1.Where in the separation procedure could you lose one or more of the panacetin components? Explain...
1.Where in the separation procedure could you lose one or more of the panacetin components? Explain which component could be lost in which step.
2.In the separation scheme, the dichloromethane solution is extracted with sodium bicarbonate. What would happen if the dichloromethane solution was extracted with hydrochloric acid instead (which has actually happened)? Would the separation scheme still work? Explain your reasoning
3. Acetaminophen (the active ingredient in Tylenol) is insoluble in water, soluble in sodium hydroxide solution, insoluble in hydrochloric acid, and insoluble in dichloromethane. If your Panacetin sample contained acetaminophen, where would it be separated in the separation scheme? Explain your reasoning.
Homework Answers
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1.Where in the separation procedure could you lose one or more
of the panacetin components? Explain...
Provide a flow chart detailing the acid/base extraction/separation of the compounds show below. Your answer must...
Provide a flow chart detailing the acid/base extraction/separation of the compounds show below. Your answer must employ the following reagents: methylene chloride, hydrochloric acid (1M & 6M), sodium hydroxide (1M & 6M), 10% sodium bicarbonate (aq). Clearly indicate the product(s) and layers formed following each step of your separation scheme. IMPORTANT: p-cresol is soluble in sodium hydroxide solution but insoluble in neutral water or sodium bicarbonate solution. 2-ethylbenzoic acid is soluble in both sodium hydroxide and sodium bicarbonate solutions. Use...
Acid/Base Extraction 1. Provide a flow chart detailing the acid/base extraction/separation of the compounds shown below....
Acid/Base Extraction
1. Provide a flow chart detailing the acid/base
extraction/separation of the compounds shown below. Your answer
must employ the following reagents: methylene chloride,
hydrochloric acid (1M & 6M), sodium hydroxide (1M & 6M),
10% sodium bicarbonate (aq). Clearly indicate the product(s) and
layers formed following each step of your separation scheme.
IMPORTANT: p-cresol is soluble in sodium hydroxide solution but
insoluble in neutral water or sodium bicarbonate solution. 2-
ethylbenzoic acid is soluble in both sodium hydroxide and...
Provide a flow chart detailing the acid/base extraction/separation of the compounds shown below. Your answer must...
Provide a flow chart detailing the acid/base extraction/separation of the compounds shown below. Your answer must employ the following reagents: methylene chloride, hydrochloric acid M 6M), sodium hydroxide (IM & 6M),10% sodium bicarbonate (aq Clearly indicate the product(s) and layers formedfollowing each step of your separation scheme. HINT: phenol is soluble in sodium hydroxide solution but insoluble in neutral water or sodium bicarbonate solution. Benzoic acid is soluble in both sodium hydroxide and sodium bicarbonate solutions. Use skeletal structures only...
Acid/Base Extraction ACID/BASE EXTRACTION Provide a flow chart detailing the acid/base extraction/separation of the compounds shown...
Acid/Base Extraction
ACID/BASE EXTRACTION Provide a flow chart detailing the acid/base extraction/separation of the compounds shown below. Your answer must employ the following reagents: methylene chloride, hydrochloric acid (1M & 6M), sodium hydroxide (1M & 6M), 10% sodium bicarbonate (aq). Clearly indicate the product(s) and layers formed following each step of your separation scheme. HINT: phenol is soluble in sodium hydroxide solution but insoluble in neutral water or sodium bicarbonate solution. Benzoic acid is soluble in both sodium hydroxide and...
Using aqueous HCl, NaHCO3, or NaOH, devise a flowchart separation scheme to separate the following two-component...
Using aqueous HCl, NaHCO3, or NaOH, devise a flowchart
separation scheme to separate the following two-component mixtures.
All the substances are soluble in ether. Be sure to indicate how
you would recover each of the compounds from its respective
salts.
4. Using aqueous hydrochloric acid, sodium bicarbonate, or sodium hydroxide solutions, devise a flow-chart separation scheme to separate the following two-component mixtures. All the substances are soluble in ether. Be sure to indicate how you would recover each of the...
1)-Briefly explain the role of the hydrochloric acid during the liquid-liquid extraction procedure. Draw the acid-base...
1)-Briefly explain the role of the hydrochloric acid during the liquid-liquid extraction procedure. Draw the acid-base reaction between lidocaine freebase and hydronium chloride to help your discussion and circle the organic species that is more soluble in water. 2)- Briefly explain the role of the potassium hydroxide during the liquid-liquid extraction procedure. Draw the acid-base reaction between lidocaine hydrochloride and potassium hydroxide to help your discussion and circle the organic species that is would be more soluble in the organic...
pre-laboratory Questions A 1 Explain why it is more efficient to make several extractions using small...
pre-laboratory Questions A 1 Explain why it is more efficient to make several extractions using small portions rather than one extraction using the same total volume. 2 Define the following terms: Drying agent intensity Drying agent capacity 3 Select the upper layer in each pair of mixed solvents (see Appendix C): Water and benzene Water and carbon tetrachloride Water and ether 4 Write an equation for the reaction of a benzoic acid with aqueous sodium bicarbonate. 5 Complete the following...
