What acidic compound is shown based on the 13C NMR and 1H NMR spectra?
I am having trouble pinpointing which acid this actually is, since I do not have a melting point associated. I attached a list of the possible ones it could be, my guess is 4-methylbenzoic acid, since there are four peaks in the H NMR, but am not 100% confident. The triplet signal shown in the top 13C spectra with ~77 ppm values are CDCL3. This was generated on a 300 MHz instrument.
![2.0765 - 11.7984 3.8985 5.0000 -7.9741 7.4412 7.4166 7.3899 7.3642 11.7363 2.4514 . 0.3909 -0.0383 (ppm] 10 15](http://img.homeworklib.com/questions/660ff440-7580-11ea-a04a-07e87c82b5a1.png?x-oss-process=image/resize,w_560)
Homework Answers
Hi Dear Friend, the unknown is 3-methyl benzoic acid (also known as m-toluic acid). To make sure our analysis and confirmation of 3-methyl benzoic acid, i am gonna attaching IR & Mass spectra here. Please cross-check them also with your spectra - this makes you confident on product confirmation.
HNMR & CNMR analysis:
Hope this helped you!
Thank You So Much! Please Rate this answer as you wish.("Thumbs Up")
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What acidic compound is shown based on the 13C NMR and 1H NMR
spectra?
I am...
MP Range: 110 degrees Celsius - 185.6 degrees Celsius Using the MP, IR& NMR spectra attached, identify the acid...
MP Range: 110 degrees Celsius - 185.6 degrees Celsius
Using the MP, IR& NMR spectra attached, identify the acid
-- from list of possibilities attached.
%Transmittance 4000 1500 1000 3500 500 3000 2500 2000 Wavenumbers (cm-1) 95.1998 8.0485 -102.1335 143.0000 -2.4552 4.6239 - 134,9771 (ppm] 8 10 12 14 [rell 200 172.3708 150 - 144.6522 130.2650 129.2161 126.5947 100 77.4381 77.0148 76.5913 21.7646 --0.0079 0 (ppm) 12 [rell 10 14 8 02 уусоехано 11 Carboxylic Acid 2-Methoxybenzoic acid 3-Phenylpropanoic acid...
On the attached image are 1H NMR, 13C NMR, and IR spectra of a compound with...
On the attached image are 1H NMR, 13C NMR, and IR
spectra of a compound with the formula C4H8O. 1H NMR signal at 1.2
is caused by 3 hydrogens, the sigbal at 2.1 is caused by 3
hydrogens, and the signal at 2.5 is caused by 2 hydrogens. Identify
the compound.
CH 1110 9 8 7 6?4 Problem 6. 'H NMR spectrum of compound HsO Problem 6. 13C NMR spectrum of compound C4HsO 200 180 160 140 120 100 80...
The 1H-NMR and 13C-NMR spectra of an unknown compound (formula C8H10) are shown below. Draw the structure of the unknown...
The 1H-NMR and 13C-NMR spectra of an unknown compound (formula
C8H10) are shown below. Draw the structure of the unknown compound.
The total integration of the peaks at around 7 ppm is 4. The
integration of the peak at around 2 ppm is 6.
7 6 5 4 3 ppm TTTTTTTTTTTTTTTT 200 180 160 140 120 100 80 60 40 20 0 pom CH3 Create OscerSketch Answer 8 Incorrect: Answer has an incorrect structure.
based on the following H NMR and C NMR determine which acid is present: 2,5- dichlorobenzoic...
based on the following H NMR and C NMR determine which acid is
present:
2,5- dichlorobenzoic acid
2,4,6- trimethylbenzoic acid
3-chlorobenzoic acid
3-hydroxybenzoic acid
2-iodobenzoic acid
7.3464 7.3243 7.3184 7.2563 See all 180 177.3251 "Bean, Klimabeth EM ACID"21" 166.5565 160 C'NMR Acid 140 140.0977 135.1928 datalos Bep_Spee Fall 2017 Section Aids - 123.5895 121.8342 120 117.5069 100 110-110 = Benene Ring 80 (ppm] CDCI 82.3304 81.9045 81,4789 50 fred H'NMR - Acid Bean irabeth NEW ACID" "5:\n\data\chnos\sep spec Mall 2019...
