We need at least 10 more requests to produce the answer.
0 / 10 have requested this problem solution
The more requests, the faster the answer.
Aldehyde: ZPA Ketone: BCK Amount of material started with: 2 mL of aldehyde and 0.5 mL...
Aldehyde: ZPA Ketone: BCK Amount of material started with: 2 mL of aldehyde and 0.5 mL of Ketone Recrystallized Mass: 1.53 g Melting Range: 196-200 C Recrystallization Solvent: 9:1 Ethanol/Acetone 1) structure of product 2)theoretical yield 3)isolated and percent yield 6.1724 7.6069 7.5891 Z-8, CDC13 Z-B, CDC13 7.2839 2724 7.6069 7.5891 4.061 7.0012 6.9836 7.2839 7.2 6.08.18 8862 7.0 4.0666 7.0012 6.9836 3.9987 -3.1154 Ippm] Ippm] component. The possible aldehydes are benzaldehyde, 4-methylbenzaldehyde (p-tolualdehyde), 4-methoxybenzaldehyde (p-anisaldehyde), and E-3-phenyl-2-propenal (cinnamaldehyde). The...
Aldehyde: ZPA Ketone: BCK Amount of material started with: 2 mL of aldehyde and 0.5 mL of Ketone Recrystallized Mass: 1.53 g Melting Range: 196-200 C Recrystallization Solvent: 9:1 Ethanol/Acetone Aldehydes ketones Cyclopentanone Cyclohexanone Acetone Benzaldehyde p-tolualdehyde p-anisaldehyde Cinnamaldehyde 113 °C 175 °C 129-130 C 144 °C 189 °C 235-236 °C 212 °C 225 °C 118°C 170 °C 159 °C 180°C 4-methyl cyclohexanone 98-99 °C 113-113.5 °C 141-142 °C 163-164 °C 6.1724 7.6069 7.5891 Z-8, CDC13 Z-B, CDC13 7.2839 2724...
Codes: Aldehyde: ZPA Ketone: BCK Amount of material started with: 2 mL of aldehyde and 0.5 mL of Ketone Recrystallized Mass: 1.53 g Melting Range: 196-200 C Recrystallization Solvent: 9:1 Ethanol/Acetone 6.1724 7.6069 7.5891 Z-8, CDC13 Z-B, CDC13 7.2839 2724 7.6069 7.5891 4.061 7.0012 6.9836 7.2839 7.2 6.08.18 8862 7.0 4.0666 7.0012 6.9836 3.9987 -3.1154 Ippm] Ippm] Aldehydes ketones Cyclopentanone Cyclohexanone Acetone Benzaldehyde p-tolualdehyde p-anisaldehyde Cinnamaldehyde 113 °C 175 °C 129-130 °C 144 °C 189 °C 235-236 °C 212 °C...
With the values of the possible products. 4) Discuss the IR spectra of your starting materials. Based on your spectra determine which unknown was the aldehyde and which was the ketone. You should discuss the key peaks you used to make these assignments. If your IR spectra were helpful in identifying which ketone or aldehyde you had, discuss this as well. For additional info, see the IR modes handout on the class web site. 5) Assign the peaks in the...