1. Is in refrence to a fischer esterification reaction using an alcohol and carboxylic acid to synthesis octyl acetate.
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Thank you in advance!
1) H2SO4 is a catalyst and a dehydrating agent. If we do not add
H2SO4 to the reaction, the reaction will not proceed.
The ester is washed with bicarbonate solution before distilling
because bicarbonate is a very weak base and neutralizes any acid
present. Thus we can remove added H2SO4 and unreacted carboxylic
acid from the ester.
2. We do not distill the citrus and coconut esters as they have high boiling points. We distill the banana, pear and pineapple ester as they have low boiling points.
3. The IR contains strong and broad peak around 3331 which indicates presence of -OH group. This indicates presence of unreated alcohol in the reaction. Hence, the reaction is incomplete and the product ester is impure.
1. Is in refrence to a fischer esterification reaction using an alcohol and carboxylic acid to...
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