Could acetone be used instead of diethyl ether to dissolve an unknown mixture and perform the microscale separation via liquid/liquid extraction of your basic,acidic, and neutral components? Explain your answer.
the solubility of given solvent for an extraction depands on several of its properities,when compared to di ethyl ether, aceton is high volatile and higher boing point. dielectric constant, polarity and polarizability influence strongly the solvent-solvent and solute-solvent interactions. Another important chemical properity of a solvent is its basicity. compounds having functional groups containing electronagative atoms aceton is higher electonagativity these influence the sepsration.
In the unknown sample nature to extracted with aceton may be inert or active with respect to the compound to extracted, aceton may be inert or active with respect to to the unknown compound to be extracted,in the unknown components in compond interact with aceton frist basic componets are separated, next to be neutral components, then followed by acidic components of the un known compounds. becouse acetone is acidic nature.
Could acetone be used instead of diethyl ether to dissolve an unknown mixture and perform the...
1. will a Grignard reagent be formed if acetone is used as solvent instead of diethyl ether. (reaction of bromobenzene with magnesium) 2. what is the product if reacting benzaldehyde with the Grignard reagent from Q1 in acetone?
if
in project 7.1, 100% ethanol was used as the reaction solvent
instead of diethyl ether, what would the product(s) of the reaction
be? be sure to explain the formation of your predicted products.
2. If in Project 7.1, 100% ethanol was used as the reaction solvent instead of diethyl ether, what would the product(s) of the reaction be? Be sure to explain the formation of your predicted products. MgBr HOCH CH3
a. How does diethyl ether stabilize the Grignard reaction? b. Could dimethylether be used instead? Why or why not?
3. A crude nonacidic product mixture dissolved in diethyl ether contains acetic acid. Describe an extraction procedure that could be used to remove the acetic acid. b. When the two layers form during an ether/water extraction, what would be an easy, convenient way to tell which layer is which if the densities were not available.
An unknown mixture (dissolved in diethyl ether) contains only 2 of the following : benzoic acid, phenol, aniline and napthalene. You use the acid-base extraction method and want to identify the 2 compounds in your original mixture. 1) To separate the organic acid you add NaOH and to separate the organic base you add HCl.In both cases these extractions are followed by extractions with water. Why do we add water? Why is this step important? (A clear explanation please). 2)When...
Extraction Q1. Why doesn’t the neutral organic compound dissolve in the 1.5 M NaOH solution? Q2. Why is diethyl ether a good choice for the organic solvent in this extraction experiment? Q3. What experimental difficulty would you encounter if you neglected to include the drying step before evaporating the ether solution of the neutral organic compound? Q4. Why are the two organic compounds recrystallized before their melting points are determined? Q5. What IR bands are most useful in distinguishing a...
From You have a mixture of benzoic acid, hexamethylenediamine, and 1-octanol dissolved in diethyl ether. You wish (for some reason) to separate these compounds and have pure samples of each. Devise a liquid-liquid extraction protocol that would allow you to do this. (up to 20 points) Your answer should be clear and concise. Ambiguous answers or those that are difficult to read will NOT receive points. Search entries or author Unread Subscribe Reply
1)When you perform a liquid-liquid extraction using a separatory funnel, which of the following organic solvent is on the bottom of the aqueous phase and which is on top? (write your answer by the solvent name) a) Ethyl acetate b) hexane c) Dichloromethane d) diethyl ether 2) If you are performing a liquid-liquid extraction and you have a mix of a carboxylic acid and a non-acidic compound, which combination of solvents would you use for the separation? a) dichloromethane/HCI b)...
The goal of this experiment is to separate a mixture of two unknown compounds into individual Components and to identify the compounds. Answer the questions below. More than one answer may be possible. Why do we need to be especially careful when working with diethyl ether? Fumes can cause drowsiness & dizziness, and in high concentration, loss of consciousness Because it is highly acidic and can burn the skin Because it is extremely volatile and flammable. Of all of the...
Provide a flow chart detailing the acid/base extraction/separation of the compounds show below. Your answer must employ the following reagents: methylene chloride, hydrochloric acid (1M & 6M), sodium hydroxide (1M & 6M), 10% sodium bicarbonate (aq). Clearly indicate the product(s) and layers formed following each step of your separation scheme. IMPORTANT: p-cresol is soluble in sodium hydroxide solution but insoluble in neutral water or sodium bicarbonate solution. 2-ethylbenzoic acid is soluble in both sodium hydroxide and sodium bicarbonate solutions. Use...