I need #2 answered Spectroscopy Problem Set15pts CHEM220B Spring 2019 1. Unknown number 44 SU 2....
I am not understanding this assignment at all. Any assistance is very much appreciated. Mass Spectrum: Molecular Ion m/z value and structure of the Molecular Ion. Base Peak m/z value and structure of that ion One other significant peak m/z value and structure of that ion C13 NMR Spectrum-- Draw Structure of Compound on the C13 NMR spectrum and identify each signal with the appropriate Carbon. Proton NMR Spectrum-- Draw Structure of Compound on the Proton NMR spectrum and identify...
Unknown H415 100 50 1000 1S00 2000 3000 BRVENUMBERI 4000 Unknown H415 ЗН 1 H-N 2H, q 1H, d 5H, m 1H, d 0 1 2 3 6 7 8 10 11 ppm HSP-00-049 Unknown H415 q 140 120 100 200 180 160 ppm CDS-00-726 20 -40 60 80 Relative Intensity 09 Unknown H415 100 MS-NJ-0442 80 20 thmpt 25 50 75 100 125 150 175 m/z Date: Name: Section/Group: Instructor: Report Sheet: Laboratory 14 MS,IR, 13C NMR, and 'H...
SPECTROSCOPY PROBLEM SET (Homework Assignment 2) [2 pts] Due November 18, 2019 Score: Name: 1. Propose a structure for a hydrocarbon whose mass spectrum shows a parention at m/z 100, a base peak at m/z 43 which gave the following 'H NMR spectrum. PPM 2. Propose a structure for a molecule whose mass spectrum shows a parent ion at m/z 86 with a base peak at m/z 29, an IR peak at 1720 cm' and which gave the following 'H...
For problems 11-12 answer the questions on the Mass Spectroscopy problem set worksheet. Problem 11 Problem (z m that IR Spectrum liquid film IR Spectrum oldim 4000 3000 2000 1600 1200 800 4000 3000 2000 V (cm 1800 ) 1200 800 Vom) 0.0 100F Mass Spectrum Mass Spectrum of base peak No significant UV absorption above 220 mm of base 107/109 1015486162 UV spectrum 530 mg/10mis path length: 100 cm solvencyclohexane 120 40 80 120 160 m/e 200 240 280...
2. The H NMR spectrum of an unknown compound with the molecular formula CgH902 is provided below. The IR spectrum for this compound shows a large, broad peak at 3147 cm ? and a strong, sharp peak at 1645 cm-7. Provide a structure for this unknown. 2H 2H 10 98 HSP-06-318 ppm
The m/z of the M+ peak of an unknown is 146, and this peak is the base peak (i.e., the tallest peak). (See below mass spectrum of the unknown.) Combustion analysis data indicate 49.03% carbon and 2.74% hydrogen. The IR spectrum and 13C-NMR spectrum of this compound also were obtained and are shown below. Given this information, what is the name of this unknown molecule? MASS SPECTRUM 100 80 60 面 40 20 0.0 120 160 40 80 0.0 m/z...
Which types of bonds can be identified in the IR spectrum of Molecule A? I Select] By identifying the molecular ion, determine which composition is consistent with the mass spectrum of A. I Select ] How many hydrogen environments are there in Molecule A? ISelect ] The peak at 2.1 ppm in the 1H NMR spectrum of Molecule A is most likely to be a: ISelect ] The peak at 3.1 ppm in the 1H NMR spectrum of Molecule A...
Spectroscopic Analysis Unknown 1: Molecule Number a) Determine the empirical formula from the microanalysis data, showing your working: Empirical Formula b) Does the mass spectrum imply the molecular formula is the same as the empirical formula? Why/Why not? Molecular Formula c) Use the 'double bond equivalents' formula to determine the degree on unsaturation for this molecule: d) What structural information can you garner from the IR spectrum? e) What structural information can you garner from the 'H NMR spectrum? Specify...
Spectroscopic Analysis Unknown 1: Molecule Number a) Determine the empirical formula from the microanalysis data, showing your working: Empirical Formula b) Does the mass spectrum imply the molecular formula is the same as the empirical formula? Why/Why not? Molecular Formula c) Use the 'double bond equivalents' formula to determine the degree on unsaturation for this molecule: d) What structural information can you garner from the IR spectrum? e) What structural information can you garner from the 'H NMR spectrum? Specify...
The low-resolution mass spectrum of an unknown monosubstituted benzene showed a molecular ion (M+) peak at m/z 150. Combustion analysis of a sample of this compound indicated that the compound contained C, H, and O only and had an empirical formula of C3H1002. The IR spectrum of the unknown compound is shown below. The 'H NMR spectrum of the unknown compound did not show a peak in the 9.10 ppm range. D 4000 9000 2000 1500 1000 RAVENUGERII What is...