Draw the acid-base reaction showing protonation of acetic anhydride by phosphoric acid (a strong acid). Pay attention to which atom is most basic.
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Draw the acid-base reaction showing protonation of acetic anhydride by phosphoric acid (a strong acid). Pay...
In the mechanism for formation of acetylsalicylic acid via reaction of salicylic acid with acetic anhydride, phosphoric acid acts as a catalyst by O cleaving an acetyl group from acetic anhydride via protonation of the bridging oxygen O neutralizing the hydroxide ion side product protonating the carbonyl oxygen in the acetic anhydride protonating the phenolic oxygen of salicylic acid Question 10 (3 points) What would be the predicted major product from the thermodynamically controlled dehydration of the following material OH
Salicylic acid and acetic anhydride are synthesized with phosphoric acid to catalyze the reaction to make acetylsalicylic acid (aspirin). How will you know if you have successfully synthesized acetylsalicylic acid? What compound will you have if you did NOT successfully synthesize acetylsalicylic acid, and how can you confirm it?
1. For the acetylation of ferrocene, ferrocene is mixed with acetic anhydride and 85% phosphoric acid and heated for 20 mins. Why is phosphoric acid used rather than a stronger acid such as sulfuric acid? 2. For the oxidation of ferrocene, NH4[PF6] is added to the reaction mixture of ferrocene, acetone, distilled water, and anhydrous FeCl3. What is the purpose of adding NH4[PF6]?
How could the yield of diacetylated product be increased? (this reaction associated with Acetylation of ferrocene in present with acetic anhydride and phosphoric acid, diacetylaeted is minor product in the reaction)
Question 7 What is the nucleophile in the following reaction Ferrocene + acetic anhydride + Phosphoric acid Acetyl ferrocene + acetic acid Ferrocene A B. Acyllium ion oc. Fe2+ D.H3PO4 Question 8 is specifically important because it has the highest melting point and prevents lipstick from melting. A) candelilla wax B) Carnauba wax C) beeswax D) Natural Waxes А B D Question 9 Which reaction is Fischer Esterification A) CH3COCI + CH3CH2OH → CH3COOCH2CH3 + HCI B)(CH3CO)20 + CH3CH2OH →...
3. 0.69g of salicylic acid was reacted with 0.6g acetic anhydride in the presence of concentrated phosphoric acid to yield 0.80g of acetyl salicylic acid (see below). Determine the limiting reagent and percent yield. C-CH OH COOH CH, COOH CHC Salicylic acid MW 138.12. mp 159C Acetic anhydride Acetylsalicylic acid M W 102.09. bp 140CMW 180.15. mp 128-1370 4. How do you account for the smell of vinegar when an old bottle of aspirin opened?
In this lab you are synthesizing acetylsalicylic acid (ASA) from salicylic acid using acetic anhydride, with phosphoric acid as a catalyst. If the amount of salicylic acid at the start of the reaction was 1.05 g, what is the theoretical yield of ASA in g? Assume acetic anhydride is in excess.
Show the mechanism of the acid catalyzed reaction of an alcohol with acetic anhydride, indicating the involvement of the strong acid catalyst in the reaction. H2SO4 (cat.) R'OH ROR ROH ROD +
In this lab you are synthesizing acetylsalicylic acid (ASA) from salicylic acid using acetic anhydride, with phosphoric acid as a catalyst. If the amount of salicylic acid at the start of the reaction was 1.05 g, what is the theoretical yield of ASA in g? Assume acetic anhydride is in excess. HINT: The structures of all the compounds you need are in the lab manual.
1) Which reactant, salicylic acid or acetic anhydride, is in excess? Show your work. 2) If you were to use 3.17 g of starting material, how much product would you expect? Again, show your work. 3) Why is phosphoric acid added to the reaction? 4) A small amount of water is added at the end of the reaction to react with the excess acetic anhydride. Show a balanced equation for that reaction. 5) Explain the purpose of the FeCl3 test...