Question
can you please answer all

1. When you run a TLC of the reaction in ethyl acetate : hexanes :: 1:1, the plate below is produced. Give a solvent system t
0 0
Add a comment Improve this question Transcribed image text
Answer #1

Date: - Page: -- An(D) 4 solvente systeryETOAC i Hexent -lit - Dear students as you all know TLC made of silra which is polarDato: Page: Ans @ =xa 7:7 R2 spot R2_s mall_poleiras compared to sport Ry because with silice is potur se more tightly bent pis

Add a comment
Know the answer?
Add Answer to:
can you please answer all 1. When you run a TLC of the reaction in ethyl...
Your Answer:

Post as a guest

Your Name:

What's your source?

Earn Coins

Coins can be redeemed for fabulous gifts.

Not the answer you're looking for? Ask your own homework help question. Our experts will answer your question WITHIN MINUTES for Free.
Similar Homework Help Questions
  • can you please answer all 1. When you run a TLC of the reaction in ethyl...

    can you please answer all 1. When you run a TLC of the reaction in ethyl acetate : hexanes 1:1, the plate below is produced. Give a solvent system that would be expected to produce greater separation and a BRIEF (8 words) justification about your choice. (5 points) 7 6 5 4 3 b. Calculate the R for the bottom spot. (5 points) c. Which compound on the TLC plate is the most polar? (5 points) 2. Why is it...

  • A TLC plate was run in 1:1 ethyl acetate and hexane, but when developed the plate...

    A TLC plate was run in 1:1 ethyl acetate and hexane, but when developed the plate only showed baseline spots. What change could be made to get the spot(s) to move further up the plate? -Spot a new plate and run again in the same solvent system -Spot a new plate and run in neat hexane -Spot a new plate and run in 1:2 ethyl acetate/hexane -Spot a new plate and run in 2:1 ethyl acetate/hexane

  • If aspirin (acetylsalicylic acid) is used in a TLC experiment with 1:1 Hexanes / Ethyl acetate...

    If aspirin (acetylsalicylic acid) is used in a TLC experiment with 1:1 Hexanes / Ethyl acetate as the solvent system, explain in terms of polarity why the spot would move fast or slow up the TLC plate?

  • d. The following TLC plate was run with a mobile phase that consisted of 5% Ethyl...

    d. The following TLC plate was run with a mobile phase that consisted of 5% Ethyl Acetate:95% Hexanes. Explain the result and describe what change to the mobile phase you would make to correct the issue. Solvent Fruct Speed Compound Line of One

  • Common solvents used in TLC analysis are hexane and ethyl acetate, the latter being more polar. A TLC has been performed...

    Common solvents used in TLC analysis are hexane and ethyl acetate, the latter being more polar. A TLC has been performed on a mixture of two compounds. The solvent ran for 3 cm(plate length is 6cm) with 5% ethyl acetate in hexane. The two spots were not resolved, meaning they showed up too close to each other. What can you suggest to possible improve the results of the separation?

  • 4. Consider the following silica gel TLC plac or compounds A, B, and hexines: developed in...

    4. Consider the following silica gel TLC plac or compounds A, B, and hexines: developed in Fo-o- og a) Determine the Rr values of compounds A, B, and C run on a silica gel TLC plate using hexanes as the solvent b) Which compound, A, B, or C. is the most polar? values if you used acetone instead c) What would you expect to happen to the of hexanes as the eluting solvent? 5) Consider a sample that is a...

  • Possible Quiz Questions 1 What two methods of visualizing spots on a TLC plate will you...

    Possible Quiz Questions 1 What two methods of visualizing spots on a TLC plate will you use in this Give two reasons why would you predict that the elution solvents (hexanes or acetate) would not be visible under UV visualization? week's lab? ethyl 2. Define R 3. Calculate the R of the spot on the following TLC plate. 4. Which compound in each pair is predicted to have the higher Ri? a. CH3CH2CH2CH2OH and CH3CH2CH2CH28r b. CH3CH2CH2CH2OH and CH3CH2CH2CH2CH2CH2CH3 c....

  • 2. A solution containing a mixture of naphthalene, benzoic acid, and benzaldehyde is analyzed via TLC...

    2. A solution containing a mixture of naphthalene, benzoic acid, and benzaldehyde is analyzed via TLC and GC. Use the structures and properties of the compounds to aid in answering the following questions. A. In the TLC experiment, the mixture is spotted on a silica TLC plate and eluted with a 1:1 mixture of hexanes and ethyl acetate. Three spots are observed on the plate, with Re values of 0.25, 0.58, and 0.74. Indicate which spot corresponds to which compound....

  • Pre Lab Questions 1. Complete the following table: Compound Acetanilide (A) Benzophenone (B) Mandelic acid (C) Benzi...

    Pre Lab Questions 1. Complete the following table: Compound Acetanilide (A) Benzophenone (B) Mandelic acid (C) Benzil (D) Benzoic acid (E) Structure Solubility in hexanes Solubility in ethyl acetate 2. Using the following diagram of a TLC plate, answer the following questions: solvent front a) Which compound is more polar if the stationary phase is silica gel? b) True or False: If the solvent mixture was made less polar, the compounds would move farther. c) Use a ruler and calculate...

  • 3. If the TLC plate development had stopped before the solvent front reached the top of...

    3. If the TLC plate development had stopped before the solvent front reached the top of the TLC plate (i.e. maybe it reached the middle of the TLC plate when it was stopped, instead): a) Would the Rf values have been affected? If so, how? If not, why not? Give a numerical example to support your answer. b) Would the size of the spots have been affected? If so, how? If not, why not? (Hint: think about the diffusion of...

ADVERTISEMENT
Free Homework Help App
Download From Google Play
Scan Your Homework
to Get Instant Free Answers
Need Online Homework Help?
Ask a Question
Get Answers For Free
Most questions answered within 3 hours.
ADVERTISEMENT
ADVERTISEMENT
ADVERTISEMENT