Create OscerSkotch Answer 6 Th e 1H-NMR and 13C-NMR spectra of an unknown compound s (formula...
Create OscerSkotch Answer 6 Th e 1H-NMR and 13C-NMR spectra of an unknown compound s (formula CoMzo) are shown below. Draw the structure of B. The total integration of the peaks at around 7 ppm is 4. The integration of the peak at around 2 ppm is 6 ppm 200 180 160 140 120 100 060 4020
What information can we gather from these three spectra (IR, H NMR, 13C NMR) to correctly...
What information can we gather from these three spectra (IR, H
NMR, 13C NMR) to correctly identify the unknown compound? What is
the identity of my unknown? Please explain how we get there and
from what information we do so. I understand that I must initially
use the rule of 13.
IR Spectrum:
H NMR Spectrum:
13C NMR spectra:
OOT 08 TRANSMITTANCE [%] 09 0+ 4000 3500 3000 2500 2000 WAVENUMBER [cm-1] 15:00 10:00 500 1H NMR 2 3 12.10ģ...
What is the structure of unknown compound based on 1H and 13C NMR and IR Spectra...
What is the structure of unknown compound based on 1H and 13C
NMR and IR Spectra
BRUKER 3500 3000 2500 2000 Wavenumber cm-1 1500 1000 500 C1OPUS 65)MEASIGB Product 20 GB Product 2 Instrument type and / or accessony 01/03/2018 Page 1/1
What is the structure of the known compound based on 1H and 13C NMR. Explain steps...
What is the structure of the known compound based on 1H and 13C
NMR. Explain steps and reasoning
N-acetylanthranilic acid ppm
The following slides contain 1H and 13C-NMR spectra as well as GC/MS spectra for compound 2...
The following slides contain 1H and 13C-NMR spectra as well as
GC/MS spectra for compound 2 shown below. After analyzing the
spectra, assign all proton and carbon NMR signals using the
numbering given on the structure. Additionally, present your data
in table form including chemical shift, integration, coupling
pattern, and coupling constants (where possible). For mass spectral
data, justify key fragmentations (those which are starred*) by
proposing fragment structures.
5 96337 03828 047734 739073 23444 14703 3 8 9 2...
5-A compound (CH40) has the following 1H NMR, 13C NMR, and IR spectra. Propose a structure...
5-A compound (CH40) has the following 1H NMR, 13C NMR, and IR spectra. Propose a structure consistent with this data. Part marks are available so show your work! Clearly indicate your final proposed structure (10 Marks) C8H140 TOO -140 SI 30 3000 1000 2000 1000 Warenumbers (cm) 200 180 160 140 120 100 80 60 40 20 ppm ketone ble 1530 1510 1500 H 5.0 4.5 4.0 3.5 3.0 2.5 2.0 15 pm 4
MP Range: 110 degrees Celsius - 185.6 degrees Celsius
Using the MP, IR& NMR spectra attached, identify the acid
-- from list of possibilities attached.
%Transmittance 4000 1500 1000 3500 500 3000 2500 2000 Wavenumbers (cm-1) 95.1998 8.0485 -102.1335 143.0000 -2.4552 4.6239 - 134,9771 (ppm] 8 10 12 14 [rell 200 172.3708 150 - 144.6522 130.2650 129.2161 126.5947 100 77.4381 77.0148 76.5913 21.7646 --0.0079 0 (ppm) 12 [rell 10 14 8 02 уусоехано 11 Carboxylic Acid 2-Methoxybenzoic acid 3-Phenylpropanoic acid...
