Sort these statemetns describing requirements for suitable solvents for rexrystalization. Statements describing requirements for suitable solvents...
Sort these statemetns describing requirements for suitable solvents for rexrystalization.
Homework Answers
Hot recrystallisation is a method used for the purification of a substance by dissolving it in a hot solvent
If the compound is soluble in the hot solvent, impurity is insoluble and vice-versa.
The solvent should not dissolve the compound when cold. This statement is true.
The solvent should not dissolve the compound while hot. This statement is false.
The solvent should dissolve the compound while cold. This statement is false.
The solvent should dissolve the compound while hot. This statement is true.
The solvent should either dissolve the impurities at all temperatures or not dissolve the impurities at all. This statement is true.
The solvent should chemically react with the compound. This statement is false.
The solvent should not chemically react with the compound. This statement is true.
Ans: Part aThe solvent should not dissolve the compound when cold. This statement is true.
Part bThe solvent should not dissolve the compound while hot. This statement is false.
Part cThe solvent should dissolve the compound while cold. This statement is false.
Part dThe solvent should dissolve the compound while hot. This statement is true.
Part eThe solvent should either dissolve the impurities at all temperatures or not dissolve the impurities at all. This statement is true.
Part fThe solvent should chemically react with the compound. This statement is false.
Part gThe solvent should not chemically react with the compound. This statement is true.
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Sort these statemetns describing requirements for suitable solvents for rexrystalization.
Statements describing requirements for suitable solvents...
please answer all parts I am trying to check my answers. Recrystallization of Acetanilide Recrystallization is...
please answer all parts I am trying to check my
answers.
Recrystallization of Acetanilide Recrystallization is an important method used by chemists to purify solid compounds. When a chemist conducts a chemical reaction as shown in Scheme 1, it will rarely go to 100% completion, and will frequently produce byproducts. These byproducts and some of the unreacted starting materials will be present in the end as impurities. Chemists need ways to remove these unwanted impurities so they can isolate their...
Choose four requirements that must be met when choosing a solvent for recrystallization. Solute must be...
Choose four requirements that must be met when choosing a solvent for recrystallization. Solute must be soluble both at room temperature and the boiling point. Solvent must be easily removed (i.e., have a low boiling point and high vapor pressure). Solute may react with the solvent, as long as the reaction is incomplete. Impurities must be insoluble at the boiling point or soluble at room temperature. A small amount of crystals should be obtained. A fine powder should be obtained...
Benzydrol will be recrystallized from hexane during this experiment. Please identify the following statements about recrystallization...
Benzydrol will be recrystallized from hexane during this experiment. Please identify the following statements about recrystallization as true or false. Select all that are True. 1 Start heating the flask with just enough solvent in the flask to cover the sample. 2 When you collect your crystals you can wash them with a small amount of the recrystallization solvent, but you should cool the solvent down in an ice bath before using it. 3 If you are short on time,...
4c. Identify from the list below characteristics of an a organic solid. (Circle all choices that...
4c. Identify from the list below characteristics of an a organic solid. (Circle all choices that apply) (4 points) (or a solvent mixture) to recrystallize a crude t should chemically react with the substance to be recrysta (8) The solvent should completely dissolve soluble impurit G) The solvent should not dissolve insoluble impurities even when it is (D) At room tempe rities even when it is boiled. t should have very low solubility of the substance to be recrystalized The...
please provide clear answers. Thank you! 1. (8 pts) A crude reaction product (50 mg) is...
please provide clear answers.
Thank you!
1. (8 pts) A crude reaction product (50 mg) is to be purified by recrystallization from a single solvent. a) (5 pts) The crude solubility in ethanol at boiling temperature (BT) is 50 mg/mL and at O'C is 5 mg/mL. Read the statements and fill in True or False Describe in a few words the reason. True False Describe reason for true or false Statement The crude was dissolved in 5 mL of hot...
Please right an in depth discussion about part C. We we’re not able to get any...
Please right an
in depth discussion about part C. We we’re not able to get any
recrystallization from our unknown. Talk about possible failures
that could of happen that prevented us to not get any or our
unknown to recrystallize. Thanks so much!
Experiment 1: Solids: Recrystallization and Melting Point Learning Outcomes: Upon completion of this lab, students will be able to perform the technique of recrystallization of an impure solid as well as be able to determine an appropriate...
Which property or properties would be the most useful in characterizing an organic compound that a...
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You will apply what you have learned earlier in the semester when performing the Acid-Base Extraction...
