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17. Draw a flow sheet to show how you would separate a mixture of benzoic acid,...
Acid/Base Extraction ACID/BASE EXTRACTION Provide a flow chart detailing the acid/base extraction/separation of the compounds shown...
Acid/Base Extraction
ACID/BASE EXTRACTION Provide a flow chart detailing the acid/base extraction/separation of the compounds shown below. Your answer must employ the following reagents: methylene chloride, hydrochloric acid (1M & 6M), sodium hydroxide (1M & 6M), 10% sodium bicarbonate (aq). Clearly indicate the product(s) and layers formed following each step of your separation scheme. HINT: phenol is soluble in sodium hydroxide solution but insoluble in neutral water or sodium bicarbonate solution. Benzoic acid is soluble in both sodium hydroxide and...
Given a solid mixture of the following molecules determine a separate scheme that can be used...
Given a solid mixture of the following molecules determine a separate scheme that can be used to separate the mixture using acid base extraction. - 2-hydroxybenzoic acid - 4-chloroanaline - trans-stillbene The following solvents and reagents will be available for use during the experiment 1. 5% sodium bicarbonate 2. 10% sodium hydroxide 3. Saturated sodium chloride 4. 5% hydrochloric acid 5. 6 M hydrochloric acid 6. Diethyl ether 7. Anhydrous sodium or magnesium sulfate *Can you include a experimental procedure...
Provide a flow chart detailing the acid/base extraction/separation of the compounds show below. Your answer must...
Provide a flow chart detailing the acid/base extraction/separation of the compounds show below. Your answer must employ the following reagents: methylene chloride, hydrochloric acid (1M & 6M), sodium hydroxide (1M & 6M), 10% sodium bicarbonate (aq). Clearly indicate the product(s) and layers formed following each step of your separation scheme. IMPORTANT: p-cresol is soluble in sodium hydroxide solution but insoluble in neutral water or sodium bicarbonate solution. 2-ethylbenzoic acid is soluble in both sodium hydroxide and sodium bicarbonate solutions. Use...
Acid/Base Extraction 1. Provide a flow chart detailing the acid/base extraction/separation of the compounds shown below....
Acid/Base Extraction
1. Provide a flow chart detailing the acid/base
extraction/separation of the compounds shown below. Your answer
must employ the following reagents: methylene chloride,
hydrochloric acid (1M & 6M), sodium hydroxide (1M & 6M),
10% sodium bicarbonate (aq). Clearly indicate the product(s) and
layers formed following each step of your separation scheme.
IMPORTANT: p-cresol is soluble in sodium hydroxide solution but
insoluble in neutral water or sodium bicarbonate solution. 2-
ethylbenzoic acid is soluble in both sodium hydroxide and...
Given: 50mL of solution diethyl ether solution containing 1.00g each of benzoic acid, phenol and aniline,50 mL of sodium...
Given: 50mL of solution diethyl ether solution containing 1.00g each of benzoic acid, phenol and aniline,50 mL of sodium bicarbonate solution, 50 ml of sodium hydroxide solution, sodium sulfate and HCl. 1. Which layer in the separatory funnel (top or bottom layer) is the organic layer during an extraction process? 2. Given that sodium bicarbonate and sodium hydroxide solution are 5% by weight, what would be the volume of 1M HCl needed to be added for acidification to crystalize the...
Provide a flow chart detailing the acid/base extraction/separation of the compounds shown below. Your answer must...
Provide a flow chart detailing the acid/base extraction/separation of the compounds shown below. Your answer must employ the following reagents: methylene chloride, hydrochloric acid M 6M), sodium hydroxide (IM & 6M),10% sodium bicarbonate (aq Clearly indicate the product(s) and layers formedfollowing each step of your separation scheme. HINT: phenol is soluble in sodium hydroxide solution but insoluble in neutral water or sodium bicarbonate solution. Benzoic acid is soluble in both sodium hydroxide and sodium bicarbonate solutions. Use skeletal structures only...
Extraction of benzoic acid and 9-fluorenone using diethyl ether. (please do not include ethyl 4- aminobenzoate)....
Extraction of benzoic acid and 9-fluorenone using diethyl ether. (please do not include ethyl 4- aminobenzoate). I have to create a flow chart to diagram the key steps of the experiment and isolation of products. 0.100g of benzoic acid and 9-fluorenone are dissolved in diethyl ether. The extraction solvent is 5% sodium hydroxide (to extract the acidic component from the organic phase). Saturated sodium chloride is added to the organic layer. drying the organic solution: anhydrous sodium sulfate is added...
Write a small introduction in words and a conclusion for this lab report Experiment 9 Acid-Base Extraction Liquid-liquid extraction utilizes the contrast solubilities of solutes in two immiscible...
Write a small introduction in words and a conclusion for this
lab report
Experiment 9 Acid-Base Extraction Liquid-liquid extraction utilizes the contrast solubilities of solutes in two immiscible solvents the separation of a mixture. An extracting solvent can be reactive that changes the character of solute. Consider a mixture of organic acid, organic base, and neutral substance, for example, benzoic acid, aniline, biphenyl, nd phenol. They sodium benzoate. Sodium hydroxide changes phenol to sodium phenoxide. Hydrochloric acid changes aniline to...
