Homework Answers
Option D is correct.
A = tolmetin
B= Phenacetin
C = nambutone
Less polar is acetophenone .
Then more polar is amide.
Most polar is acid.
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2. A silica gel TLC plate developed with 5% acetic acid in ethyl acetate is depicted...
4. Consider the following silica gel TLC plac or compounds A, B, and hexines: developed in...
4. Consider the following silica gel TLC plac or compounds A, B, and hexines: developed in Fo-o- og a) Determine the Rr values of compounds A, B, and C run on a silica gel TLC plate using hexanes as the solvent b) Which compound, A, B, or C. is the most polar? values if you used acetone instead c) What would you expect to happen to the of hexanes as the eluting solvent? 5) Consider a sample that is a...
TLC Consider the following silica gel TLC plate of compounds A, B, and developed in hexanes:...
TLC Consider the following silica gel TLC plate of compounds A, B, and developed in hexanes: solvent front 0 D origin A B C 22. Determine the Ry values of compounds A, B, and Crun on a silica gel TLC plate using hexanes as the solvent. 23. Which compound, A, B, or C, is the most polar? 24. What would you expect to happen to the Ry values if you used acetone instead of hexanes as the eluting solvent? 25.TLC...
A TLC plate was run in 1:1 ethyl acetate and hexane, but when developed the plate...
A TLC plate was run in 1:1 ethyl acetate and hexane, but when developed the plate only showed baseline spots. What change could be made to get the spot(s) to move further up the plate? -Spot a new plate and run again in the same solvent system -Spot a new plate and run in neat hexane -Spot a new plate and run in 1:2 ethyl acetate/hexane -Spot a new plate and run in 2:1 ethyl acetate/hexane
6. Silica gel was used as the solid support for the TLC plate. Which of the...
6. Silica gel was used as the solid support for the TLC plate.
Which of the three compounds (A, B, or C) in the APPLIED MIXTURE is
the least polar? (See the figure attached.)
8. Which compound below will have the highest Rf on a TLC
plate? Explain your reasoning. (See figure attached.)
10. The following TLC plates have been spotted with two
different compounds and are about to be eluted. For each plate,
explain if it has been spotted...
A silica gel TLC plate was spotted using compounds A-D and developed in hexane. Spot “B”...
A silica gel TLC plate was spotted using compounds A-D and developed in hexane. Spot “B” traveled a distance of 2.0 cm from the solvent front at 4.0 cm, which of the following is a correct way to calculate its Rf value? Spot Distance traveled (cm) A 0.50 B 2.0 C 3.0 D 1.0 Spot B Rfis 4.0 cm/0.20 cm = 2.0 Spot B Rf is 4.0 cm/(4*2.0 cm) = 0.50 Spot B Rfis 2.0 cm/4.0 cm = 0.50 Spot...
Please help 2. Consider the TLC plate shown below that was done on silica gel using...
Please help
2. Consider the TLC plate shown below that was done on silica gel using a solvent mixture of 4:1 hexane/EtoAc as the eluent. 4:1 Hexane:EtOAC marked solvent front Spot B Spot A A origin (a) Which of the two organic compounds labeled A and B is less polar? (b) Calculate the Rf value of compound B. (c) How would the following changes affect the Rf values of A and B? i. Change to a more polar solvent mixture...
Question 9 1 pts Considering the silica gel TLC plate shown, which compound is the most...
Question 9 1 pts Considering the silica gel TLC plate shown, which compound is the most polar (the solvent front is at 4.0 cm)? Spot Distance traveled (cm) A 0.50 В 2.0 IC 3.0 D 1.0 O Compound B (spot B) Compound A (spot A) O Compound D (spot D) O Compound C (spot C)
Which of the following compounds would you expect to have the lowest Rf value on a...
Which of the following compounds would you expect to have the lowest Rf value on a silica gel TLC plate developed with dichloromethane? O A. Naphthalene O B. Phenyl acetate OC Butyric acid QUESTION 3 Which of the following compounds would you expect to have the highest Rf value on a silica gel TLC plate developed with dichloromethane? O A 2-octanone O B. Acetic acid C. 1-butanol OD. decane E. acetaldehyde
Possible Quiz Questions 1 What two methods of visualizing spots on a TLC plate will you...
Possible Quiz Questions 1 What two methods of visualizing spots on a TLC plate will you use in this Give two reasons why would you predict that the elution solvents (hexanes or acetate) would not be visible under UV visualization? week's lab? ethyl 2. Define R 3. Calculate the R of the spot on the following TLC plate. 4. Which compound in each pair is predicted to have the higher Ri? a. CH3CH2CH2CH2OH and CH3CH2CH2CH28r b. CH3CH2CH2CH2OH and CH3CH2CH2CH2CH2CH2CH3 c....
