The Grignard reaction is one of the most general methods for carbon- carbon bond formation in all of organic chemistry....
1. Procedure A. Lithium 2,6-dimethylphenoxide. In a 300-ml. flask, equipped with a magnetic stirrer and a...
1. Procedure A. Lithium 2,6-dimethylphenoxide. In a 300-ml. flask, equipped with a magnetic stirrer and a reflux condenser and flushed with nitrogen, are placed 150 ml. of toluene (freshly distilled from sodium), 1.40 g. (0.202 mole) of lithium metal (Note 1) and 25.0 g. (0.205 mole) of resublimed 2,6-dimethylphenol. The mixture is heated under reflux with stirring for 36 hours; a nitrogen atmosphere is maintained for the reflux period (Note 2). The condenser is replaced by a distillation head with...
Separating a Mixture, Recrystallization, pre-lab assignment could you also explain why you chose that substance for...
Separating a Mixture, Recrystallization, pre-lab
assignment
could you also explain why you chose that substance for the empty
spaces and question marks
EXPERIMENT 4 Pre-Lab Assignment Separating a Mixture, Recrystalliration Name Date 1. Complete the following flowchart which shows how to separate a mixture of sand, sodium chloride and acetanilide. Notice that after a separation process (a down arrow) the filtered solids are shown on the left and the filtrate (the liquid) is shown on the right. The terminal step...
PREPARATION OF PHARMACEUTICALS - Fischer Esterification Reactions Q: Calculate the expected mass of both methyl salicylate and aspirin assuming 100% yield. EXPERIMENT7 PREPARATION OF PHARMACEUTICALS...
PREPARATION OF PHARMACEUTICALS - Fischer Esterification
Reactions
Q: Calculate the expected mass of both methyl salicylate and
aspirin assuming 100% yield.
EXPERIMENT7 PREPARATION OF PHARMACEUTICALS Fischer Esterification Reactions Almost 2500 years ago, physicians such as Hippocrates recommended that patients chew on the bark of the willow to alleviate pain. The active ingredient in willow bark was found to be salicin, a compound made of a molecule of salicyl alcohol bonded to a p-D-glucose molecule. In the stomach, the bond between...
help with identifiying each unknown in extraction and washing experiment. the ir spectra are given below,...
help with identifiying each unknown in extraction and washing
experiment. the ir spectra are given below, along with data, and
the lab sheet is attached.
Neutral Solid Primary amine (Aniline) 3403cm - NE presence Transmittance 60 3258cm 1 streren NOUD Streich 50 Ctretcher strator NH2 aromatto 11 NO2 aring 2-nitroaniline K LILI 3600 3200 2800 2400 2000 1800 1600 Wavenumber cm-1 1400 1200 1000 800 600 Basic Solid primary amine Transmittance I NH2 Stretch p-acetvianiline 70 60 CS HG NO...
Working on the questions at the end of this lab report
(see above). I need help answering questions 2, 3, and 4 completely
and thoroughly. Thank you!
s, until the I hexano 1 clean disti CYCLOHEXENE from CYCLOHEXANOL be dehydrated with solfuric acid to yield cyclohexene and waterf Add a 0°C (record ct and cal H,SO + H20 ainer. s in purification of any crude product are (a) the preliminary separation of the product from the reaction mixture by distillation...
The following questions are from an experiment titled
Friedel-Crafts Alkylation for Organic Chemistry II Lab. There are
pictures attached of the lab manual.
2) Is this method a good route for the preparation of
p-sec-butyltoulene? Give reasons for your answer.
3) Why do you use a large excess of toulene. What are its
functions?
4) What is the purpose for adding the hydrochloric acid to the
water in the separatory funnel in step 5? Hint: If no acid is
added,...
using pictures and a maximum of 10 words, explain why an oven-dried
5-ml conical vial and drying tube(step 1 and 2 of part 1) are used
in the reaction. do both please! also the notebook pages are the
procedure
(1) Using pictures and a maximum of 10 words, explain why an oven-dried 5-ml conical vial and drying tube (step 1 and 2 of Part 1) are used in the reaction. (2) After the addition of benzophenone to the mixture of...
i need help with the postlab questions please
Grignard reagent THE GRIGNARD REAGENT-PREPARATION AND REACTION In this experiment, you will prepare a Grignard reagent, phenyl magnesium bromide, from bromobenzene and magnesium metal. The Grignard reagent will then react with methyl benzoate to form triphenylmethanol. Introduction Grignard reagents, such as organomagnesium halides, were discovered in 1910 by French chemist Victor Grignard. The Grignard reaction is one of the most general methods for carbon- carbon bond formation in all of organic chemistry....
1. Procedure A. Lithium 2,6-dimethylphenoxide. In a 300-ml. flask, equipped with a magnetic stirrer and a reflux condenser and flushed with nitrogen, are placed 150 ml. of toluene (freshly distilled from sodium), 1.40 g. (0.202 mole) of lithium metal (Note 1) and 25.0 g. (0.205 mole) of resublimed 2,6-dimethylphenol. The mixture is heated under reflux with stirring for 36 hours; a nitrogen atmosphere is maintained for the reflux period (Note 2). The condenser is replaced by a distillation head with...
Separating a Mixture, Recrystallization, pre-lab
assignment
could you also explain why you chose that substance for the empty
spaces and question marks
EXPERIMENT 4 Pre-Lab Assignment Separating a Mixture, Recrystalliration Name Date 1. Complete the following flowchart which shows how to separate a mixture of sand, sodium chloride and acetanilide. Notice that after a separation process (a down arrow) the filtered solids are shown on the left and the filtrate (the liquid) is shown on the right. The terminal step...
PREPARATION OF PHARMACEUTICALS - Fischer Esterification
Reactions
Q: Calculate the expected mass of both methyl salicylate and
aspirin assuming 100% yield.
EXPERIMENT7 PREPARATION OF PHARMACEUTICALS Fischer Esterification Reactions Almost 2500 years ago, physicians such as Hippocrates recommended that patients chew on the bark of the willow to alleviate pain. The active ingredient in willow bark was found to be salicin, a compound made of a molecule of salicyl alcohol bonded to a p-D-glucose molecule. In the stomach, the bond between...
help with identifiying each unknown in extraction and washing
experiment. the ir spectra are given below, along with data, and
the lab sheet is attached.
Neutral Solid Primary amine (Aniline) 3403cm - NE presence Transmittance 60 3258cm 1 streren NOUD Streich 50 Ctretcher strator NH2 aromatto 11 NO2 aring 2-nitroaniline K LILI 3600 3200 2800 2400 2000 1800 1600 Wavenumber cm-1 1400 1200 1000 800 600 Basic Solid primary amine Transmittance I NH2 Stretch p-acetvianiline 70 60 CS HG NO...
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BaS crystallizes in a cubic unit cell with S2- ions on each
corner and each face....
asked 16 minutes ago -
A. 0≤P(Oi)≤10≤P(Oi)≤1 for each i
B. P(Oi)≤0P(Oi)≤0
C. P(Oi)=1+P(OCi)P(Oi)=1+P(OiC)
D. P(Oi)≥1P(Oi)≥1
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