13. A solution of naphthalene, aniline, and benzoic acid in CH;Cl2 is treated with aqueous NaOH....
13. A solution of naphthalene, aniline, and benzoic acid in CH;Cl2 is treated with aqueous NaOH. What compound is extracted into the aqueous layer? NH2 он naphthalene benzoic acid aniline a. naphthalene b. aniline, as its sodium salt c. benzoic acid, as its sodium salt d. aniline and naphthalene 14. Which of the following Sy1 reactions did the Spartan program predict to have the lowest energy (AHrn, kcal/mol)? a. CH;CH;CH;CH;CI → CH;CHCH;CH, + Cr b. CH;CH;CHCICH3 CH;CH2CHCH, + Cr to...
Given a mixture (0.5g total) with 50% 2-chlorobenzoic acid, 40% fluorene, and 10% 1,4-dibromobenzene, write a...
Given a mixture (0.5g total) with 50% 2-chlorobenzoic acid, 40% fluorene, and 10% 1,4-dibromobenzene, write a complete scheme/procedure for separation and purification. The following reagents will be available to use in the lab: 1M NaOH, 6M NaOH, 1M HCl, 6M HCl, 1M NaHCO3, saturated NaCl, diethyl ether, 95% ethanol, nethanol, isopropyl alcohol, acetone, hexane, toluene, methylene chloride, and anhydrous sodium sulfate. In addition, N2 gas will be available for evaporation and a vacuum will be available for filtration. Once you...
Acid/Base Extraction
ACID/BASE EXTRACTION Provide a flow chart detailing the acid/base extraction/separation of the compounds shown below. Your answer must employ the following reagents: methylene chloride, hydrochloric acid (1M & 6M), sodium hydroxide (1M & 6M), 10% sodium bicarbonate (aq). Clearly indicate the product(s) and layers formed following each step of your separation scheme. HINT: phenol is soluble in sodium hydroxide solution but insoluble in neutral water or sodium bicarbonate solution. Benzoic acid is soluble in both sodium hydroxide and...
Provide a flow chart detailing the acid/base extraction/separation of the compounds show below. Your answer must employ the following reagents: methylene chloride, hydrochloric acid (1M & 6M), sodium hydroxide (1M & 6M), 10% sodium bicarbonate (aq). Clearly indicate the product(s) and layers formed following each step of your separation scheme. IMPORTANT: p-cresol is soluble in sodium hydroxide solution but insoluble in neutral water or sodium bicarbonate solution. 2-ethylbenzoic acid is soluble in both sodium hydroxide and sodium bicarbonate solutions. Use...
Acid/Base Extraction
1. Provide a flow chart detailing the acid/base
extraction/separation of the compounds shown below. Your answer
must employ the following reagents: methylene chloride,
hydrochloric acid (1M & 6M), sodium hydroxide (1M & 6M),
10% sodium bicarbonate (aq). Clearly indicate the product(s) and
layers formed following each step of your separation scheme.
IMPORTANT: p-cresol is soluble in sodium hydroxide solution but
insoluble in neutral water or sodium bicarbonate solution. 2-
ethylbenzoic acid is soluble in both sodium hydroxide and...
Provide a flow chart detailing the acid/base extraction/separation of the compounds shown below. Your answer must employ the following reagents: methylene chloride, hydrochloric acid M 6M), sodium hydroxide (IM & 6M),10% sodium bicarbonate (aq Clearly indicate the product(s) and layers formedfollowing each step of your separation scheme. HINT: phenol is soluble in sodium hydroxide solution but insoluble in neutral water or sodium bicarbonate solution. Benzoic acid is soluble in both sodium hydroxide and sodium bicarbonate solutions. Use skeletal structures only...
Write a small introduction in words and a conclusion for this
lab report
Experiment 9 Acid-Base Extraction Liquid-liquid extraction utilizes the contrast solubilities of solutes in two immiscible solvents the separation of a mixture. An extracting solvent can be reactive that changes the character of solute. Consider a mixture of organic acid, organic base, and neutral substance, for example, benzoic acid, aniline, biphenyl, nd phenol. They sodium benzoate. Sodium hydroxide changes phenol to sodium phenoxide. Hydrochloric acid changes aniline to...
13. A solution of naphthalene, aniline, and benzoic acid in CH;Cl2 is treated with aqueous NaOH. What compound is extracted into the aqueous layer? NH2 он naphthalene benzoic acid aniline a. naphthalene b. aniline, as its sodium salt c. benzoic acid, as its sodium salt d. aniline and naphthalene 14. Which of the following Sy1 reactions did the Spartan program predict to have the lowest energy (AHrn, kcal/mol)? a. CH;CH;CH;CH;CI → CH;CHCH;CH, + Cr b. CH;CH;CHCICH3 CH;CH2CHCH, + Cr to...
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