Convert Cyclohexanol to Cyclohexene via a Acid-Catalyzed Dehydration reaction 1. Why does the product ‘come over’...
Convert Cyclohexanol to Cyclohexene via a Acid-Catalyzed Dehydration reaction
1. Why does the product ‘come over’ after being formed? Please
think about the properties of the starting material and
product.
2. If there was no acid present, would you expect to get a product?
Why/why not?
3. If we start off with 10 molecules of the starting alcohol and
only get an 80% yield, how many molecules will we find in the
product flask?
4. Look up the concept of 'moles' and then answer question 3 again,
but this time consider if we started with 10 grams of cyclohexanol.
Consult your instructor if you have problems understanding the
concept of moles.
Homework Answers
Add Answer to:
Convert Cyclohexanol to Cyclohexene via a Acid-Catalyzed
Dehydration reaction
1. Why does the product ‘come over’...
1) Draw a complete scheme and mechanism for the dehydration of cyclohexanol to cyclohexene. Propose a...
1) Draw a complete scheme and mechanism for the dehydration of cyclohexanol to cyclohexene. Propose a scheme and conditions for the preparation of cyclohexanol from cyclohexene. How would you track the progress of your reactions and confirm product identification? 2) Create a chart comparing E1, E2, SN1 and SN2 reactions. Be detailed and cover: structure of RX, reactivity of nucleophile, concentration of nucleophile, solvent and stereochemistry. 3) Mixing cyclohexanol with phosphoric acid is an exothermic process, whereas the production of...
This is the IR for CYclohexanol and acid This is the NMR of product for the...
This is the IR for CYclohexanol and acid
This is the NMR of product for the acid-catalyzed elimination
from the cyclohexanol
Saturation results
Assume, that when bromine is added to the product, the resulting
mixture is colorless. If potassium permanganate is added to the
product, the formation of a brown precipitate is observed.
starting material info: product and reactants
HERE ARE TWO MORE QUESTIONS:
5. Discussion: Explain how your data gives evidence of correct product identity and purity. Include: a....
convert from moles to g or ml no structure was given the starting product is ketal...
convert from moles to g or ml
no structure was given
the starting product is ketal alcohol
yes convert 0.01 moles of the starting material into
grams or ml
Keto-alcohol (3). The ketal protecting group is removed by mixing 0.01 moles of ketal- alcohol 2 with 2 mL of water, 5-7 drops of concentrated hydrochloric acid, and 15 mL of reagent grade acetone. (Excess ketal-alcohol should be placed in a vial, labeled, and submitted to the instructor). The mixture is...
Working on the questions at the end of this lab report (see above). I need help answering questio...
Working on the questions at the end of this lab report
(see above). I need help answering questions 2, 3, and 4 completely
and thoroughly. Thank you!
s, until the I hexano 1 clean disti CYCLOHEXENE from CYCLOHEXANOL be dehydrated with solfuric acid to yield cyclohexene and waterf Add a 0°C (record ct and cal H,SO + H20 ainer. s in purification of any crude product are (a) the preliminary separation of the product from the reaction mixture by distillation...
Convert playlist Diction QUESTIONS 1. (2 Points) Why is it essential to keep the diazonium salt...
Convert playlist Diction QUESTIONS 1. (2 Points) Why is it essential to keep the diazonium salt at zero degrees while you are preparing the sodium 2-naphthoxide solution? 2. (2 Points) Would you need to use sodium carbonate for the diazotization of meta- nitroaniline? Explain your answer. 3. (2 Points) What would be the IUPAC name for the azo dye if you would have used p-chloroaniline instead of sulfanilic acid? Experiment 12 4. (4 Points) Calculate the theoretical yield for Orange...
POGIL-Stoichiometry How do chemists use balanced chemical equations? got bit D 23 mosquitoes? 10 He got...
POGIL-Stoichiometry How do chemists use balanced chemical equations? got bit D 23 mosquitoes? 10 He got Mol-aria Why? Chemists use balanced chemical equations as a basis to calculate how much reactant is needed or product is formed in a reaction. This is called Stoichiometry- (stoi-key-ah-meh-tree) Another way of looking at it is using the mole ratio from the balanced equation and information about one compound in the reaction to determine information about another compound in the equation. A mole ratio...
Please explain what is going on in this lab for STEP 3. what are some important...
Please explain what is going on in this lab for STEP 3. what
are some important factors?
Multistep Synthesis Preparation of 4,4-Diphenyl-3-buten-2-one! This experiment illustrates se multistep synthesis, in which the the next. This process is very common iment illustrates several important concepts of organic synthesis. It is a synthesis, in which the product of one reaction becomes the starting material of This process is very common in industry and research, and demands careful to vields and techniques. The experiment...
Synthesis of 1-Bromobutane: An SN2 Reaction Pre-Laboratory Exercises PRE-LABORATORY EXERCISES NAME: Cynthesis of 1-Bromobutane: An SN...
Synthesis of 1-Bromobutane: An SN2 Reaction Pre-Laboratory
Exercises
PRE-LABORATORY EXERCISES NAME: Cynthesis of 1-Bromobutane: An SN 2 Reaction Butylbromide was prepared by refluxing in a 100-ml round bottomed flask a solution containing 13:35 Br 15 ml of water, 10 mL of n-butyl alcohol. 15 ml of concentrated H.SO. and a few boiling stories, 1. 2. R." d 1.275 laborales Nel CH3CH2CH2CH2OH + NaBr H2SO4 Superletalyst CHCH2CH2CHBr + NaHSO + HO (eq. 16) 1-butanol bp 118 C 1-bromobutane d 0.810 bp...
