3. The melting point of unknown A was measured to be 110-120°C and unknown B was...
03) Based on what you know about solubility and recrystallization, which of the following solid/solvent combinations can be used for recrystallization? (5 pts) a) Naphthalene/water b) Urea/hexane c) Benzoic acid/ water d) All of the above 04) Which of the following is something you can NOT determine by looking at a TLC plate? (4 pts) a) Polarity b) Impurities c) Retardation factor d) Retention time
4. Based on what you know about solubility and recrystallization, which of the following solid/solvent combinations can be used for recrystallization? (5 pts) A. Naphthalene/ water B. Urea/hexane c. Benzoic acid/ water D. All of the above
Recrystallization: Percent error of melting point and how impurities affect melting point: Please explain both questions below: (Part A) During a recrystallization experiment, the literature melting point of a compound is 105-107 °C. The melting point temperature you obtain from your recrystallized compound is 103-105 °C. Which of the following would be the proper way to set up the percent error of your mp? (a) (104/106)*100 (b) [(106-104)/106] *100 (c) (107/105)*100 (d) [(107-105)/107] *100 (Part B) For a recrystallization experiment...
Please right an in depth discussion about part C. We we’re not able to get any recrystallization from our unknown. Talk about possible failures that could of happen that prevented us to not get any or our unknown to recrystallize. Thanks so much! Experiment 1: Solids: Recrystallization and Melting Point Learning Outcomes: Upon completion of this lab, students will be able to perform the technique of recrystallization of an impure solid as well as be able to determine an appropriate...
Question 14 The melting point of a pure compound is known to be 110-111º. Describe the melting behavior expected if this compound is contaminated with 5% of an impurity. 90-96 111-113 90-91 110-111 5 pts Question 15 You and your lab partner take melting points of the same sample. You observe a melting point of 101-107°C, while your partner observes a value of 110-112°C. Explain how you can get two different values with exactly the same sample. One of the...
Cinnamic acid and urea melt at 133°C. The melting point of an unknown is found to be 133°C. What experiments using melting range determinations could be done to determine if the unknown is cinnamic acid or urea?
PART B MELTING POINTS OF SOME ORGANIC SUBSTANCES Circle the pair of substances of which you measured the melting point range 7 2-naphthol (A) and naphthalene (B) benzophenone (A) and benzil (B Complete the following table: [6 marks] Hint Molecules containing only Cand H can be assumed to be non-polar Present in Present in А Stronger in which substance? Why? Intermolecular Force В (yes or no) (yes or no) London Dispersion Dipole-Dipole Hydrogen Bonding Which of the two substances that...
It is important that the melting point of the solid being recrystallized is above the boiling point of the recrystallization solvent to prevent oiling out! True False A pure solid sample will have a melting point range of approximately of 1 °C or less True False Question 20 8 pts Predict the positions where an electrophile is directed in the following substituted aromatic compounds. Fill in the table. (8 pts) Position(s) where electrophile is directed (eg. ortho, meta, para Seles...
What would you expect the observed boiling point to be at 10 torrs of a liquid which has a boiling point of 300 °C at 760 torrs? (Use Figure) Would it be possible to establish the composition of an unknown binary mixture of two substances from mixture melting-point data? Explain. After recording the R values using as a solvent system ethyl acetate and hexane (1:4), determine what solvent system is needed to obtain values between 0.3-0.4 for each of the...
30pts total) 1. Irwo known substances have the same melting point as an unknown substance that you obtained, how could you determine if either of the two known substances is your unknown compound? 2. You are given an impure mix of substances that contains a solid substance, Chemical X, that is soluble in ethanol at all temperatures. You know there is an insoluble impurity in the mix as well as a very soluble impurity, both in ethanol. Can you recrystallize...