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Provide a flow chart detailing the acid/base extraction/separation of the compounds shown below. Your answer must...
Acid/Base Extraction ACID/BASE EXTRACTION Provide a flow chart detailing the acid/base extraction/separation of the compounds shown...
Acid/Base Extraction
ACID/BASE EXTRACTION Provide a flow chart detailing the acid/base extraction/separation of the compounds shown below. Your answer must employ the following reagents: methylene chloride, hydrochloric acid (1M & 6M), sodium hydroxide (1M & 6M), 10% sodium bicarbonate (aq). Clearly indicate the product(s) and layers formed following each step of your separation scheme. HINT: phenol is soluble in sodium hydroxide solution but insoluble in neutral water or sodium bicarbonate solution. Benzoic acid is soluble in both sodium hydroxide and...
Provide a flow chart detailing the acid/base extraction/separation of the compounds show below. Your answer must...
Provide a flow chart detailing the acid/base extraction/separation of the compounds show below. Your answer must employ the following reagents: methylene chloride, hydrochloric acid (1M & 6M), sodium hydroxide (1M & 6M), 10% sodium bicarbonate (aq). Clearly indicate the product(s) and layers formed following each step of your separation scheme. IMPORTANT: p-cresol is soluble in sodium hydroxide solution but insoluble in neutral water or sodium bicarbonate solution. 2-ethylbenzoic acid is soluble in both sodium hydroxide and sodium bicarbonate solutions. Use...
Acid/Base Extraction 1. Provide a flow chart detailing the acid/base extraction/separation of the compounds shown below....
Acid/Base Extraction
1. Provide a flow chart detailing the acid/base
extraction/separation of the compounds shown below. Your answer
must employ the following reagents: methylene chloride,
hydrochloric acid (1M & 6M), sodium hydroxide (1M & 6M),
10% sodium bicarbonate (aq). Clearly indicate the product(s) and
layers formed following each step of your separation scheme.
IMPORTANT: p-cresol is soluble in sodium hydroxide solution but
insoluble in neutral water or sodium bicarbonate solution. 2-
ethylbenzoic acid is soluble in both sodium hydroxide and...
Write a small introduction in words and a conclusion for this lab report Experiment 9 Acid-Base Extraction Liquid-liquid extraction utilizes the contrast solubilities of solutes in two immiscible...
Write a small introduction in words and a conclusion for this
lab report
Experiment 9 Acid-Base Extraction Liquid-liquid extraction utilizes the contrast solubilities of solutes in two immiscible solvents the separation of a mixture. An extracting solvent can be reactive that changes the character of solute. Consider a mixture of organic acid, organic base, and neutral substance, for example, benzoic acid, aniline, biphenyl, nd phenol. They sodium benzoate. Sodium hydroxide changes phenol to sodium phenoxide. Hydrochloric acid changes aniline to...
The Separation of Three Organic Compounds by Acid, Base Reactions and Liquid, Liquid Extraction. Okay, so...
The Separation of Three Organic Compounds by Acid, Base Reactions and Liquid, Liquid Extraction. Okay, so we had solid benzoic acid, ethyl 4- aminobenzoate, and 9-fluorenone all dissolved in methyleene chloride. We separated the basic component by adding 3M HCl, we separated the acidic component by adding 3M NaOH. I don't understand what happens here. To isolate the acidic solution, we added 6 M NaOH and used the vacuum to recover the solid. To isolate the basic solution we added...
1.Where in the separation procedure could you lose one or more of the panacetin components? Explain...
1.Where in the separation procedure could you lose one or more of the panacetin components? Explain which component could be lost in which step. 2.In the separation scheme, the dichloromethane solution is extracted with sodium bicarbonate. What would happen if the dichloromethane solution was extracted with hydrochloric acid instead (which has actually happened)? Would the separation scheme still work? Explain your reasoning 3. Acetaminophen (the active ingredient in Tylenol) is insoluble in water, soluble in sodium hydroxide solution, insoluble in...
17. Draw a flow sheet to show how you would separate a mixture of benzoic acid,...
17. Draw a flow sheet to show how you would separate a mixture of benzoic acid, 2-naphthol, aniline, and naphthalene. (indicate the solvent, location and composition of each layer). Draw all balanced equations. (6') Reagents available: 3M hydrochloric acid solution, 3M sodium hydroxide solution, 3M sodium bicarbonate solution, saturated sodium chloride solution Solvent available: water, dichloromethane, ethanol, and diethyl ether.
17. Draw a flow sheet to show how you would separate a mixture of benzoic acid, 2-naphthol, aniline, and naphthalene....
The Separation of Three Organic Compounds by Acid, Base Reactions and Liquid, Liquid Extraction. Okay, so...
The Separation of Three Organic Compounds by Acid, Base Reactions and Liquid, Liquid Extraction. Okay, so we had solid benzoic acid, ethyl 4- aminobenzoate, and 9-fluorenone all dissolved in diethyl ether. We separated the basic component by adding 3M HCl, we separated the acidic component by adding 3M NaOH. I don't understand what happens here. To isolate the acidic solution, we added 6 M NaOH and used the vacuum to recover the solid. To isolate the basic solution we added...