2. A solution containing a mixture of naphthalene, benzoic acid, and benzaldehyde is analyzed via TLC...
2. A solution containing a mixture of naphthalene, benzoic acid, and benzaldehyde is analyzed via TLC and GC. Use the structures and properties of the compounds to aid in answering the following questions. A. In the TLC experiment, the mixture is spotted on a silica TLC plate and eluted with a 1:1 mixture of hexanes and ethyl acetate. Three spots are observed on the plate, with Re values of 0.25, 0.58, and 0.74. Indicate which spot corresponds to which compound....
4. Consider the following silica gel TLC plac or compounds A, B, and hexines: developed in Fo-o- og a) Determine the Rr values of compounds A, B, and C run on a silica gel TLC plate using hexanes as the solvent b) Which compound, A, B, or C. is the most polar? values if you used acetone instead c) What would you expect to happen to the of hexanes as the eluting solvent? 5) Consider a sample that is a...
TLC Consider the following silica gel TLC plate of compounds A, B, and developed in hexanes: solvent front 0 D origin A B C 22. Determine the Ry values of compounds A, B, and Crun on a silica gel TLC plate using hexanes as the solvent. 23. Which compound, A, B, or C, is the most polar? 24. What would you expect to happen to the Ry values if you used acetone instead of hexanes as the eluting solvent? 25.TLC...
6. Silica gel was used as the solid support for the TLC plate.
Which of the three compounds (A, B, or C) in the APPLIED MIXTURE is
the least polar? (See the figure attached.)
8. Which compound below will have the highest Rf on a TLC
plate? Explain your reasoning. (See figure attached.)
10. The following TLC plates have been spotted with two
different compounds and are about to be eluted. For each plate,
explain if it has been spotted...
A silica gel TLC plate was spotted using compounds A-D and developed in hexane. Spot “B” traveled a distance of 2.0 cm from the solvent front at 4.0 cm, which of the following is a correct way to calculate its Rf value? Spot Distance traveled (cm) A 0.50 B 2.0 C 3.0 D 1.0 Spot B Rfis 4.0 cm/0.20 cm = 2.0 Spot B Rf is 4.0 cm/(4*2.0 cm) = 0.50 Spot B Rfis 2.0 cm/4.0 cm = 0.50 Spot...
Please help
2. Consider the TLC plate shown below that was done on silica gel using a solvent mixture of 4:1 hexane/EtoAc as the eluent. 4:1 Hexane:EtOAC marked solvent front Spot B Spot A A origin (a) Which of the two organic compounds labeled A and B is less polar? (b) Calculate the Rf value of compound B. (c) How would the following changes affect the Rf values of A and B? i. Change to a more polar solvent mixture...
Question 9 1 pts Considering the silica gel TLC plate shown, which compound is the most polar (the solvent front is at 4.0 cm)? Spot Distance traveled (cm) A 0.50 В 2.0 IC 3.0 D 1.0 O Compound B (spot B) Compound A (spot A) O Compound D (spot D) O Compound C (spot C)
Which of the following compounds would you expect to have the lowest Rf value on a silica gel TLC plate developed with dichloromethane? O A. Naphthalene O B. Phenyl acetate OC Butyric acid QUESTION 3 Which of the following compounds would you expect to have the highest Rf value on a silica gel TLC plate developed with dichloromethane? O A 2-octanone O B. Acetic acid C. 1-butanol OD. decane E. acetaldehyde
Possible Quiz Questions 1 What two methods of visualizing spots on a TLC plate will you use in this Give two reasons why would you predict that the elution solvents (hexanes or acetate) would not be visible under UV visualization? week's lab? ethyl 2. Define R 3. Calculate the R of the spot on the following TLC plate. 4. Which compound in each pair is predicted to have the higher Ri? a. CH3CH2CH2CH2OH and CH3CH2CH2CH28r b. CH3CH2CH2CH2OH and CH3CH2CH2CH2CH2CH2CH3 c....
2. A solution containing a mixture of naphthalene, benzoic acid, and benzaldehyde is analyzed via TLC and GC. Use the structures and properties of the compounds to aid in answering the following questions. A. In the TLC experiment, the mixture is spotted on a silica TLC plate and eluted with a 1:1 mixture of hexanes and ethyl acetate. Three spots are observed on the plate, with Re values of 0.25, 0.58, and 0.74. Indicate which spot corresponds to which compound....
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