The term “column bleeding” refers to: _______________. A) leak of carrier gas from the column. B)...
The term “column bleeding” refers to: _______________.
A) leak of carrier gas from the column.
B) poor resolution of low volatility compounds.
C) stationary phase decomposition.
D) decomposition of analytes on the column.
E) stationary phase contamination.
Homework Answers
Column bleeding results from thermal breakdown of the stationary phase at temperatures close to the upper temperature limit of the column. Hence (C) Stationary Phase Decomposition, is the correct option.
Add Answer to:
The term “column bleeding” refers to: _______________.
A) leak of carrier gas from the column.
B)...
As you increase the gas chromatography column temperature, analytes’ ______________ increases and stationary phase solubility _______________....
As you increase the gas chromatography column temperature, analytes’ ______________ increases and stationary phase solubility _______________. A) boiling point; increases B) vapor pressure; decreases C) vapor pressure; increases D) retention time; increases E) retention time; decreases
1. Select an appropriate type of column for separating these steroids and give the rationale for...
1. Select an appropriate type of column for separating these steroids and give the rationale for your selection. HO HO ОН OH Prednisolone Prednisone 2. You are using a C18 Reverse Phase column and the parameters shown below to separate Acetaminophen, Caffeine, and Benzoic Acid. You observe three peaks in your chromatogram (Huzzah!). Which corresponds to which compound? Explain the rationale behind your assignment. OH C18 REVERSED PHASE COLUMN Acetaminophen HC N H, O Caffeine Column: Legacy L1 Size: 4.6...
PRELABORATORY ASSIGNMENT 1. Provide the key term that corresponds to each of the following definitions. (a)...
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Put the analytes in order of increasing hydrophobicity. Which of the compounds is most hydrophilic? Which...
Put the analytes in order of increasing hydrophobicity. Which of
the compounds is most hydrophilic? Which is most hydrophobic? What
is the predicted elution order from a reverse phase chromatography
column?
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A group of analysts was working on developing a method to separate and determine carbamate insecticides...
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Chromatography Basics Multiple Choice: Answer the following multiple choice questions about Chromatography Basics (SHOW WORKING): 1) In...
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Which of the following statements holds true for the term, community wage level? a. It refers...
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question #2 please Reverse phase chromatography is the most common type of liquid chromatography which the...
question #2 please
Reverse phase chromatography is the most common type of liquid chromatography which the solid phase is made up of a packing material that is largely hydrophobic and the eluents are of varying polarities. In general, the more polar compounds elute first from the column followed by more hydrophobic compounds. PRELAB QUESTIONS 1. Draw structures for the following analytes for the simulation: a. acetophenone b. benzophenone c. butylparaben d. propiopheneone e. ethylparaben f. propylparaben g. ketoprofen h. 3-nitrophenol...
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1. Select an appropriate type of column for separating these steroids and give the rationale for your selection. HO HO ОН OH Prednisolone Prednisone 2. You are using a C18 Reverse Phase column and the parameters shown below to separate Acetaminophen, Caffeine, and Benzoic Acid. You observe three peaks in your chromatogram (Huzzah!). Which corresponds to which compound? Explain the rationale behind your assignment. OH C18 REVERSED PHASE COLUMN Acetaminophen HC N H, O Caffeine Column: Legacy L1 Size: 4.6...
PRELABORATORY ASSIGNMENT 1. Provide the key term that corresponds to each of the following definitions. (a) the study of compounds derived from plants and animals (b) a method for separating a mixture into its components as a result of a varying attraction of compounds for a mobile solvent on a stationary solid (c) the leading edge of the solvent, which travels from the bottom of the developing chamber to the upper portion of the chromatogram (d) refers to solvent that...
Put the analytes in order of increasing hydrophobicity. Which of
the compounds is most hydrophilic? Which is most hydrophobic? What
is the predicted elution order from a reverse phase chromatography
column?
a. acetophenone b. benzophenone c. butylparaben d. propiopheneone e. ethylparaben f. propylparaben g. ketoprofen h. 3-nitrophenol i. 4-nitrophenol 2. Put the analytes in order of increasing hydrophobicity. Which of the compounds is most hydrophilic? Which is most hydrophobic? What is the predicted elution order from a reverse phase chromatography...
question #2 please
Reverse phase chromatography is the most common type of liquid chromatography which the solid phase is made up of a packing material that is largely hydrophobic and the eluents are of varying polarities. In general, the more polar compounds elute first from the column followed by more hydrophobic compounds. PRELAB QUESTIONS 1. Draw structures for the following analytes for the simulation: a. acetophenone b. benzophenone c. butylparaben d. propiopheneone e. ethylparaben f. propylparaben g. ketoprofen h. 3-nitrophenol...
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