Calculate th reaction mass efficiency for the reaction. Note that 20 pipettes drops of any liquid...
Experiment Write Up Proposal You will write up a synthesis procedure for one reaction that could be potentially run in a face- to-face Chem 2321 lab session. Your proposal will include an introduction and procedure. The procedure will include step-by-step instructions for running the reaction (including reaction monitoring), work-up. (product isolation and purification), and analysis (characterization). You will need to include sample calculations for percent yield and provide sample spectra analysis. You must upload your proposal as a single document...
i uploaded everything that was given. Where would I find the experiemental values? Complete the calculation summary below. READ THE EXPERIMENTAL DISCUSSION FIRST! REPORT ALL ANSWERS TO THE CORRECT SIGNIFICANT FIGURES. SHOW CALCULATION SET-UP on the next page. PART B: Molarity Determination via Solution Stoichiometry 7.625 g Mass of Empty 50 mL Beaker 7.976 g Mass of Beaker and NaCl (final heating) Mass of NaCl Produced (Experimental Yield of NaCl) moles Moles of Na,CO, Consumed 0.00500 Liter Volume of Na,CO,...
Grignard Reaction with a Ketone: Triphenylmethanol Introduction: The purpose of this lab is to prepare phenylmagnesium bromide, a Grignard reagent, and react it with benzophenone to give triphenylmethanol. Grignard reagents are very reactive and must be synthesized in an environment free of water or any other source of potential proton donor. Once made, the Grignard reagent will do a nucleophilic attack on the carbonyl carbon of the ketone, benzophenone. The result is an alkoxide that is then protonated to give...
(If you need any more information just let me know) Determine the limiting reagent for the preparation of 2-bromo-2-methylbutane and calculate the theoretical yield of product. 1 CHEM-2223 Organic Chemistry Laboratory I Exp. 7: Synthesis of 2-chloro-2-methylbutane In this reaction a tertiary alcohol, 2-methyl-2-butanol, is converted to a tertiary halide, 2-chloro- 2-methylbutane through a SN1 reaction. 1) Chemicals 2-Methyl-2-butanol Hydrochloric acid, HCl (12 M) Saturated sodium bicarbonate Saturated sodium chloride (380 g/L) Anhydrous sodium sulfate...
Give a detailed mechanism for this reaction and give a separation scheme NUCLEOPHILIC ACYL SUBSTITUTION: Synthesis of an Ester Isoamyl acetate (Banana Oil) Purpose This experiment demonstrat and alcohol. The technique of refluxing the reaction mixture is introduced. es the procedure for the synthesis of an ester from a carboxylic acid Esters are an important functional group in organic chemistry, and esters are found widely distributed in nature. Many lower molecular weight esters are associated with natural fuit flavors and...