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Phenyl Acetate or Methyl Benzoate "C227 Baeyer-Villiger Reaction" 2 1.0000 0.4998 U.98.39 - M 7.4235 -...
NMR Data: Attach 1H NMR spectrum; draw the Lewis structure and an acceptable name of the...
NMR Data: Attach 1H NMR spectrum; draw the Lewis structure and an acceptable name of the identified compound on the spectrum. Show all bonds to the hydrogens. Label the different sets of hydrogens (i.e. Ha. Hy, H1, H2, etc.). Create a table that summarizes the chemical shift, integration, multiplicity, the proton assignment, and justification of each signal. Phenyl Acetate or Methyl Benzoate "C227 Baeyer-Villiger Reaction" 2 1.0000 0.4998 U.98.39 - M 7.4235 - M 7.2793 - M 7.1626 1 "C:\CHEM...
Baeyer Villiger Can someone explain the GCMS of this sample? This was the procedure: A solution...
Baeyer Villiger
Can someone explain the GCMS of this sample?
This was the procedure:
A solution of acetophenone, 20 mmoles, and
metha-chloroperbenzoic acid (mCPBA)
36mmoles, are stirred in 50mL of distilled water at 80°C for 4 h
and monitored by
TLC (eluent: ethyl acetate). The reaction mixture is cooled to
room temperature and
extracted with dichloromethane (3x30mL). The combined organic
layers are
washed with saturated NaHCO3, and NaCl brine solution. The
solution is then dried
with MgSO4 and the solvent...
I need help with questions 5, 6, & 7. The FTIR and NMR is provided. I...
I need help with questions 5,
6, & 7. The FTIR and NMR is provided. I also need help creating
a reaction mechanism using the following:
Starting material: methyl acetate.
Solvent: diethyl ether
Reagent: sodium methoxide
Product: methyl acetoacetate
THANK YOU!!!!!
11-8: Claisen Condensation - 1 For this assignment, the target compound that you should synthesize is methyl acetoacetate.This is another carbonyl addition variation. Examine the product and determine which ester is the nucleophile and which is the electrophile. Keep...
Only need help with 5,6,7 and mechanism FTIR and NMR Spectra After completing a reaction and...
Only need help with 5,6,7
and mechanism
FTIR and NMR Spectra After completing a reaction and working up the products, it is still necessary to confirm that the correct product was formed. The most common tools used for this analysis are Fourier Transform Infrared (FTIR) and Nuclear Magnetic Resonance (NMR) spectroscopy. In the virtual laboratory, 'H and C NMR spectra are available. Details on interpreting FTIR and NMR spectra are found in your textbook. Your instructor may or may not...
NMR Data: Attach 1H NMR spectrum; draw the Lewis structure and an acceptable name of the identified compound on the spectrum. Show all bonds to the hydrogens. Label the different sets of hydrogens (i.e. Ha. Hy, H1, H2, etc.). Create a table that summarizes the chemical shift, integration, multiplicity, the proton assignment, and justification of each signal. Phenyl Acetate or Methyl Benzoate "C227 Baeyer-Villiger Reaction" 2 1.0000 0.4998 U.98.39 - M 7.4235 - M 7.2793 - M 7.1626 1 "C:\CHEM...
Baeyer Villiger
Can someone explain the GCMS of this sample?
This was the procedure:
A solution of acetophenone, 20 mmoles, and
metha-chloroperbenzoic acid (mCPBA)
36mmoles, are stirred in 50mL of distilled water at 80°C for 4 h
and monitored by
TLC (eluent: ethyl acetate). The reaction mixture is cooled to
room temperature and
extracted with dichloromethane (3x30mL). The combined organic
layers are
washed with saturated NaHCO3, and NaCl brine solution. The
solution is then dried
with MgSO4 and the solvent...
I need help with questions 5,
6, & 7. The FTIR and NMR is provided. I also need help creating
a reaction mechanism using the following:
Starting material: methyl acetate.
Solvent: diethyl ether
Reagent: sodium methoxide
Product: methyl acetoacetate
THANK YOU!!!!!
11-8: Claisen Condensation - 1 For this assignment, the target compound that you should synthesize is methyl acetoacetate.This is another carbonyl addition variation. Examine the product and determine which ester is the nucleophile and which is the electrophile. Keep...
Only need help with 5,6,7
and mechanism
FTIR and NMR Spectra After completing a reaction and working up the products, it is still necessary to confirm that the correct product was formed. The most common tools used for this analysis are Fourier Transform Infrared (FTIR) and Nuclear Magnetic Resonance (NMR) spectroscopy. In the virtual laboratory, 'H and C NMR spectra are available. Details on interpreting FTIR and NMR spectra are found in your textbook. Your instructor may or may not...
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