On the attached image are 1H NMR, 13C NMR, and IR
spectra of a compound with the formula C4H8O. 1H NMR signal at 1.2
is caused by 3 hydrogens, the sigbal at 2.1 is caused by 3
hydrogens, and the signal at 2.5 is caused by 2 hydrogens. Identify
the compound.
CH 1110 9 8 7 6?4 Problem 6. 'H NMR spectrum of compound HsO Problem 6. 13C NMR spectrum of compound C4HsO 200 180 160 140 120 100 80...
The 1H-NMR and 13C-NMR spectra of an unknown compound (formula
C8H10) are shown below. Draw the structure of the unknown compound.
The total integration of the peaks at around 7 ppm is 4. The
integration of the peak at around 2 ppm is 6.
7 6 5 4 3 ppm TTTTTTTTTTTTTTTT 200 180 160 140 120 100 80 60 40 20 0 pom CH3 Create OscerSketch Answer 8 Incorrect: Answer has an incorrect structure.
based on the following H NMR and C NMR determine which acid is
present:
2,5- dichlorobenzoic acid
2,4,6- trimethylbenzoic acid
3-chlorobenzoic acid
3-hydroxybenzoic acid
2-iodobenzoic acid
7.3464 7.3243 7.3184 7.2563 See all 180 177.3251 "Bean, Klimabeth EM ACID"21" 166.5565 160 C'NMR Acid 140 140.0977 135.1928 datalos Bep_Spee Fall 2017 Section Aids - 123.5895 121.8342 120 117.5069 100 110-110 = Benene Ring 80 (ppm] CDCI 82.3304 81.9045 81,4789 50 fred H'NMR - Acid Bean irabeth NEW ACID" "5:\n\data\chnos\sep spec Mall 2019...
Create OscerSkotch Answer 6 Th e 1H-NMR and 13C-NMR spectra of an unknown compound s (formula CoMzo) are shown below. Draw the structure of B. The total integration of the peaks at around 7 ppm is 4. The integration of the peak at around 2 ppm is 6 ppm 200 180 160 140 120 100 060 4020
What information can we gather from these three spectra (IR, H
NMR, 13C NMR) to correctly identify the unknown compound? What is
the identity of my unknown? Please explain how we get there and
from what information we do so. I understand that I must initially
use the rule of 13.
IR Spectrum:
H NMR Spectrum:
13C NMR spectra:
OOT 08 TRANSMITTANCE [%] 09 0+ 4000 3500 3000 2500 2000 WAVENUMBER [cm-1] 15:00 10:00 500 1H NMR 2 3 12.10ģ...
What is the structure of unknown compound based on 1H and 13C
NMR and IR Spectra
BRUKER 3500 3000 2500 2000 Wavenumber cm-1 1500 1000 500 C1OPUS 65)MEASIGB Product 20 GB Product 2 Instrument type and / or accessony 01/03/2018 Page 1/1
What is the structure of the known compound based on 1H and 13C
NMR. Explain steps and reasoning
N-acetylanthranilic acid ppm
The following slides contain 1H and 13C-NMR spectra as well as
GC/MS spectra for compound 2 shown below. After analyzing the
spectra, assign all proton and carbon NMR signals using the
numbering given on the structure. Additionally, present your data
in table form including chemical shift, integration, coupling
pattern, and coupling constants (where possible). For mass spectral
data, justify key fragmentations (those which are starred*) by
proposing fragment structures.
5 96337 03828 047734 739073 23444 14703 3 8 9 2...
5-A compound (CH40) has the following 1H NMR, 13C NMR, and IR spectra. Propose a structure consistent with this data. Part marks are available so show your work! Clearly indicate your final proposed structure (10 Marks) C8H140 TOO -140 SI 30 3000 1000 2000 1000 Warenumbers (cm) 200 180 160 140 120 100 80 60 40 20 ppm ketone ble 1530 1510 1500 H 5.0 4.5 4.0 3.5 3.0 2.5 2.0 15 pm 4
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