PART ONE: Sodium hydrogen carbonate NaHCO3, also known as sodium bicarbonate or "baking soda", can be...
PART ONE: Sodium hydrogen carbonate NaHCO3, also known as sodium bicarbonate or "baking soda", can be used to relieve acid indigestion. Acid indigestion is the burning sensation you get in your stomach when it contains too much hydrochloric acid HCl, which the stomach secretes to help digest food. Drinking a glass of water containing dissolved NaHCO3 neutralizes excess HCl through this reaction: HCl(aq)+NaHCO3(aq)→NaCl(aq)+H2O(l)+CO2(g) The CO2 gas produced is what makes you burp after drinking the solution. Suppose the fluid in...
PART ONE: Sodium hydrogen carbonate NaHCO3, also known as sodium bicarbonate or "baking soda", can be...
PART ONE: Sodium hydrogen carbonate NaHCO3, also known as sodium bicarbonate or "baking soda", can be used to relieve acid indigestion. Acid indigestion is the burning sensation you get in your stomach when it contains too much hydrochloric acid HCl, which the stomach secretes to help digest food. Drinking a glass of water containing dissolved NaHCO3 neutralizes excess HCl through this reaction: HCl(aq)+NaHCO3(aq)→NaCl(aq)+H2O(l)+CO2(g) The CO2 gas produced is what makes you burp after drinking the solution. Suppose the fluid in...
Extraction of solids: Experiment outlined below Draw a “roadmap” of the experiment, containing chemical structures and...
Extraction of solids: Experiment outlined below
Draw a “roadmap” of the experiment, containing chemical
structures and “layers” (organic and aqueous). This should contain
the individual reactions occurring in each step, and show which
layer the various components are present. Make sure you think about
whether the acetaminophen, caffeine and aspirin are neutral,
protonated or deprotonated.
Preliminary separation obtain a sample (1.0g) of the mixture. weigh the sample and record it. this sample should consist of a 2:1:1 mixture (by mass)...
Provide a flow chart detailing the acid/base extraction/separation of the compounds show below. Your answer must employ the following reagents: methylene chloride, hydrochloric acid (1M & 6M), sodium hydroxide (1M & 6M), 10% sodium bicarbonate (aq). Clearly indicate the product(s) and layers formed following each step of your separation scheme. IMPORTANT: p-cresol is soluble in sodium hydroxide solution but insoluble in neutral water or sodium bicarbonate solution. 2-ethylbenzoic acid is soluble in both sodium hydroxide and sodium bicarbonate solutions. Use...
Acid/Base Extraction
1. Provide a flow chart detailing the acid/base
extraction/separation of the compounds shown below. Your answer
must employ the following reagents: methylene chloride,
hydrochloric acid (1M & 6M), sodium hydroxide (1M & 6M),
10% sodium bicarbonate (aq). Clearly indicate the product(s) and
layers formed following each step of your separation scheme.
IMPORTANT: p-cresol is soluble in sodium hydroxide solution but
insoluble in neutral water or sodium bicarbonate solution. 2-
ethylbenzoic acid is soluble in both sodium hydroxide and...
Provide a flow chart detailing the acid/base extraction/separation of the compounds shown below. Your answer must employ the following reagents: methylene chloride, hydrochloric acid M 6M), sodium hydroxide (IM & 6M),10% sodium bicarbonate (aq Clearly indicate the product(s) and layers formedfollowing each step of your separation scheme. HINT: phenol is soluble in sodium hydroxide solution but insoluble in neutral water or sodium bicarbonate solution. Benzoic acid is soluble in both sodium hydroxide and sodium bicarbonate solutions. Use skeletal structures only...
Acid/Base Extraction
ACID/BASE EXTRACTION Provide a flow chart detailing the acid/base extraction/separation of the compounds shown below. Your answer must employ the following reagents: methylene chloride, hydrochloric acid (1M & 6M), sodium hydroxide (1M & 6M), 10% sodium bicarbonate (aq). Clearly indicate the product(s) and layers formed following each step of your separation scheme. HINT: phenol is soluble in sodium hydroxide solution but insoluble in neutral water or sodium bicarbonate solution. Benzoic acid is soluble in both sodium hydroxide and...
Using aqueous HCl, NaHCO3, or NaOH, devise a flowchart
separation scheme to separate the following two-component mixtures.
All the substances are soluble in ether. Be sure to indicate how
you would recover each of the compounds from its respective
salts.
4. Using aqueous hydrochloric acid, sodium bicarbonate, or sodium hydroxide solutions, devise a flow-chart separation scheme to separate the following two-component mixtures. All the substances are soluble in ether. Be sure to indicate how you would recover each of the...
Extraction of solids: Experiment outlined below
Draw a “roadmap” of the experiment, containing chemical
structures and “layers” (organic and aqueous). This should contain
the individual reactions occurring in each step, and show which
layer the various components are present. Make sure you think about
whether the acetaminophen, caffeine and aspirin are neutral,
protonated or deprotonated.
Preliminary separation obtain a sample (1.0g) of the mixture. weigh the sample and record it. this sample should consist of a 2:1:1 mixture (by mass)...
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