You will apply what you have learned earlier in the semester when performing the Acid-Base Extraction experiment to perform a different separation: that of an organic neutral compound and organic base. You will also need to purify and characterize these compounds. You will have one lab period to execute your plan for separating the assigned mixture given below. There will be a 1:1 (by mass) mixture placed in the lab: 1,4-dichlorobenzene/ethyl 4-aminobenzoate. You will take approximately 1 g of your...
Discussion Questions The structures of acetanilide and malonic acid are provided below 1. For each structure,...
Discussion Questions The structures of acetanilide and malonic acid are provided below 1. For each structure, draw circles around the polar and nonpolar regions of the molecule, and label each circled regiorn with the type of intermolecular attractive force it can use to interact with other molecules. Acetanilide Malonic Acid но CH2 OH 2. Now-thoroughly explain (on the basis of polarity/nonpolarity and intermolecular attractive forces) how the acetanilide was separated from the malonic acid by recrystallization from water. And explain...
1. Why do soluble impurities affect the melting point while insoluble impurities are expected not to...
1. Why do soluble impurities affect the melting point while insoluble impurities are expected not to affect the melting point? (3 points) 2. Why cold solvents are preferred during recrystallization and when is recrystallization selected vs other purification techniques you have learned during 3210 labs. (3 points) 3. The solid compound "X" has two components (A and B). After heating the solid powder (X), one component (A) is left and the other component (B) evaporated directly. Comment on the nature...
please answer all parts I am trying to check my
answers.
Recrystallization of Acetanilide Recrystallization is an important method used by chemists to purify solid compounds. When a chemist conducts a chemical reaction as shown in Scheme 1, it will rarely go to 100% completion, and will frequently produce byproducts. These byproducts and some of the unreacted starting materials will be present in the end as impurities. Chemists need ways to remove these unwanted impurities so they can isolate their...
Choose four requirements that must be met when choosing a solvent for recrystallization. Solute must be soluble both at room temperature and the boiling point. Solvent must be easily removed (i.e., have a low boiling point and high vapor pressure). Solute may react with the solvent, as long as the reaction is incomplete. Impurities must be insoluble at the boiling point or soluble at room temperature. A small amount of crystals should be obtained. A fine powder should be obtained...
4c. Identify from the list below characteristics of an a organic solid. (Circle all choices that apply) (4 points) (or a solvent mixture) to recrystallize a crude t should chemically react with the substance to be recrysta (8) The solvent should completely dissolve soluble impurit G) The solvent should not dissolve insoluble impurities even when it is (D) At room tempe rities even when it is boiled. t should have very low solubility of the substance to be recrystalized The...
please provide clear answers.
Thank you!
1. (8 pts) A crude reaction product (50 mg) is to be purified by recrystallization from a single solvent. a) (5 pts) The crude solubility in ethanol at boiling temperature (BT) is 50 mg/mL and at O'C is 5 mg/mL. Read the statements and fill in True or False Describe in a few words the reason. True False Describe reason for true or false Statement The crude was dissolved in 5 mL of hot...
Please right an
in depth discussion about part C. We we’re not able to get any
recrystallization from our unknown. Talk about possible failures
that could of happen that prevented us to not get any or our
unknown to recrystallize. Thanks so much!
Experiment 1: Solids: Recrystallization and Melting Point Learning Outcomes: Upon completion of this lab, students will be able to perform the technique of recrystallization of an impure solid as well as be able to determine an appropriate...
Which property or properties would be the most useful in characterizing an organic compound that a solid at room temperature. melting point 1L refractive index IL boiling pointIV. color is a solid at room a. b. II and IV f. II and II1 js a lvguid a rooeriy or propertis would be the most usctaul in characteriving an organic compound that I. melting point I. refractive index III. boiling pointIV. color a. b. III and IV c.? f. II and...
Discussion Questions The structures of acetanilide and malonic acid are provided below 1. For each structure, draw circles around the polar and nonpolar regions of the molecule, and label each circled regiorn with the type of intermolecular attractive force it can use to interact with other molecules. Acetanilide Malonic Acid но CH2 OH 2. Now-thoroughly explain (on the basis of polarity/nonpolarity and intermolecular attractive forces) how the acetanilide was separated from the malonic acid by recrystallization from water. And explain...
1. Why do soluble impurities affect the melting point while insoluble impurities are expected not to affect the melting point? (3 points) 2. Why cold solvents are preferred during recrystallization and when is recrystallization selected vs other purification techniques you have learned during 3210 labs. (3 points) 3. The solid compound "X" has two components (A and B). After heating the solid powder (X), one component (A) is left and the other component (B) evaporated directly. Comment on the nature...
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