A solution possibly contains Ag+, Pb2+, Bi3+, Fe3+, Ba2+ and Na+. You are about to begin the separation of the group I cations but no HCl is available. Would the following reagents be an acceptable replacement for separation of the group I cations in this sample? To justify your choice as yes or no, write the NIE for all precipitates you expect to form. If only group I solids are precipitating, that will be a “yes” and if more than the group I solids precipitate, that will be a “no.”
a) HBr b) HC2H3O2 c) NaOH d) NaI
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A solution possibly contains Ag+, Pb2+, Bi3+, Fe3+, Ba2+ and Na+. You are about to begin...
2) You are presented with an unknown that possibly has Ag-, Bi-, Sn+, Zn2+, Co2+ and Na'. You divide the solution into three equal volumes, labeling one "A," one "B," and one "C." To "A" you add 6 M HCl and do not observe any precipitate forming. In tube B, you add 6 M HCl until the pH is 0.5 then add thioacetamide and heat the solution in a hot water bath for seven minutes, eventually observing a black precipitate....
Ex: Separation of Group 1 Cations (Pb+ and Ag+) 10 drops of unknown was place along with 6 drops of 6M HCl, centrifuge. 2 more drops of 6M HCl, centrifuge. Decant supernate, use precipitate and add 5 drops of cold water, centrifuge. Test for Pb2+ 15 drops of water to precipitate & put in hot water, centrifuge then decant supernate. repeat x2 Combine supernates and save precipitate for Ag+ analysis. Add 3 drops of 1M K2CrO4 to supernate. yellow precipitate...
I concluded that my unknown was Pb2+. since yellow
precipitate formed. can you help me answer the questions for the
Known and unknown report
Qualitative Analysis: Group I Cations 10 ORECTIVES A Leam some chemistry of Group I cations, R Analyze an unknown for Group I cations. THEORY AND DISCUSSION Group I cations are precipitated as insoluble chlorides: Ag, Pb, Hg2 +Cr-AgCl, PbCh, HgCla The colors of the following species will be helpful in the analysis for Group I cations....