100 80- 60 40- 25 50 75 100 125 150 m/z
label peaks Butane MASS SPECTRUM 100 Molar mass- 58.12 q/mol 80 40 20 0.0 10 20 30 40 50 m/z IST Char:-. 60 60 Rel. Intensity
Identify 5 of the major peaks on each spectrum Liquid T MS 100 80 60 40- 20- M* 0 10 30 40 60 70 8 100 m/z
180 140 100 200 160 120 80 60 40 20 11 10 9 6 pm 7 3 2 ppm 100- 80- 60- 40- 20- 75 100 125 150 25 50 m/z Relative Intensity o Write all of your notes on the spectra Type a justification of each structure in the same order they appear in your stapled packet o Insert page breaks so each structure is on a separate page o Include page numbers o Type your name in the...
Check 200 180 160 120 80 60 40 20 0 140 a 100 ppm s, 3H t, 3 H d. 2 a. 2 H d. 2H s, 1 H 1 10 9 8 7 6 4 3 2 1 5 ppm 1) Which compound gives the following spectra? For the 'H-NMR assign all signals. Interpret mol peak and base peak in the mass spectrum if a mole peak exists. Assign at least two 13C signals, How does the IR spectrum...
Use given spectroscopy to give a structure of a molecule. 100 MS-NU-1560 80 40 20 50 75 100 125 i 150 m/z
MASS SPECTRUM 100 80- m/z 150 60 40 0.2 20. 00 1000 4500 2500 2000 150) 000 3500 3000 0.0+ 0.0 Wavenurbers (cm-1) on 160 40 120 13C NMR 2 peaks overlapping 100 20 40 120 60 80 PPM 140 6H H NMR 2H 2H 2H 1H 1H 2 7 5 8 PPM 1. Using the spectra on the next page, solve for the structure of an unknown organic compound. Fòi full credit (and consideration for partial credit) show your...
is is the mass spectrum of 2-pentanol. 100 MS-NW-8471 6 80 60 40 20 omt 10 20 30 40 60 70 80 50 m/z Provide a reasonable fragmentation pathway for the indicated fragments. Make sure that you discuss the relative intensity of the same fragments. | m/z 27.0 7.6 29.0 5.3 31.0 5.0 41.0 5.8 43.0 13.7 44.0 7.5 45.0 100.0 55.0 18.7 73.0 7.1
what are possible structures for each spectra 100 MS 80 - 60 Relative Intensity 40 20- 0 10 20 30 40 60 70 80 50 m/z 100- 80 Relative Intensity 40 20 0 10 15 20 25 30 35 40 50 55 60 65 70 75 80 45 m/z
40 20 20 -60 -80 -100 0.1 100 10 Frequency (radis) -50 -100 -150 200 250 -300 0.1 10 100 Frequency (rad/s) Phase (degrees) 20 log M O Pictuve UShg upon Bode Plot of KGIS) Closed lop syStem's chaactentic eguation is Des)= 1+KG(S) (4) uhg Magnitude Plot, Detamine the torm of Transfer fevction from slope of HigL fretueney, Slope t low freguency, Cut-aft fefuency an Sretch the Voot -locuS t(wro Miw) 20d8 Vampng atto =1) on a seand -order System)...