Extraction Complete the separation scheme for the following compounds that are dissolved in an ether solution:...
Extraction
Complete the separation scheme for the following compounds
that are dissolved in an ether solution: benzoic acid (AH), ethyl
4-aminobenzoate (:B), and napthalene (Neu). You may complete the
separation scheme using the abbreviations.
Week One Post-Lab Question 2. Separation Scheme. AH bende acid B ethy H-aminobenzoate Neu naplatene Nooreen indien IM HCI Write balanced equations for the reaction of each species with HIC soluble in Circle the major species. Indicate the solubility of cach of the major species in...
Construct a flow chart that follows the separation of a mixture of 2-nitrophenol (an organic acid...
Construct a flow chart that follows the separation of a mixture
of 2-nitrophenol (an organic acid not used in this experiment with
a pKa = 7.26) and anthracene (neutral organic). Use scheme 1 as a
template. Your reagents available are the same ones used in this
lab.
Scheme 1. The acid-base extraction of p-creol (an acidic phenol) and para-nitrotoluene (a neutral organic compound). OH 1. dissolve in TBME 2. Add NaOH/H,0 ON less dense TBME Layer Remove bottom laver Place...
Acid/Base Extraction
ACID/BASE EXTRACTION Provide a flow chart detailing the acid/base extraction/separation of the compounds shown below. Your answer must employ the following reagents: methylene chloride, hydrochloric acid (1M & 6M), sodium hydroxide (1M & 6M), 10% sodium bicarbonate (aq). Clearly indicate the product(s) and layers formed following each step of your separation scheme. HINT: phenol is soluble in sodium hydroxide solution but insoluble in neutral water or sodium bicarbonate solution. Benzoic acid is soluble in both sodium hydroxide and...
Provide a flow chart detailing the acid/base extraction/separation of the compounds show below. Your answer must employ the following reagents: methylene chloride, hydrochloric acid (1M & 6M), sodium hydroxide (1M & 6M), 10% sodium bicarbonate (aq). Clearly indicate the product(s) and layers formed following each step of your separation scheme. IMPORTANT: p-cresol is soluble in sodium hydroxide solution but insoluble in neutral water or sodium bicarbonate solution. 2-ethylbenzoic acid is soluble in both sodium hydroxide and sodium bicarbonate solutions. Use...
Acid/Base Extraction
1. Provide a flow chart detailing the acid/base
extraction/separation of the compounds shown below. Your answer
must employ the following reagents: methylene chloride,
hydrochloric acid (1M & 6M), sodium hydroxide (1M & 6M),
10% sodium bicarbonate (aq). Clearly indicate the product(s) and
layers formed following each step of your separation scheme.
IMPORTANT: p-cresol is soluble in sodium hydroxide solution but
insoluble in neutral water or sodium bicarbonate solution. 2-
ethylbenzoic acid is soluble in both sodium hydroxide and...
Write a small introduction in words and a conclusion for this
lab report
Experiment 9 Acid-Base Extraction Liquid-liquid extraction utilizes the contrast solubilities of solutes in two immiscible solvents the separation of a mixture. An extracting solvent can be reactive that changes the character of solute. Consider a mixture of organic acid, organic base, and neutral substance, for example, benzoic acid, aniline, biphenyl, nd phenol. They sodium benzoate. Sodium hydroxide changes phenol to sodium phenoxide. Hydrochloric acid changes aniline to...
17. Draw a flow sheet to show how you would separate a mixture of benzoic acid, 2-naphthol, aniline, and naphthalene. (indicate the solvent, location and composition of each layer). Draw all balanced equations. (6') Reagents available: 3M hydrochloric acid solution, 3M sodium hydroxide solution, 3M sodium bicarbonate solution, saturated sodium chloride solution Solvent available: water, dichloromethane, ethanol, and diethyl ether.
17. Draw a flow sheet to show how you would separate a mixture of benzoic acid, 2-naphthol, aniline, and naphthalene....
Extraction
Complete the separation scheme for the following compounds
that are dissolved in an ether solution: benzoic acid (AH), ethyl
4-aminobenzoate (:B), and napthalene (Neu). You may complete the
separation scheme using the abbreviations.
Week One Post-Lab Question 2. Separation Scheme. AH bende acid B ethy H-aminobenzoate Neu naplatene Nooreen indien IM HCI Write balanced equations for the reaction of each species with HIC soluble in Circle the major species. Indicate the solubility of cach of the major species in...
Construct a flow chart that follows the separation of a mixture
of 2-nitrophenol (an organic acid not used in this experiment with
a pKa = 7.26) and anthracene (neutral organic). Use scheme 1 as a
template. Your reagents available are the same ones used in this
lab.
Scheme 1. The acid-base extraction of p-creol (an acidic phenol) and para-nitrotoluene (a neutral organic compound). OH 1. dissolve in TBME 2. Add NaOH/H,0 ON less dense TBME Layer Remove bottom laver Place...
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