The given 2 compounds belong to alcohol and ketone family hence
they can be separated using extraction
techniques using appropriate solvents. Since the first compound is
a simple alkane alcohol it should be soluble
in water and the other ketonic compound
should be soluble in methylene chloride.
You will observe the
separation of aqueous and organic layer, to increase the
effectiveness of separation salts like NH4Cl can be
added.
The organic layer can be washed with alkaline
Na2CO3 to make it pure. Further TLC can be
employed to separate
and identify the compounds effectively.
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