Exercise 2 Separation of a Mixture Based on Acid-Base Properties One purpose of this exercise is...
Exercise 2 Separation of a Mixture Based on Acid-Base Properties One purpose of this exercise is to learn how to use a separatory funnel to extract a single component away from other compounds in solution. To do so, we will apply the principles of solubility and acid-base behavior you’re seeing in class. One of the compounds is neutral in the acid-base sense. It has no ability to either donate or accept a proton from an aqueous solution, and will remain...
Grignard reagent THE GRIGNARD REAGENT-PREPARATION AND REACTION In this experiment, you will prepa...
i need help with the postlab questions please
Grignard reagent THE GRIGNARD REAGENT-PREPARATION AND REACTION In this experiment, you will prepare a Grignard reagent, phenyl magnesium bromide, from bromobenzene and magnesium metal. The Grignard reagent will then react with methyl benzoate to form triphenylmethanol. Introduction Grignard reagents, such as organomagnesium halides, were discovered in 1910 by French chemist Victor Grignard. The Grignard reaction is one of the most general methods for carbon- carbon bond formation in all of organic chemistry....
This is the IR for CYclohexanol and acid
This is the NMR of product for the acid-catalyzed elimination
from the cyclohexanol
Saturation results
Assume, that when bromine is added to the product, the resulting
mixture is colorless. If potassium permanganate is added to the
product, the formation of a brown precipitate is observed.
starting material info: product and reactants
HERE ARE TWO MORE QUESTIONS:
5. Discussion: Explain how your data gives evidence of correct product identity and purity. Include: a....
convert from moles to g or ml
no structure was given
the starting product is ketal alcohol
yes convert 0.01 moles of the starting material into
grams or ml
Keto-alcohol (3). The ketal protecting group is removed by mixing 0.01 moles of ketal- alcohol 2 with 2 mL of water, 5-7 drops of concentrated hydrochloric acid, and 15 mL of reagent grade acetone. (Excess ketal-alcohol should be placed in a vial, labeled, and submitted to the instructor). The mixture is...
Working on the questions at the end of this lab report
(see above). I need help answering questions 2, 3, and 4 completely
and thoroughly. Thank you!
s, until the I hexano 1 clean disti CYCLOHEXENE from CYCLOHEXANOL be dehydrated with solfuric acid to yield cyclohexene and waterf Add a 0°C (record ct and cal H,SO + H20 ainer. s in purification of any crude product are (a) the preliminary separation of the product from the reaction mixture by distillation...
Convert playlist Diction QUESTIONS 1. (2 Points) Why is it essential to keep the diazonium salt at zero degrees while you are preparing the sodium 2-naphthoxide solution? 2. (2 Points) Would you need to use sodium carbonate for the diazotization of meta- nitroaniline? Explain your answer. 3. (2 Points) What would be the IUPAC name for the azo dye if you would have used p-chloroaniline instead of sulfanilic acid? Experiment 12 4. (4 Points) Calculate the theoretical yield for Orange...
POGIL-Stoichiometry How do chemists use balanced chemical equations? got bit D 23 mosquitoes? 10 He got Mol-aria Why? Chemists use balanced chemical equations as a basis to calculate how much reactant is needed or product is formed in a reaction. This is called Stoichiometry- (stoi-key-ah-meh-tree) Another way of looking at it is using the mole ratio from the balanced equation and information about one compound in the reaction to determine information about another compound in the equation. A mole ratio...
Please explain what is going on in this lab for STEP 3. what
are some important factors?
Multistep Synthesis Preparation of 4,4-Diphenyl-3-buten-2-one! This experiment illustrates se multistep synthesis, in which the the next. This process is very common iment illustrates several important concepts of organic synthesis. It is a synthesis, in which the product of one reaction becomes the starting material of This process is very common in industry and research, and demands careful to vields and techniques. The experiment...
Synthesis of 1-Bromobutane: An SN2 Reaction Pre-Laboratory
Exercises
PRE-LABORATORY EXERCISES NAME: Cynthesis of 1-Bromobutane: An SN 2 Reaction Butylbromide was prepared by refluxing in a 100-ml round bottomed flask a solution containing 13:35 Br 15 ml of water, 10 mL of n-butyl alcohol. 15 ml of concentrated H.SO. and a few boiling stories, 1. 2. R." d 1.275 laborales Nel CH3CH2CH2CH2OH + NaBr H2SO4 Superletalyst CHCH2CH2CHBr + NaHSO + HO (eq. 16) 1-butanol bp 118 C 1-bromobutane d 0.810 bp...
i need help with the postlab questions please
Grignard reagent THE GRIGNARD REAGENT-PREPARATION AND REACTION In this experiment, you will prepare a Grignard reagent, phenyl magnesium bromide, from bromobenzene and magnesium metal. The Grignard reagent will then react with methyl benzoate to form triphenylmethanol. Introduction Grignard reagents, such as organomagnesium halides, were discovered in 1910 by French chemist Victor Grignard. The Grignard reaction is one of the most general methods for carbon- carbon bond formation in all of organic chemistry....
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