From You have a mixture of benzoic acid, hexamethylenediamine, and 1-octanol dissolved in diethyl ether. You...
An unknown mixture (dissolved in diethyl ether) contains only 2 of the following : benzoic acid, phenol, aniline and napthalene. You use the acid-base extraction method and want to identify the 2 compounds in your original mixture. 1) To separate the organic acid you add NaOH and to separate the organic base you add HCl.In both cases these extractions are followed by extractions with water. Why do we add water? Why is this step important? (A clear explanation please). 2)When...
3. A crude nonacidic product mixture dissolved in diethyl ether contains acetic acid. Describe an extraction procedure that could be used to remove the acetic acid. b. When the two layers form during an ether/water extraction, what would be an easy, convenient way to tell which layer is which if the densities were not available.
4. A mixture of dodecano ic acid and dodecan - 1 -ol is dissolved in diethyl ether. Suggest a procedure for separating the two compounds. (1 point)
Started dissolving mixture with diethyl ether. And shook 3M HCL in sep funnel. Collected. Now: 1) You added NaOH to organic phase collected in problem 2 to extract another compound, Which compound was extracted in NaOH solution? Justify with chemical equation 2) to the aqueous phase you added HCL solution until it’s ph was less than 7. What happens if it’s ph is 7 or above? 3) when you acidified the solution by adding HCL, a white precipitate was produced....
Given a mixture of KI, benzoic acid, naphthalene, and 1-adamantanamine, how would you separate them into individual components using liquid-liquid extraction? Use a flow chart to explain the process.
You have a separatory funnel that contains a solution of 4-methyl benzoic acid and ethoxybenzene in methylene chloride. By adding KOH (aq) into this solution for extraction, what compound(s) would be expected to form in the aqueous layer? Write the equation. Compound X has a hexane/water distribution coefficient of 2.0. (a) Does compound X have a higher or lower solubility in hexane comparing to water? (b) How much of a 3.0 g sample of compound X dissolved in 100 ml...
You will apply what you have learned earlier in the semester when performing the Acid-Base Extraction experiment to perform a different separation: that of an organic neutral compound and organic base. You will also need to purify and characterize these compounds. You will have one lab period to execute your plan for separating the assigned mixture given below. There will be a 1:1 (by mass) mixture placed in the lab: 1,4-dichlorobenzene/ethyl 4-aminobenzoate. You will take approximately 1 g of your...
Separating a Mixture, Recrystallization, pre-lab assignment could you also explain why you chose that substance for the empty spaces and question marks EXPERIMENT 4 Pre-Lab Assignment Separating a Mixture, Recrystalliration Name Date 1. Complete the following flowchart which shows how to separate a mixture of sand, sodium chloride and acetanilide. Notice that after a separation process (a down arrow) the filtered solids are shown on the left and the filtrate (the liquid) is shown on the right. The terminal step...
i need help with the postlab questions please Grignard reagent THE GRIGNARD REAGENT-PREPARATION AND REACTION In this experiment, you will prepare a Grignard reagent, phenyl magnesium bromide, from bromobenzene and magnesium metal. The Grignard reagent will then react with methyl benzoate to form triphenylmethanol. Introduction Grignard reagents, such as organomagnesium halides, were discovered in 1910 by French chemist Victor Grignard. The Grignard reaction is one of the most general methods for carbon- carbon bond formation in all of organic chemistry....
Part A 1. If you had used more methylene chloride in each step, you could have extracted more caffeine. Explain why you did not. Hint - What step would have taken longer (Hint: not drying). PART A Mass of Beaker & Caffeine Mass of Beaker 167.750g 67.6809 Mass of Caffeine 0.0 75 Calculations. Show your work and circle the answers. Mass of caffeine recovered: 012919 b) Actual:.07 % caffeine recovered: a) Predicted: 9 7:213% b) Actual: 92.105% PART B Unknown...