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This is the H NMR spectrum for the product of a reaction between either benzaldehyde, 4-methybenzaldehyde,...
5) Assign the peaks in the 'H NMR spectrum of your product. Draw your structure on the NMR spectrum and label each set of inequivalent protons. Use these labels in assigning the peaks. In some cases the aromatic peaks may overlap, so it is OK to assign groups of protons to a series of overlapping peaks if necessary. Try to be as specific as possible in your assignment, though. Discuss in detail how the NMR spectrum is only consistent with...
Aldehyde: ZPA Ketone: BCK Amount of material started with: 2 mL of aldehyde and 0.5 mL of Ketone Recrystallized Mass: 1.53 g Melting Range: 196-200 C Recrystallization Solvent: 9:1 Ethanol/Acetone 1) structure of product 2)theoretical yield 3)isolated and percent yield 6.1724 7.6069 7.5891 Z-8, CDC13 Z-B, CDC13 7.2839 2724 7.6069 7.5891 4.061 7.0012 6.9836 7.2839 7.2 6.08.18 8862 7.0 4.0666 7.0012 6.9836 3.9987 -3.1154 Ippm] Ippm] component. The possible aldehydes are benzaldehyde, 4-methylbenzaldehyde (p-tolualdehyde), 4-methoxybenzaldehyde (p-anisaldehyde), and E-3-phenyl-2-propenal (cinnamaldehyde). The...
Codes: Aldehyde: ZPA Ketone: BCK Amount of material started with: 2 mL of aldehyde and 0.5 mL of Ketone Recrystallized Mass: 1.53 g Melting Range: 196-200 C Recrystallization Solvent: 9:1 Ethanol/Acetone 6.1724 7.6069 7.5891 Z-8, CDC13 Z-B, CDC13 7.2839 2724 7.6069 7.5891 4.061 7.0012 6.9836 7.2839 7.2 6.08.18 8862 7.0 4.0666 7.0012 6.9836 3.9987 -3.1154 Ippm] Ippm] Aldehydes ketones Cyclopentanone Cyclohexanone Acetone Benzaldehyde p-tolualdehyde p-anisaldehyde Cinnamaldehyde 113 °C 175 °C 129-130 °C 144 °C 189 °C 235-236 °C 212 °C...
With the values of the possible products. 4) Discuss the IR spectra of your starting materials. Based on your spectra determine which unknown was the aldehyde and which was the ketone. You should discuss the key peaks you used to make these assignments. If your IR spectra were helpful in identifying which ketone or aldehyde you had, discuss this as well. For additional info, see the IR modes handout on the class web site. 5) Assign the peaks in the...
Aldehyde: ZPA Ketone: BCK Amount of material started with: 2 mL of aldehyde and 0.5 mL of Ketone Recrystallized Mass: 1.53 g Melting Range: 196-200 C Recrystallization Solvent: 9:1 Ethanol/Acetone Aldehydes ketones Cyclopentanone Cyclohexanone Acetone Benzaldehyde p-tolualdehyde p-anisaldehyde Cinnamaldehyde 113 °C 175 °C 129-130 C 144 °C 189 °C 235-236 °C 212 °C 225 °C 118°C 170 °C 159 °C 180°C 4-methyl cyclohexanone 98-99 °C 113-113.5 °C 141-142 °C 163-164 °C 6.1724 7.6069 7.5891 Z-8, CDC13 Z-B, CDC13 7.2839 2724...
Aldehyde: ZPA Ketone: BCK Amount of material started with: 2 mL of aldehyde and 0.5 mL of Ketone Recrystallized Mass: 1.53 g Melting Range: 196-200 C Recrystallization Solvent: 9:1 Ethanol/Acetone please ans 1 and 2 (label ans). UNKNOWN KETONE IS CYCLOPENTAONE UNKOWN ALDEHYDE IS 4-methoxybenzaldehyde 4 457 05 1267 0 1278 49 LP 00051 BL000 BCK 6 PER 12 160 TESIS Ota TL 6201 11 ESTI 29 TEZE LT SELF 09 200 18 DIL 0 ore 1400 28 2004 25...
This experiment was based on Aldol-dehydration reaction using unknown aldehydes and ketones. We carried out an aldol condensation between an unknown aldehyde and an unknown ketone. Here are the list of possible unknown aldehydes and ketones that were used. Here is the NMR of the final product. Please predict the structure given the melting point is 163 degrees Celsius. The analysis of the 1H NMR spectrum should include a detailed assignment of each of the NMR resonances to the protons...